Standard Test Methods for Compatibility of Screening Analysis of Waste

SCOPE
1.1 These test methods cover assessment of the compatibility/reactivity of waste. The individual test methods are as follows:  SectionsTest Method A-Commingled Waste Compatibility8-12 Test Method B-Polymerization Potential (Reaction with  Triethylamine)13-18Test Method C-Water Compatibility19-25
1.2 These test methods are applicable to waste liquids, sludges, semi-solids, and solids.
1.3 These test methods are designed and intended as a preliminary or supplementary test to complement the more sophisticated quantitative analytical techniques that should be used to determine waste composition and compatibilities. This standard offers the user the option and the ability to screen wastes for potentially hazardous reactions when the more sophisticated techniques are not available and the total waste composition is unknown and to screen compatibility when the composition is known.
Note 1--Warning: Delayed or slow reactions of wastes may go unnoticed.
1.4 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Sections 10, 15, and 23 and Notes 1 and 2.

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31-Dec-2000
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ASTM D5058-90(2001) - Standard Test Methods for Compatibility of Screening Analysis of Waste
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
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Designation:D5058–90 (Reapproved 2001)
Standard Test Methods for
1
Compatibility of Screening Analysis of Waste
This standard is issued under the fixed designation D5058; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope E1 Specification for ASTM Thermometers
E200 Practice for Preparation, Standardization, and Stor-
1.1 These test methods cover assessment of the
age of Standard Solutions for Chemical Analysis
compatibility/reactivity of waste. The individual test methods
are as follows:
3. Terminology
Sections
3.1 Definition of Term Specific to This Standard:
Test Method A—Commingled Waste Compatibility 8-12
Test Method B—Polymerization Potential (Reaction with
3.1.1 screening—a preliminary qualitative or semi-
Triethylamine) 13-18
quantitative test, developed from classical qualitative and
Test Method C—Water Compatibility 19-25
quantitative techniques, that is designed to efficiently give the
1.2 These test methods are applicable to waste liquids,
user specific information about a waste that will aid in
sludges, semi-solids, and solids.
determining waste identification, process compatibility, and
1.3 These test methods are designed and intended as a
safety in handling.
preliminary or supplementary test to complement the more
4. Summary of Test Methods
sophisticated quantitative analytical techniques that should be
used to determine waste composition and compatibilities. This
4.1 Test Method A— Representative samples of waste are
standard offers the user the option and the ability to screen
added to each other. The generation of heat or violent reaction
wastes for potentially hazardous reactions when the more
is noted. In addition, the production of mists, fumes, dusts,
sophisticated techniques are not available and the total waste
gases,layering,polymerization,precipitation,emulsificationor
composition is unknown and to screen compatibility when the
increase in viscosity and other chemical or physical changes
composition is known.
are noted.
4.2 Test Method B— Reactivity of wastes is determined by
NOTE 1—Warning:Delayed or slow reactions of wastes may go
adding an aliquot of a sample to an equal volume of reagent
unnoticed.
and observing any characteristic reaction, such as temperature
1.4 The values stated in SI units are to be regarded as the
increase, gas evolution, gelling, or polymerization.
standard. The values given in parentheses are for information
4.3 Test Method C— Water and the waste are mixed in an
only.
approximate 10+1 ratio to test for compatibility.Athermom-
1.5 This standard does not purport to address all of the
eter is used to measure heat generation when applicable.
safety concerns, if any, associated with its use. It is the
Qualitative solubility and relative apparent density are ob-
responsibility of the user of this standard to establish appro-
served concurrently.
priate safety and health practices and determine the applica-
bility of regulatory limitations prior to use. For specific hazard
5. Purity of Reagents
statements, see Sections 10, 15, and 23 and Notes 1 and 2.
5.1 Purity of Reagents—Reagent grade chemicals shall be
used in all tests. Unless otherwise indicated, it is intended that
2. Referenced Documents
all reagents conform to the specifications of the Committee on
2
2.1 ASTM Standards:
Analytical Reagents of theAmerican Chemical Society, where
D1193 Specification for Reagent Water
3
such specifications are available. Other grades may be used
provided it is first ascertained that the reagent is of sufficiently
1
These test methods are under the jurisdiction of ASTM Committee D34 on
WasteManagementandarethedirectresponsibilityofSubcommitteeD34.01.05on
Screening Methods.
3
Current edition approved May 25, 1990. Published July 1990. “ReagentChemicals,AmericanChemicalSocietySpecifications,”Am.Chemi-
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or cal Soc., Washington, DC. For suggestions on the testing of reagents not listed by
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM theAmericanChemicalSociety,see“ReagentChemicalsandStandards,”byJoseph
Standards volume information, refer to the standard’s Document Summary page on Rosin, D. Van Nostrand Co., Inc., New York, NY, and the “United States
the ASTM website. Pharmacopeia.”
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
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D5058–90 (2001)
high purity to permit its use without lessening the accuracy of 11.2 Determine the total quantity B of the was
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