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ASTM C1304-23

(Test Method)

Standard Test Method for Assessing the Odor Emission of Thermal Insulation Materials

Standard Test Method for Assessing the Odor Emission of Thermal Insulation Materials

SIGNIFICANCE AND USE
4.1 Thermal insulating materials that produce objectionable odors could cause discomfort to persons occupying a structure insulated with such materials. Therefore, an examination to determine the odor potential of a particular insulation is desirable.
SCOPE
1.1 This test method covers a laboratory procedure for subjective determination of the existence, nature, and degree of odors present in all types of thermal insulation materials. This test method is not intended to evaluate the air quality aspects that any such odors may present.  
1.2 The standard test condition for material evaluated under this test method is 149 ± 1.8°F (65 ± 1°C). Standard specifications referencing this test method may require other test conditions.  
1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
31-May-2023
ICS
13.040.99 - Other standards related to air quality
Technical Committee
C16 - Thermal Insulation
Drafting Committee
C16.31 - Chemical and Physical Properties
Current Stage
Ref Project

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Standards Content (Sample)

This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: C1304 − 23
Standard Test Method for
Assessing the Odor Emission of Thermal Insulation
1
Materials
This standard is issued under the fixed designation C1304; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 4. Significance and Use
1.1 This test method covers a laboratory procedure for
4.1 Thermal insulating materials that produce objectionable
subjective determination of the existence, nature, and degree of odors could cause discomfort to persons occupying a structure
odors present in all types of thermal insulation materials. This
insulated with such materials. Therefore, an examination to
test method is not intended to evaluate the air quality aspects determine the odor potential of a particular insulation is
that any such odors may present. desirable.
1.2 The standard test condition for material evaluated under
5. Apparatus
this test method is 149 6 1.8°F (65 6 1°C). Standard
specifications referencing this test method may require other
5.1 Stainless Steel Containers or Glass Jars, with all-
test conditions.
metallic lids with air-tight seals are required. Containers shall
not produce discernible odors of their own. The volume of the
1.3 The values stated in inch-pound units are to be regarded
container shall be 2.5 to 3 times the volume of the test
as standard. The values given in parentheses are mathematical
specimen. Transparent containers will be wrapped with alumi-
conversions to SI units that are provided for information only
num foil to eliminate visual bias.
and are not considered standard.
NOTE 1—See 6.2 for the minimum mass requirement for the test
1.4 This standard does not purport to address all of the
specimen, which influences test container volume.
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appro-
5.2 Oven, capable of maintaining a temperature of 149 6
priate safety, health, and environmental practices and deter-
1.8°F (65 6 1°C).
mine the applicability of regulatory limitations prior to use.
5.3 Odor Assessment Panel, consisting of five persons who
1.5 This international standard was developed in accor-
have demonstrated the ability to detect odors both accurately
dance with internationally recognized principles on standard-
and consistently. A guideline for selection of panelists is given
ization established in the Decision on Principles for the
3
in ASTM STP 758.
Development of International Standards, Guides and Recom-
5.4 Odor- and Draft-Free Area, where the required oven is
mendations issued by the World Trade Organization Technical
immediately accessible.
Barriers to Trade (TBT) Committee.
2. Referenced Documents
6. Sample Preparation
2
2.1 ASTM Standards:
6.1 Number of Tests—Unless otherwise dictated by a speci-
C168 Terminology Relating to Thermal Insulation
fication standard, one specimen of the material is selected at
random for testing. The sample shall be protected from
3. Terminology
contamination prior to testing. One empty container shall be
3.1 For definitions of terms related to this standard, see
used as a control for each sample tested.
Terminology C168.
6.2 Specimen Size—Test specimens shall have a minimum
1
mass of 2 oz (57 g). Where applicable, the specimens shall be
This test method is under the jurisdiction of ASTM Committee C16 on Thermal
Insulation and is the direct responsibility of Subcommittee C16.31 on Chemical and
cut with a clean knife and tested at the full product thickness.
Physical Properties.
If the product is faced, the facing shall remain as an integral
Current edition approved June 1, 2023. Published June 2023. Originally
part of the test specimen.
approved in 1995. Last previous edition approved in 2018 as C1304 – 18. DOI:
10.1520/C1304-23.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
3
Standards volume information, refer to the standard’s Document Summary page on “Guidelines for the Selection and Training of Sensory Panel Members,” ASTM
the ASTM website. STP 758, ASTM, 1981.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
C1304 − 23
7. Procedure their evaluation at the end of the second 3 min, discard and
begin with a new specimen.
7.1 The test containers shall be washed
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: C1304 − 18 C1304 − 23
Standard Test Method for
Assessing the Odor Emission of Thermal Insulation
1
Materials
This standard is issued under the fixed designation C1304; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This test method covers a laboratory procedure for subjective determination of the existence, nature, and degree of odors
present in all types of thermal insulation materials. This test method is not intended to evaluate the air quality aspects that any such
odors may present.
1.2 The standard test condition for material evaluated under this test method is 149 6 1.8°F (65 6 1°C). Standard specifications
referencing this test method may require other test conditions.
1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical
conversions to SI units that are provided for information only and are not considered standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of
regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
C168 Terminology Relating to Thermal Insulation
3. Terminology
3.1 For definitions of terms related to this standard, see Terminology C168.
4. Significance and Use
4.1 Thermal insulating materials that produce objectionable odors could cause discomfort to persons occupying a structure
insulated with such materials. Therefore, an examination to determine the odor potential of a particular insulation is desirable.
1
This test method is under the jurisdiction of ASTM Committee C16 on Thermal Insulation and is the direct responsibility of Subcommittee C16.31 on Chemical and
Physical Properties.
Current edition approved Sept. 1, 2018June 1, 2023. Published September 2018June 2023. Originally approved in 1995. Last previous edition approved in 20132018 as
C1304 – 08 (2013).C1304 – 18. DOI: 10.1520/C1304-18.10.1520/C1304-23.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
C1304 − 23
5. Apparatus
5.1 Stainless Steel Containers or Glass Jars, with all-metallic lids with air-tight seals are required. Containers shall not produce
discernible odors of their own. The volume of the container shall be 2.5 to 3 times the volume of the test specimen. Transparent
containers will be wrapped with aluminum foil to eliminate visual bias.
NOTE 1—See 5.26.2 for the minimum mass requirement for the test specimen, which influences test container volume.
5.2 Oven, capable of maintaining a temperature of 149 6 1.8°F (65 6 1°C).
5.3 Odor Assessment Panel, consisting of five persons who have demonstrated the ability to detect odors both accurately and
3
consistently. A guideline for selection of panelists is given in ASTM STP 758.
5.4 Odor- and Draft-Free Area, where the required oven is immediately accessible.
6. Sample Preparation
6.1 Number of Tests—Unless otherwise dictated by a specification standard, one specimen of the material is selected at random
for testing. The sample shall be protected from contamination prior to testing. One empty container shall be used as a control for
each sample tested.
6.2 Specimen Size—Test specimens shall have a minimum mass of 2 oz (57 g). Where applicable, the specimens shall be cut with
a clean knife and tested at the full product thickness. If the product is faced, the facing shall remain as an integral part of the test
specimen.
7. Procedure
7.1 The test containers shall be washe
...

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Note 1: Each combination of wipes (two wipes, three wipes, and four wipes) constitutes a different matrix and must be separately validated.
SCOPE
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1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
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1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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5.1 This practice is intended for the digestion of lead in dust wipe samples collected during various lead hazard activities performed in and around buildings and related structures.  
5.2 This practice is also intended for the digestion of lead in dust wipe samples collected during and after building renovations.  
5.3 This practice is applicable to the digestion of dust wipe samples that have or have not been collected in accordance with Practice E1728/E1728M using wipes that may or may not conform to Specification E1792.  
5.4 This practice is applicable to the digestion of dust wipe samples that were placed in either hard-walled, rigid containers such as 50-mL centrifuge tubes or flexible plastic bags.
Note 2: Due to the difficulty in performing quantitative transfers of some samples from plastic bags, hard-walled rigid containers such as 50-mL plastic centrifuge tubes are recommended in Practice E1728/E1728M for sample collection.  
5.5 Digestates prepared according to this practice are intended to be analyzed for lead concentration using spectrometric techniques such as Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES) and Flame Atomic Absorption Spectrometry (FAAS) (see Test Methods E1613, E3193, and E3203), or using electrochemical techniques such as anodic stripping voltammetry (see Practice E2051).  
5.6 This practice is not capable of determining lead bound within matrices, such as silica, that are not soluble in nitric acid.  
5.7 This practice is capable of determining lead bound within paint.
SCOPE
1.1 This practice covers the acid digestion of surface dust samples (collected using wipe sampling practices) and associated quality control (QC) samples for the determination of lead.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.2.1 Exception—Informational inch-pound units are provided in Note 3.  
1.3 This practice contains notes which are explanatory and not part of mandatory requirements of the standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D6330-20(Practice)
Standard Practice for Determination of Volatile Organic Compounds (Excluding Formaldehyde) Emissions from Wood-Based Panels Using Small Environmental Chambers Under Defined Test Conditions

SIGNIFICANCE AND USE
4.1 The effects of VOC sources on the indoor air quality in buildings have not been well established. One basic requirement that has emerged from indoor air quality studies is the need for well-characterized test data on the emission factors of VOCs from building materials. Standard test method and procedure are a requirement for the comparison of emission factor data from different products.  
4.2 This practice describes a procedure for using a small environmental test chamber to determine the emission factors of VOCs from wood-based panels over a specified period of time. A pre-screening analysis procedure is also provided to identify the VOCs emitted from the products, to determine the appropriate GC-MS or GC-FID analytical procedure, and to estimate required sampling volume for the subsequent environmental chamber testing.  
4.3 Test results obtained using this practice provide a basis for comparing the VOC emission characteristics of different wood-based panel products. The emission data can be used to inform manufacturers of the VOC emissions from their products. The data can also be used to identify building materials with reduced VOC emissions over the time interval of the test.  
4.4 While emission factors determined by using this practice can be used to compare different products, the concentrations measured in the chamber shall not be considered as the resultant concentrations in an actual indoor environment.
SCOPE
1.1 The practice measures the volatile organic compounds (VOC), excluding formaldehyde, emitted from manufactured wood-based panels. A pre-screening analysis is used to identify the VOCs emitted from the panel. Emission factors (that is, emission rates per unit surface area) for the VOCs of interest are then determined by measuring the concentrations in a small environmental test chamber containing a specimen. The test chamber is ventilated at a constant air change rate under the standard environmental conditions. For formaldehyde determination, see Test Method D6007.  
1.2 This practice describes a test method that is specific to the measurement of VOC emissions from newly manufactured individual wood-based panels, such as particleboard, plywood, and oriented strand board (OSB), for the purpose of comparing the emission characteristics of different products under the standard test condition. For general guidance on conducting small environmental chamber tests, see Guide D5116.  
1.3 VOC concentrations in the environmental test chamber are determined by adsorption on an appropriate single adsorbent tube or multi-adsorbent tube, followed by thermal desorption and combined gas chromatograph/mass spectrometry (GC-MS) or gas chromatograph/flame ionization detection (GC-FID). The air sampling procedure and the analytical method recommended in this practice are generally valid for the identification and quantification of VOCs with saturation vapor pressure between 500 and 0.01 kPa at 25°C, depending on the selection of adsorbent(s).
Note 1: VOCs being captured by an adsorbent tube depend on the adsorbent(s) and sampling procedure selected (see Practice D6196). The user should have a thorough understanding of the limitations of each adsorbent used. Although canisters can be used to sample VOCs, this standard is limited to sampling VOCs from the chamber air using adsorbent tubes.  
1.4 The emission factors determined using the above procedure describe the emission characteristics of the specimen under the standard test condition. These data can be used directly to compare the emission characteristics of different products and to estimate the emission rates up to one month after the production. They shall not be used to predict the emission rates over longer periods of time (that is, more than one month) or under different environmental conditions.  
1.5 Emission data from chamber tests can be used for predicting the impact of wood-based panels on the VOC concentrations...

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