SIST EN ISO 5264-2:2003
(Main)Pulps - Laboratory beating - Part 2: PFI mill method (ISO 5264-2:2002)
Pulps - Laboratory beating - Part 2: PFI mill method (ISO 5264-2:2002)
ISO 5264-2:2002 specifies a method, using a PFI mill, for the laboratory beating of pulp. The description is limited to the sampling and beating of the pulp, the withdrawal and distribution of samples, and the beating equipment.
NOTE Beating is a preliminary step in testing the physical properties of pulp.
In principle, this method is applicable to all kinds of chemical and semi-chemical pulps. In practice, the method may not give satisfactory results with certain pulps with extremely long fibres.
Faserstoffe - Labormahlung - Teil 2: PFI-Mühle Verfahren (ISO 5264-2:2002)
Dieser Teil von ISO 5264 legt ein Verfahren zur Labormahlung von Zellstoff unter Verwendung einer PFI-Mühle fest. Die Beschreibung ist auf die Probenahme und das Mahlen von Zellstoff, das Austragen und Verteilen der Durchschnittsprobe sowie die Mahleinrichtung beschränkt.
Anmerkung Das Mahlen ist die Vorstufe zur Prüfung der physikalischen Eigenschaften von Zellstoff.
Grundsätzlich ist dieses Verfahren auf alle Arten von Chemie- und Halbzellstoff anwendbar. In der Praxis kann dieses Verfahren bei extrem langfaserigen Zellstoffen keinDieser Teil von ISO 5264 legt ein Verfahren zur Labormahlung von Zellstoff unter Verwendung einer PFI-Mühle fest. Die Beschreibung ist auf die Probenahme und das Mahlen von Zellstoff, das Austragen und Verteilen der Durchschnittsprobe sowie die Mahleinrichtung beschränkt.
ANMERKUNG Anmerkung Das Mahlen ist die Vorstufe zur Prüfung der physikalischen Eigenschaften von Zellstoff.
Grundsätzlich ist dieses Verfahren auf alle Arten von Chemie- und Halbzellstoff anwendbar. In der Praxis kann dieses Verfahren bei extrem langfaserigen Zellstoffen keine zufriedenstellenden Ergebnisse liefern.
Pâtes - Raffinage de laboratoire - Partie 2: Méthode au moulin PFI (ISO 5264-2:2002)
L'ISO 5264:2002 spécifie une méthode utilisant un moulin PFI pour le raffinage de la pâte en laboratoire. La description se limite à l'échantillonnage et au raffinage en pile de la pâte, au prélèvement et à la répartition des échantillons, ainsi qu'à l'appareillage de raffinage.
NOTE Le raffinage en pile est une phase préliminaire dans la détermination des propriétés physiques d'une pâte.
En principe, la présente méthode est applicable à tous les types de pâtes chimiques et mi-chimiques. En pratique, cette méthode peut ne pas donner de résultats satisfaisants avec certaines pâtes à fibres extrêmement longues.
Vlaknine - Laboratorijsko mletje - 2. del: Metoda z mlinom PFI (ISO 5264-2:2002)
General Information
Relations
Standards Content (Sample)
SLOVENSKI STANDARD
SIST EN ISO 5264-2:2003
01-september-2003
1DGRPHãþD
SIST EN 25264-2:2000
Vlaknine - Laboratorijsko mletje - 2. del: Metoda z mlinom PFI (ISO 5264-2:2002)
Pulps - Laboratory beating - Part 2: PFI mill method (ISO 5264-2:2002)
Faserstoffe - Labormahlung - Teil 2: PFI-Mühle Verfahren (ISO 5264-2:2002)
Pâtes - Raffinage de laboratoire - Partie 2: Méthode au moulin PFI (ISO 5264-2:2002)
Ta slovenski standard je istoveten z: EN ISO 5264-2:2002
ICS:
85.040 Vlaknine Pulps
SIST EN ISO 5264-2:2003 en
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.
---------------------- Page: 1 ----------------------
SIST EN ISO 5264-2:2003
---------------------- Page: 2 ----------------------
SIST EN ISO 5264-2:2003
EUROPEAN STANDARD
EN ISO 5264-2
NORME EUROPÉENNE
EUROPÄISCHE NORM
November 2002
ICS 85.040 Supersedes EN 25264-2:1994
English version
Pulps - Laboratory beating - Part 2: PFI mill method (ISO 5264-
2:2002)
Pâtes - Raffinage de laboratoire - Partie 2: Méthode au Faserstoffe - Labormahlung - Teil 2: PFI-Mühle Verfahren
moulin PFI (ISO 5264-2:2002) (ISO 5264-2:2002)
This European Standard was approved by CEN on 30 September 2002.
CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European
Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national
standards may be obtained on application to the Management Centre or to any CEN member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation
under the responsibility of a CEN member into its own language and notified to the Management Centre has the same status as the official
versions.
CEN members are the national standards bodies of Austria, Belgium, Czech Republic, Denmark, Finland, France, Germany, Greece,
Iceland, Ireland, Italy, Luxembourg, Malta, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
Management Centre: rue de Stassart, 36 B-1050 Brussels
© 2002 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 5264-2:2002 E
worldwide for CEN national Members.
---------------------- Page: 3 ----------------------
SIST EN ISO 5264-2:2003
EN ISO 5264-2:2002 (E)
CORRECTED 2003-02-05
Foreword
This document (EN ISO 5264-2:2002) has been prepared by Technical Committee ISO/TC 6
"Paper, board and pulps" in collaboration with Technical Committee CEN/TC 172 "Pulp, paper
and board", the secretariat of which is held by DIN.
This European Standard shall be given the status of a national standard, either by publication of
an identical text or by endorsement, at the latest by May 2003, and conflicting national standards
shall be withdrawn at the latest by May 2003.
This document supersedes EN 25264-2:1994.
According to the CEN/CENELEC Internal Regulations, the national standards organizations of
the following countries are bound to implement this European Standard: Austria, Belgium, Czech
Republic, Denmark, Finland, France, Germany, Greece, Iceland, Ireland, Italy, Luxembourg,
Malta, Netherlands, Norway, Portugal, Spain, Sweden, Switzerland and the United Kingdom.
Endorsement notice
The text of ISO 5264-2:2002 has been approved by CEN as EN ISO 5264-2:2002 without any
modifications.
NOTE Normative references to International Standards are listed in Annex ZA (normative).
2
---------------------- Page: 4 ----------------------
SIST EN ISO 5264-2:2003
EN ISO 5264-2:2002 (E)
Annex ZA
(normative)
Normative references to international publications
with their relevant European publications
This European Standard incorporates by dated or undated reference, provisions from other
publications. These normative references are cited at the appropriate places in the text and the
publications are listed hereafter. For dated references, subsequent amendments to or revisions of
any of these publications apply to this European Standard only when incorporated in it by
amendment or revision. For undated references the latest edition of the publication referred to
applies (including amendments).
NOTE Where an International Publication has been modified by common modifications, indicated
by (mod.), the relevant EN/HD applies.
Publication Year Title EN Year
ISO 638 1978 Pulps – Determination of dry EN 20638 1993
matter content
ISO 4119 1995 Pulps - Determination of stock EN ISO 4119 1996
concentration
ISO 5263 1995 Pulps - Laboratory wet EN ISO 5263 1997
disintegration
ISO 5267-1 1999 Pulps - Determination of EN ISO 5267-1 2000
drainability - Part 1: Schopper-
Riegler method
ISO 7213 1981 Pulps - Sampling for testing EN 27213 1993
3
---------------------- Page: 5 ----------------------
SIST EN ISO 5264-2:2003
---------------------- Page: 6 ----------------------
SIST EN ISO 5264-2:2003
INTERNATIONAL ISO
STANDARD 5264-2
Second edition
2002-11-15
Pulps — Laboratory beating —
Part 2:
PFI mill method
Pâtes — Raffinage de laboratoire —
Partie 2: Méthode au moulin PFI
Reference number
ISO 5264-2:2002(E)
© ISO 2002
---------------------- Page: 7 ----------------------
SIST EN ISO 5264-2:2003
ISO 5264-2:2002(E)
PDF disclaimer
This PDF file may contain embedded typefaces. In accordance with Adobe's licensing policy, this file may be printed or viewed but shall not be
edited unless the typefaces which are embedded are licensed to and installed on the computer performing the editing. In downloading this file,
parties accept therein the responsibility of not infringing Adobe's licensing policy. The ISO Central Secretariat accepts no liability in this area.
Adobe is a trademark of Adobe Systems Incorporated.
Details of the software products used to create this PDF file can be found in the General Info relative to the file; the PDF-creation parameters
were optimized for printing. Every care has been taken to ensure that the file is suitable for use by ISO member bodies. In the unlikely event
that a problem relating to it is found, please inform the Central Secretariat at the address given below.
© ISO 2002
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized in any form or by any means,
electronic or mechanical, including photocopying and microfilm, without permission in writing from either ISO at the address below or ISO's
member body in the country of the requester.
ISO copyright office
Case postale 56 CH-1211 Geneva 20
Tel. + 41 22 749 01 11
Fax + 41 22 749 09 47
E-mail copyright@iso.ch
Web www.iso.ch
Printed in Switzerland
©
ii ISO 2002 – All rights reserved
---------------------- Page: 8 ----------------------
SIST EN ISO 5264-2:2003
ISO 5264-2:2002(E)
Contents Page
1 Scope . 1
2 Normative references . 1
3 Principle . 1
4 Apparatus and auxiliary materials . 1
5 Sampling . 2
6 Preparation of sample . 2
7 Procedure . 2
8 Test report . 4
Annexes
A PFI mill. 5
B Control and maintenance of the PFI mill. 7
C Checking the stability of the PFI mill . 9
Bibliography. 10
©
ISO 2002 – All rights reserved iii
---------------------- Page: 9 ----------------------
SIST EN ISO 5264-2:2003
ISO 5264-2:2002(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO
member bodies). The work of preparing International Standards is normally carried out through ISO technical
committees. Each member body interested in a subject for which a technical committee has been established has
the right to be represented on that committee. International organizations, governmental and non-governmental, in
liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical
Commission (IEC) on all matters of electrotechnical standardization.
International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 3.
Draft International Standards adopted by the technical committees are circulated to the member bodies for voting.
Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote.
Attention is drawn to the possibility that some of the elements of this part of ISO 5264 may be the subject of patent
rights. ISO shall not be held responsible for identifying any or all such patent rights.
International Standard ISO 5264-2 was prepared by Technical Committee ISO/TC 6, Paper, board and pulps,
Subcommittee SC 5, Test methods and quality specifications for pulps.
This second edition cancels and replaces the first edition (ISO 5264-2:1979), which has been technically revised.
ISO 5264 consists of the following parts, under the general title Pulps — Laboratory beating:
— Part 1: Valley beater method
— Part 2: PFI mill method
— Part 3: Jokro mill method
Annexes A and B form a normative part of this part of ISO 5264. Annex C is for information only.
©
iv ISO 2002 – All rights reserved
---------------------- Page: 10 ----------------------
SIST EN ISO 5264-2:2003
ISO 5264-2:2002(E)
Introduction
In view of the widespread use of the following beaters:
— Valley beater;
— PFI mill;
— Jokro mill;
it has been decided to provide guidance on the use of these beaters in order to achieve consistency of results with
each instrument. Although all three beaters show similar trends in the effect on pulp properties, there is no correlation
between the actual results obtained with the different types of beaters.
ISO 5264-1 specifies a method of laboratory beating using a Valley beater and ISO 5264-3 a method using a Jokro
mill.
Beating is a preliminary step in the preparation of laboratory sheets for testing the physical properties of pulps. In the
PFI mill, each beating is performed separately, i.e. a new test portion of unbeaten pulp is taken for each beating.
NOTE A complete test of physical properties normally comprises unbeaten pulp and several beatings of the same pulp, where
the beating is carried out for different numbers of roll revolutions. The number of roll revolutions depends on the type of pulp and
the beating load. After beating, the drainability is measured according to ISO 5267-1 or ISO 5267-2, and laboratory sheets are
prepared according to ISO 5269-1 or ISO 5269-2.
©
ISO 2002 – All rights reserved v
---------------------- Page: 11 ----------------------
SIST EN ISO 5264-2:2003
---------------------- Page: 12 ----------------------
SIST EN ISO 5264-2:2003
INTERNATIONAL STANDARD ISO 5264-2:2002(E)
Pulps — Laboratory beating —
Part 2:
PFI mill method
1 Scope
This part of ISO 5264 specifies a method, using a PFI mill, for the laboratory beating of pulp. The description is
limited to the sampling and beating of the pulp, the withdrawal and distribution of samples, and the beating
equipment.
NOTE Beating is a preliminary step in testing the physical properties of pulp.
In principle, this method is applicable to all kinds of chemical and semi-chemical pulps. In practice, the method may
not give satisfactory results with certain pulps having extremely long fibres.
2 Normative references
The following normative documents contain provisions which, through reference in this text, constitute provisions of
this part of ISO 5264. For dated references, subsequent amendments to, or revisions of, any of these publications do
not apply. However, parties to agreements based on this part of ISO 5264 are encouraged to investigate the
possibility of applying the most recent editions of the normative documents indicated below. For undated references,
the latest edition of the normative document referred to applies. Members of ISO and IEC maintain registers of
currently valid International Standards.
ISO 638, Pulps — Determination of dry matter content
ISO 4119, Pulps — Determination of stock concentration
ISO 5263, Pulps — Laboratory wet disintegration
ISO 5267-1, Pulps — Determination of drainability — Part 1: Schopper-Riegler method
ISO 5267-2, Pulps — Determination of drainability — Part 2: “Canadian Standard” freeness method
ISO 7213, Pulps — Sampling for testing
ISO 14487, Pulps — Standard water for physical testing
3 Principle
A measured amount of pulp at a specified stock concentration is beaten between a roll with bars and a smooth beater
housing, both rotating in the same direction, but at different peripheral speeds.
4 Apparatus and auxiliary materials
Ordinary laboratory equipment and the following.
©
ISO 2002 – All rights reserved 1
---------------------- Page: 13 ----------------------
SIST EN ISO 5264-2:2003
ISO 5264-2:2002(E)
4.1 PFI mill, as specified in annex A.
See normative annex B and informative annex C.
4.2 Disintegrator, as specified in ISO 5263.
4.3 Balance, capable of weighing the sample with an error of less than ± 0,2 g.
◦
4.4 Standard water, purified to an electrical conductivity � 0,25 mS/m at 25 C, as specified in ISO 14487.
4.5 A reference pulp, kept for beating-control purposes and stored for a time sufficiently long to avoid further
changes in physical properties. The reference pulp should, if possible, be of the same grade as that normally beaten
in the beating equipment concerned. Since some pulp grades are not stable, it might be necessary to choose
another grade.
To avoid the influence of storage time, the reference pulp should be kept at room temperature (not at too high a
relative humidity) in a dark and dust-free place.
NOTE Stored under the recommended conditions, the reference pulp will, in most cases, be stable for approximately 10 years.
Changes in the level of the tensile strength and tear strength values may be an indication that the reference pulp is no longer
stable. The stability can be checked by measuring the viscosity of the reference pulp, e.g. twice a year.
5 Sampling
If the beating is being done to evaluate a lot of pulp, the sample shall be selected in accordance with ISO 7213.
If the beating is done on another type of sample, report the source of the sample and, if possible, the sampling
procedure used.
Select the test portions so that they are representative of the gross sample received.
6 Preparation of sample
If the sample is wet or air-dry, weigh a test portion for the determination of dry-matter content in accordance with
ISO 638. If the sample is in the form of an aqueous pulp suspension, determine the dry matter content in accordance
with ISO 4119.
Take a test portion of the sample corresponding to (30,0± 0,5) g of oven-dry pulp. Do not cut pulp sheets and avoid
the use of cut edges. If the sample is in the form of machine-dried sheets or flash-dried slabs, soak the pulp
thoroughly in 0,5 litre of standard water (4.4) at room temperature for not less than 4h. Tear the soaked pulp into
pieces approximately 25 mm× 25 mm in size. It is essential that the pulp sample be thoroughly softened by soaking,
to ensure that the preliminary disintegration leads to only a minimal beating effect. Wet pulps may be disintegrated
without soaking.
7 Procedure
7.1 General
For each test portion (each degree of beating), carry out the following procedure.
7.2 Disintegration
Disintegrate the initially wet portion or the soaked test portion as described in ISO 5263. Use standard water (4.4) at
◦
...
Questions, Comments and Discussion
Ask us and Technical Secretary will try to provide an answer. You can facilitate discussion about the standard in here.