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ASTM D5-06e1

(Test Method)

Standard Test Method for Penetration of Bituminous Materials

Standard Test Method for Penetration of Bituminous Materials

SIGNIFICANCE AND USE
The penetration test is used as a measure of consistency. Higher values of penetration indicate softer consistency.
SCOPE
1.1 This test method covers determination of the penetration of semi-solid and solid bituminous materials.
1.2 The needles, containers and other conditions described in this test method provide for the determinations of penetrations up to 500.For guidance in preparing and testing emulsion residue specimens for this test method, please refer to Section 35 of Test Method D 244.
1.3 The values stated in SI units are to be considered standard.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
31-May-2006
ICS
75.140 - Waxes, bituminous materials and other petroleum products
Technical Committee
D04 - Road and Paving Materials
Drafting Committee
D04.44 - Rheological Tests
Current Stage
Ref Project

Relations

Replaces
ASTM D5-06 - Standard Test Method for Penetration of Bituminous Materials
Effective Date
01-Jun-2006
Replaced By
ASTM D5/D5M-13 - Standard Test Method for Penetration of Bituminous Materials
Effective Date
01-Jan-2013
Referred By
ASTM C782-13(2023) - Standard Test Method for Softness of Preformed Tape Sealants
Effective Date
01-Jun-2006
Referred By
ASTM D244-09(2017) - Standard Test Methods and Practices for Emulsified Asphalts
Effective Date
01-Jun-2006
Referred By
ASTM D5801-17 - Standard Test Method for Toughness and Tenacity of Asphalt Materials
Effective Date
01-Jun-2006
Referred By
ASTM D3666-16 - Standard Specification for Minimum Requirements for Agencies Testing and Inspecting Road and Paving Materials
Effective Date
01-Jun-2006
Referred By
ASTM D1321-16a - Standard Test Method for Needle Penetration of Petroleum Waxes
Effective Date
01-Jun-2006

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ASTM D5-06e1 - Standard Test Method for Penetration of Bituminous MaterialsASTM D5-06e1 - Standard Test Method for Penetration of Bituminous Materials
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ASTM D5-06e1 - Standard Test Method for Penetration of Bituminous Materials
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
´1
Designation: D5 − 06
StandardTest Method for
1
Penetration of Bituminous Materials
This standard is issued under the fixed designation D5; the number immediately following the designation indicates the year of original
adoptionor,inthecaseofrevision,theyearoflastrevision.Anumberinparenthesesindicatestheyearoflastreapproval.Asuperscript
epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1
´ NOTE—Editorial changes were made to Section 11 clarifing the use of the precision statement in July 2006.
1. Scope 2.2 ANSI Standard:
3
B46.1Surface Texture
1.1 Thistestmethodcoversdeterminationofthepenetration
2.3 ISO Standard:
of semi-solid and solid bituminous materials.
ISO Standard 468Surface Roughness—Parameters, Their
1.2 The needles, containers and other conditions described
3
Values and General Rules for Specifying Requirements
in this test method provide for the determinations of penetra-
tions up to 500.
3. Terminology
NOTE 1—For guidance in preparing and testing emulsion residue
3.1 Definitions:
specimens for this test method, please refer to Section 35 of Test Method
3.1.1 penetration, n—consistency of a bituminous material
D244.
expressed as the distance in tenths of a millimetre that a
1.3 The values stated in SI units are to be considered
standard needle vertically penetrates a sample of the material
standard.
under known conditions of loading, time, and temperature.
1.4 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the 4. Summary of Test Method
responsibility of the user of this standard to establish appro-
4.1 The sample is melted (if starting at ambient tempera-
priate safety and health practices and determine the applica-
ture) and cooled under controlled conditions. The penetration
bility of regulatory limitations prior to use.
ismeasuredwithapenetrometerbymeansofwhichastandard
needle is applied to the sample under specific conditions.
2. Referenced Documents
2
5. Significance and Use
2.1 ASTM Standards:
D36TestMethodforSofteningPointofBitumen(Ring-and-
5.1 The penetration test is used as a measure of consis-
Ball Apparatus)
tency. Higher values of penetration indicate softer consistency.
D244Test Methods and Practices for Emulsified Asphalts
E1Specification for ASTM Liquid-in-Glass Thermometers
6. Apparatus
E77Test Method for Inspection and Verification of Ther-
6.1 Penetration Apparatus—Any apparatus that permits the
mometers
needle holder (spindle) to move vertically without measurable
E1137/E1137MSpecification for Industrial Platinum Resis-
friction and is capable of indicating the depth of penetration to
tance Thermometers
the nearest 0.1 mm, will be acceptable. The weight of the
E2251Specification for Liquid-in-Glass ASTM Thermom-
spindle shall be 47.5 6 0.05 g. The total weight of the needle
eters with Low-Hazard Precision Liquids
and spindle assembly shall be 50.0 6 0.05 g.Weights of 50 6
0.05 g and 100 6 0.05 g shall also be provided for total loads
of100gand200g,asrequiredforsomeconditionsofthetest.
1
This test method is under the jurisdiction of ASTM Committee D04 on Road
The surface on which the sample container rests shall be flat
and Paving Materials and is the direct responsibility of Subcommittee D04.44 on
andtheaxisoftheplungershallbeatapproximately90°tothis
Rheological Tests.
surface. The apparatus shall have a leveling indicator. The
Current edition approved June 1, 2006. Published June 2006. Originally
approved in 1959. Last previous edition approved in 2005 as D5–05a. DOI:
spindle shall be easily detached for checking its weight.
10.1520/D0005-06E01.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
3
Standards volume information, refer to the standard’s Document Summary page on Available from American National Standards Institute, 25 W. 43rd St., 4th
the ASTM website. Floor, New York, NY 10036.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
´1
D5−06
6.1.1 The leveling indicator shall be verified at least annu-
For penetrations below 40:
Diameter, mm 33–50
ally with a hand-held level.
Internal depth, mm 8-16
For penetrations below 200:
6.2 Penetration Needle:
Diameter, mm 55
6.2.1 The needle (see Fig. 1) shall be made from fully
Internal depth, mm 35
hardened and tempered stainless steel, Grade 440-C or equal, For penetrations between 200 and 350:
Diameter, mm 55–75
HRC 54 to 60. The standard needle shall be approximately 50
Internal depth, mm 45–70
mm (2 in.) in length, the long needle approximately 60 mm
For penetrations 350 to 500
...

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5.1 This method indicates approximate change in properties of asphalt during conventional hot-mixing at about 150 °C [302 °F] as indicated by viscosity, penetration, or ductility measurements. It yields a residue which approximates the asphalt condition as incorporated in the pavement. If the mixing temperature differs appreciably from the 150 °C [302 °F] level, more or less effect on properties will occur.
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Standard Practice for Moisture Conditioning Compacted Asphalt Mixture Specimens by Using Hydrostatic Pore Pressure

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4.1 This practice provides an accelerated conditioning method under cyclic loading. This system is capable of operating at higher than normal temperatures and creating pore pressure within a compacted asphalt mixture to achieve an acceleration of the effects that a mixture would experience over time from traffic at normal temperatures and conditions. The accelerated conditioning in this practice is intended to simulate the stresses induced in a wet pavement by a passing vehicle tire. The pulse shape produced by this system approximates a Lorentzian function with a half peak width of approximately 1 s at 276 kPa [40 psi].  
4.2 The factors that influence the potential for moisture damage to occur include aggregate mineralogy, mixture air voids, water, cyclic applied stress, and elevated temperature. This practice provides a method and apparatus that is capable of producing three of these factors: water, stress, and high temperature. Aggregate mineralogy and air voids are mixture properties.  
4.3 Specimens conditioned by this system can be tested using a variety of different tests, including Test Method D6931, Test Method D6927, bulk specific gravity difference obtained by Test Method D6926 or D6752/D6752M for before and after conditioning, dynamic modulus, flow number, AASHTO T 378, and visual inspection for stripped aggregates.
Note 1: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptance guideline provides a means of evaluating ...
SCOPE
1.1 This practice includes procedures for preparing compacted asphalt mixture specimens, exposing the specimens to hydrostatic pore pressure inside an enclosed chamber, and guidance on testing the specimens for the effect of water on the tensile strength or change in other properties of the asphalt mixture, such as density, modulus, etc.  
1.2 Specimens conditioned according to this practice can be tested using methods and test procedures referenced in this document, and those results may provide information as to the effect of the moisture conditioning of this practice on the moisture sensitivity of those mixtures.  
1.3 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D7173-20(Practice)
Standard Practice for Determining the Separation Tendency of Polymer from Polymer-Modified Asphalt

SIGNIFICANCE AND USE
4.1 Purchasers of polymer-modified asphalt need guidelines on proper storage and handling procedures to maintain the integrity of material they have purchased. This practice provides a significant tool for understanding the characteristics of these materials as well as comparing various sources of supply.
Note 1: The quality of the results produced by this standard are dependent on the competence of the personnel performing the procedure and the capability, calibration, and maintenance of the equipment used. Agencies that meet the criteria of Specification D3666 are generally considered capable of competent and objective testing, sampling, inspection, etc. Users of this standard are cautioned that compliance with Specification D3666 alone does not completely ensure reliable results. Reliable results depend on many factors; following the suggestions of Specification D3666 or some similar acceptable guideline provides a means of evaluating and controlling some of those factors.
SCOPE
1.1 This practice describes a laboratory procedure for determining the tendency of polymer to separate from polymer-modified asphalt under static heated storage conditions. The results of testing on material prepared according to this practice may be used as a guideline when formulating products or to establish field handling procedures. Large differences in test results between top and bottom specimens indicate that there is a degree of incompatibility between the polymer and the base asphalt.  
1.2 The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this standard.  
1.3 The text of this standard references notes and footnotes which provide explanatory material. These notes and footnotes (excluding those in tables and figures) shall not be considered as requirements of the standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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  • Standard
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