Standard Test Method for Measuring Non-Fibrous Content of Man-Made Rock and Slag Mineral Fiber Insulation

SIGNIFICANCE AND USE
Inorganic fibrous thermal insulation can contain varying amounts of non-fibrous material. Non-fibrous material does not contribute to the insulating value of the insulation and therefore a procedure for determining that amount is desirable. Several specifications refer to shot content and percent (%) retained on various screen sizes determined by this test method.
SCOPE
1.1 This test method covers a procedure for determining the non-fibrous content (shot) of man-made rock and slag mineral fiber insulation. The procedure covers a dry sieve analysis method to distinguish between fiberized and non-fiberized (shot) portions of a specimen of man-made rock and slag mineral fiber insulation specimen.
1.2 This test method does not apply to rock or slag materials containing any components other than rock and slag mineral fiber and organic thermal setting binders. Products containing other types of fibers, inorganic binders, or refractory clays are excluded.
1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:C1335–04 (Reapproved 2009)
Standard Test Method for
Measuring Non-Fibrous Content of Man-Made Rock and
Slag Mineral Fiber Insulation
This standard is issued under the fixed designation C1335; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope E691 Practice for Conducting an Interlaboratory Study to
Determine the Precision of a Test Method
1.1 This test method covers a procedure for determining the
non-fibrous content (shot) of man-made rock and slag mineral
3. Terminology
fiber insulation. The procedure covers a dry sieve analysis
3.1 Definitions—Terminology C168 shall be considered as
method to distinguish between fiberized and non-fiberized
applying to the terms used in this test method.
(shot) portions of a specimen of man-made rock and slag
3.2 Definition of Term Specific to This Standard:
mineral fiber insulation specimen.
3.2.1 shot—materialthatcannotbebrushedormechanically
1.2 This test method does not apply to rock or slag materials
shaken through a No. 100 (150 µm) sieve.
containing any components other than rock and slag mineral
fiber and organic thermal setting binders. Products containing
4. Significance and Use
other types of fibers, inorganic binders, or refractory clays are
4.1 Inorganic fibrous thermal insulation can contain varying
excluded.
amountsofnon-fibrousmaterial.Non-fibrousmaterialdoesnot
1.3 The values stated in inch-pound units are to be regarded
contributetotheinsulatingvalueoftheinsulationandtherefore
as standard. The values given in parentheses are mathematical
a procedure for determining that amount is desirable. Several
conversions to SI units that are provided for information only
specifications refer to shot content and percent (%) retained on
and are not considered standard.
various screen sizes determined by this test method.
1.4 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the
5. Apparatus
responsibility of the user of this standard to establish appro-
5.1 Furnace, capable of maintaining 1100 6 10°F (593 6
priate safety and health practices and determine the applica-
5.6°C) for rock and slag wool.
bility of regulatory limitations prior to use.
5.2 U.S.A. Standard Sieve Shaker Machine.
5.3 Balance Scale, capable of weighing to an accuracy of
2. Referenced Documents
0.00035 oz (0.01 g).
2.1 ASTM Standards:
5.4 Sieves—Three8in.(203mm)diameterU.S.A.Standard
C168 Terminology Relating to Thermal Insulation
Sieves. Nos. 20 (850 µm), 50 (300 µm), and 100 (150 µm)
C390 Practice for Sampling and Acceptance of Thermal
nested in order with bottom receiver pan. All sieve design and
Insulation Lots
construction shall be in accordance with Specification E11.
E11 SpecificationforWovenWireTestSieveClothandTest
5.5 Brush—Approximately 1 in. (25 mm) diameter plastic
Sieves
bristle brush, and approximately 1 in. (25 mm) wide soft paint
E178 Practice for Dealing With Outlying Observations
brush.
5.6 Crucible Weighing Dish, tared.
ThistestmethodisunderthejurisdictionofASTMCommitteeC16onThermal
5.7 Stoppers, rubber, No. 12 or 13.
Insulation and is the direct responsibility of Subcommittee C16.32 on Mechanical
5.8 Cork Borer, approximately 0.8 in. (20 mm) diameter.
Properties.
Current edition approved Sept. 1, 2009. Published September 2009. Originally
6. Sampling and Preparation of Test Specimen
approved in 1996. Last previous edition approved in 2004 as C1335 – 04. DOI:
10.1520/C1335-04R09.
6.1 For the purposes of standard tests, sampling shall be in
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
accordance with Practice C390 and Practice E178 with a
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
minimum of three specimens per lot to be tested.
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
C1335–04 (2009)
6.1.1 Specimen—This test method requires approximately a
WP = mass of material on all sieves, and
0.35 oz (10 g) specimen.
WT = mass of specimen after firing.
6.2 Specimen Preparation:
8.2 Adding the total percentages of all WC (s) (minimum of
6.2.1 Obtainarepresentativespecimenutilizinga0.8in.(20
three specimens/tests) and dividing by the number of WC (s)
mm) cork borer for blanket or board and random specimens for
equals the average total percent of shot (shot content).
loosefill.Firethespecimeninatareddishat1100 610°F(593
6 5.6°C) for 15 min. Remove tared dish with specimen and
9. Report
allow to cool for approximately 20 min.
9.1 Report the following information:
6.2.2 Weigh the crucible weighing dish and fiber on balance
9.1.1 A description of the material being tested, including
scale to the nearest 0.00035 oz (0.01 g), subtract tare dish
specimen source (company name and manufacturing location),
weight, noting the mass of specimen after firing as WT.
color, production code, or any other information that will help
identify specimen.
7. Procedures
9.2
...


This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation:C1335–96 (Reapproved 2002) Designation: C 1335 – 04 (Reapproved 2009)
Standard Test Method for
Measuring Non-Fibrous Content of Man-Made Rock and
Slag Mineral Fiber Insulation
This standard is issued under the fixed designation C 1335; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This test method covers a procedure for determining the non-fibrous content (shot) of man-made rock and slag mineral fiber
insulation. The procedure covers a dry sieve analysis method to distinguish between fiberized and non-fiberized (shot) portions of
a specimen of man-made rock and slag mineral fiber insulation specimen.
1.2 This test method does not apply to rock or slag materials containing any components other than rock and slag mineral fiber
and organic thermal setting binders. Products containing other types of fibers, inorganic binders, or refractory clays are excluded.
1.3The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information
only.
1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical
conversions to SI units that are provided for information only and are not considered standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2.1 ASTM Standards:
C 168 Terminology Relating to Thermal Insulation
C 390 CriteriaPractice for Sampling and Acceptance of Preformed Thermal Insulation Lots
E11 Specification for Wire-Cloth Sieves for Testing Purposes Specification for Woven Wire Test Sieve Cloth and Test Sieves
E 178 Practice for Dealing with Outlying Observations Practice for Dealing With Outlying Observations
E 691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
3. Terminology
3.1 Definitions—Terminology C 168 shall be considered as applying to the terms used in this test method.
3.2 Definition of Term Specific to This Standard:
3.2.1 shot—material that cannot be brushed or mechanically shaken through a No. 100 (150 µm) sieve.
4. Significance and Use
4.1 Inorganic fibrous thermal insulation can contain varying amounts of non-fibrous material. Non-fibrous material does not
contribute to the insulating value of the insulation and therefore a procedure for determining that amount is desirable. Several
specifications refer to shot content and percent (%) retained on various screen sizes determined by this test method.
5. Apparatus
5.1 Furnace, capable of maintaining 1100 6 10°F (593 6 5.6°C) for rock and slag wool.
5.2 U.S.A. Standard Sieve Shaker Machine.
5.3 Balance Scale, capable of weighing to an accuracy of 0.00035 oz (0.01 g).
5.4 Sieves—Three 8 in. (203 mm) diameter U.S.A. Standard Sieves. Nos. 20 (850 µm), 50 (300 µm), and 100 (150 µm) nested
in order with bottom receiver pan. All sieve design and construction shall be in accordance with Specification E 11.
This test method is under the jurisdiction of ASTM Committee C16 on Thermal Insulation and is the direct responsibility of Subcommittee C16.32 on Mechanical
Properties.
Current edition approved May 10, 1996. Published July 1996. Originally published as C1335 – 96. Last previous edition C1335 – 96.
Current edition approved Sept. 1, 2009. Published September 2009. Originally approved in 1996. Last previous edition approved in 2004 as C 1335 – 04.
For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
, Vol 04.06.volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
C 1335 – 04 (2009)
5.5 Brush—Approximately 1 in. (25 mm) diameter plastic bristle brush, and approximately 1 in. (25 mm) wide soft paint brush.
5.6 Crucible Weighing Dish, tared.
5.7 Stoppers, rubber, No. 12 or 13.
5.8 Cork Borer, approximately 0.8 in. (20 mm) diameter.
6. Sampling and Preparation of Test Specimen
6.1 For the purposes of standard tests, sampling shall be in accordance with CriteriaPractice C 390 and Practice E 178 with a
minimum of three specimens per lot to be tested.
6.1.1 Specimen—This test method requires approximately a 0.35 oz (10 g) specimen.
6.2 Specimen Preparation:
6.2.1 Obtain a representative specimen utilizing a 0.8 in. (20 mm) cork borer for blanket or board and random specimens for
loose fill. Fire the specimen in a tared dish at 1100 6 10°F (593 6 5.6°C) for 15 min. Remove tared dish with specimen and allow
to cool for approximately 20 min.
6.2.2 Weigh the crucible weighing dish and fiber on balance scale to the nearest 0.00035 oz (0.01 g), subtract tare dish weight,
noting the mass of specimen after firing as WT.
7. Procedures
7.1 Shot–Fiber Separation Procedure A (Includes Shaker Machine):
7.1.1 Assemble a nest of sieves (Nos. 20, 50, and 100) starting with a cover and the coarsest sieve on the top and a pan on the
bottom.
7.1.2 Place the specimen on the top sieve with receiver(s) in place.
7.1.3 W
...

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