ASTM D7713-18
(Specification)Standard Specification for Aqueous Engine Coolant Grade Glycol (53 % by Volume Nominal)
Standard Specification for Aqueous Engine Coolant Grade Glycol (53 % by Volume Nominal)
ABSTRACT
This specification covers both commercial products, engine coolant grade ethylene glycol and propylene glycol, including virgin glycols and those derived from the recycling of vehicle engine coolants and industrial source glycols. Types EG-1 and PG-1, which will probably be virgin materials, cover glycols with sufficiently low limits on components to allow a blended coolant to meet most Original Equipment Manufacturer (OEM) specifications. Types EG-2 and PG-2, on the other hand, can be either redistilled or virgin. These cover glycol that will be suitable for many coolants.
SCOPE
1.1 This specification covers both commercial products, engine coolant grade ethylene glycol and propylene glycol, including virgin glycols and those derived from the recycling of vehicle engine coolants and industrial source glycols.
1.2 Types EG-1 and PG-1 cover glycols with sufficiently low limits on components to allow a blended coolant to meet most OEM (Original Equipment Manufacturer) specifications. These types will probably be virgin materials, although redistillation could produce a sufficiently pure product. Types EG-2 and PG-2 cover glycol that will be suitable for many coolants. These types can be either redistilled or virgin.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
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Standards Content (Sample)
This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D7713 − 18
Standard Specification for
Aqueous Engine Coolant Grade Glycol (53 % by Volume
1
Nominal)
This standard is issued under the fixed designation D7713; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D1123 Test Methods for Water in Engine Coolant Concen-
trate by the Karl Fischer Reagent Method
1.1 This specification covers both commercial products,
D1177 Test Method for Freezing Point of Aqueous Engine
engine coolant grade ethylene glycol and propylene glycol,
Coolants
including virgin glycols and those derived from the recycling
D1209 Test Method for Color of Clear Liquids (Platinum-
of vehicle engine coolants and industrial source glycols.
Cobalt Scale)
1.2 Types EG-1 and PG-1 cover glycols with sufficiently
D1287 Test Method for pH of Engine Coolants and Antirusts
low limits on components to allow a blended coolant to meet
D1613 Test Method for Acidity in Volatile Solvents and
most OEM (Original Equipment Manufacturer) specifications.
Chemical Intermediates Used in Paint, Varnish, Lacquer,
These types will probably be virgin materials, although redis-
and Related Products
tillation could produce a sufficiently pure product. Types EG-2
D3634 Test Method for Trace Chloride Ion in Engine Cool-
and PG-2 cover glycol that will be suitable for many coolants.
ants
These types can be either redistilled or virgin.
D4052 Test Method for Density, Relative Density, and API
Gravity of Liquids by Digital Density Meter
1.3 The values stated in SI units are to be regarded as
standard. No other units of measurement are included in this D4725 Terminology for Engine Coolants and Related Fluids
D5827 Test Method for Analysis of Engine Coolant for
standard.
Chloride and Other Anions by Ion Chromatography
1.4 This standard does not purport to address all of the
D5931 Test Method for Density and Relative Density of
safety concerns, if any, associated with its use. It is the
Engine Coolant Concentrates and Aqueous Engine Cool-
responsibility of the user of this standard to establish appro-
ants by Digital Density Meter
priate safety, health, and environmental practices and deter-
D6130 Test Method for Determination of Silicon and Other
mine the applicability of regulatory limitations prior to use.
Elements in Engine Coolant by Inductively Coupled
1.5 This international standard was developed in accor-
Plasma-Atomic Emission Spectroscopy
dance with internationally recognized principles on standard-
D6660 Test Method for Freezing Point of Aqueous Ethylene
ization established in the Decision on Principles for the
Glycol Base Engine Coolants by Automatic Phase Tran-
Development of International Standards, Guides and Recom-
sition Method
mendations issued by the World Trade Organization Technical
D7736 Test Method for Determination of Acids and Glycol
Barriers to Trade (TBT) Committee.
Esters in Glycols
E202 Test Methods for Analysis of Ethylene Glycols and
2. Referenced Documents
Propylene Glycols
2
2.1 ASTM Standards:
E300 Practice for Sampling Industrial Chemicals
D1122 Test Method for Relative Density of Engine Coolant
E394 Test Method for Iron in Trace Quantities Using the
Concentrates and Engine Coolants By The Hydrometer
1,10-Phenanthroline Method
E1177 Specification for Engine Coolant Grade Glycol
3. Requirements
1
This specification is under the jurisdiction of ASTM Committee D15 on Engine
Coolants and Related Fluids and is the direct responsibility of Subcommittee
v
3.1 Engine coolant grade 53 % ( ⁄v) (nominal) ethylene
D15.07 on Specifications.
glycol or propylene glycol shall conform to the chemical and
Current edition approved Nov. 1, 2018. Published November 2018. Originally
approved in 2011. Last previous edition approved in 2012 as D7713–12. DOI: physical property requirements in Table 1.
10.1520/D7713–18.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or 4. Sampling
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
4.1 Sample ethylene or propylene glycol in accordance with
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. the appropriate sections of Practice E300 for liquid samples.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
D7713 − 18
TABLE 1 Physical and Chemical Requirements
Requirement Value for 53 %
...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D7713 − 12 D7713 − 18
Standard Specification for
Aqueous Engine Coolant Grade Glycol (53% (53 % by
1
Volume Nominal)
This standard is issued under the fixed designation D7713; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This specification covers both commercial products, engine coolant grade ethylene glycol and propylene glycol, including
virgin glycols and those derived from the recycling of vehicle engine coolants and industrial source glycols.
1.2 Types EG-1 and PG-1 cover glycols with sufficiently low limits on components to allow a blended coolant to meet most
OEM (Original Equipment Manufacturer) specifications. These types will probably be virgin materials, although redistillation
could produce a sufficiently pure product. Types EG-2 and PG-2 cover glycol that will be suitable for many coolants. These types
can be either redistilled or virgin.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety safety, health, and healthenvironmental practices and determine the
applicability of regulatory limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
D1122 Test Method for Density or Relative Density of Engine Coolant Concentrates and Engine Coolants By The Hydrometer
D1123 Test Methods for Water in Engine Coolant Concentrate by the Karl Fischer Reagent Method
D1177 Test Method for Freezing Point of Aqueous Engine Coolants
D1209 Test Method for Color of Clear Liquids (Platinum-Cobalt Scale)
D1287 Test Method for pH of Engine Coolants and Antirusts
D1613 Test Method for Acidity in Volatile Solvents and Chemical Intermediates Used in Paint, Varnish, Lacquer, and Related
Products
D3634 Test Method for Trace Chloride Ion in Engine Coolants
D4052 Test Method for Density, Relative Density, and API Gravity of Liquids by Digital Density Meter
D4725 Terminology for Engine Coolants and Related Fluids
D5827 Test Method for Analysis of Engine Coolant for Chloride and Other Anions by Ion Chromatography
D5931 Test Method for Density and Relative Density of Engine Coolant Concentrates and Aqueous Engine Coolants by Digital
Density Meter
D6130 Test Method for Determination of Silicon and Other Elements in Engine Coolant by Inductively Coupled Plasma-Atomic
Emission Spectroscopy
D6660 Test Method for Freezing Point of Aqueous Ethylene Glycol Base Engine Coolants by Automatic Phase Transition
Method
D7638D7736 Test Method for Determination of Fatty Acids and Glycol Esters in GlycerinEthylene Glycol
E177 Practice for Use of the Terms Precision and Bias in ASTM Test Methods
1
This specification is under the jurisdiction of ASTM Committee D15 on Engine Coolants and Related Fluids and is the direct responsibility of Subcommittee D15.07
on Specifications.
Current edition approved May 1, 2012Nov. 1, 2018. Published June 2012November 2018. Originally approved in 2011. Last previous edition approved in 20112012 as
D7713 – 11.D7713–12. DOI: 10.1520/D7713–12.10.1520/D7713–18.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’sstandard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
D7713 − 18
E202 Test Methods for Analysis of Ethylene Glycols and Propylene Glycols
E300 Practice for Sampling Industrial Chemicals
E394 Test Method for Iron in Trace Quantities Using the 1,10-Phenanthroline Method
E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
E1177 Specification for Engi
...
NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D7713 − 18
Standard Specification for
Aqueous Engine Coolant Grade Glycol (53 % by Volume
1
Nominal)
This standard is issued under the fixed designation D7713; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D1123 Test Methods for Water in Engine Coolant Concen-
trate by the Karl Fischer Reagent Method
1.1 This specification covers both commercial products,
D1177 Test Method for Freezing Point of Aqueous Engine
engine coolant grade ethylene glycol and propylene glycol,
Coolants
including virgin glycols and those derived from the recycling
D1209 Test Method for Color of Clear Liquids (Platinum-
of vehicle engine coolants and industrial source glycols.
Cobalt Scale)
1.2 Types EG-1 and PG-1 cover glycols with sufficiently
D1287 Test Method for pH of Engine Coolants and Antirusts
low limits on components to allow a blended coolant to meet
D1613 Test Method for Acidity in Volatile Solvents and
most OEM (Original Equipment Manufacturer) specifications.
Chemical Intermediates Used in Paint, Varnish, Lacquer,
These types will probably be virgin materials, although redis-
and Related Products
tillation could produce a sufficiently pure product. Types EG-2
D3634 Test Method for Trace Chloride Ion in Engine Cool-
and PG-2 cover glycol that will be suitable for many coolants.
ants
These types can be either redistilled or virgin.
D4052 Test Method for Density, Relative Density, and API
1.3 The values stated in SI units are to be regarded as Gravity of Liquids by Digital Density Meter
D4725 Terminology for Engine Coolants and Related Fluids
standard. No other units of measurement are included in this
standard. D5827 Test Method for Analysis of Engine Coolant for
Chloride and Other Anions by Ion Chromatography
1.4 This standard does not purport to address all of the
D5931 Test Method for Density and Relative Density of
safety concerns, if any, associated with its use. It is the
Engine Coolant Concentrates and Aqueous Engine Cool-
responsibility of the user of this standard to establish appro-
ants by Digital Density Meter
priate safety, health, and environmental practices and deter-
D6130 Test Method for Determination of Silicon and Other
mine the applicability of regulatory limitations prior to use.
Elements in Engine Coolant by Inductively Coupled
1.5 This international standard was developed in accor-
Plasma-Atomic Emission Spectroscopy
dance with internationally recognized principles on standard-
D6660 Test Method for Freezing Point of Aqueous Ethylene
ization established in the Decision on Principles for the
Glycol Base Engine Coolants by Automatic Phase Tran-
Development of International Standards, Guides and Recom-
sition Method
mendations issued by the World Trade Organization Technical
D7736 Test Method for Determination of Acids and Glycol
Barriers to Trade (TBT) Committee.
Esters in Glycols
E202 Test Methods for Analysis of Ethylene Glycols and
2. Referenced Documents
Propylene Glycols
2
2.1 ASTM Standards:
E300 Practice for Sampling Industrial Chemicals
D1122 Test Method for Relative Density of Engine Coolant
E394 Test Method for Iron in Trace Quantities Using the
Concentrates and Engine Coolants By The Hydrometer
1,10-Phenanthroline Method
E1177 Specification for Engine Coolant Grade Glycol
1 3. Requirements
This specification is under the jurisdiction of ASTM Committee D15 on Engine
Coolants and Related Fluids and is the direct responsibility of Subcommittee
v
3.1 Engine coolant grade 53 % ( ⁄v) (nominal) ethylene
D15.07 on Specifications.
glycol or propylene glycol shall conform to the chemical and
Current edition approved Nov. 1, 2018. Published November 2018. Originally
physical property requirements in Table 1.
approved in 2011. Last previous edition approved in 2012 as D7713–12. DOI:
10.1520/D7713–18.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or 4. Sampling
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
4.1 Sample ethylene or propylene glycol in accordance with
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. the appropriate sections of Practice E300 for liquid samples.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
D7713 − 18
TABLE 1 Physical and Chemical Requirements
Requirement Value for 53 % Value for 53 % Value for 53 % Value for 53 % ASTM
Ethylene Glycol, Type Propylene Glycol, Type Ethylene Glycol, Type Propylene-Glycol, Test
EG-1 53 %
...
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