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ASTM D1796-97e1

(Test Method)

Standard Test Method for Water and Sediment in Fuel Oils by the Centrifuge Method (Laboratory Procedure)

Standard Test Method for Water and Sediment in Fuel Oils by the Centrifuge Method (Laboratory Procedure)

SCOPE
1.1 This test method covers the laboratory test for determination of water and sediment in fuel oils by using the centrifuge method in the range from 0 to 30 % volume. This chapter, along with API MPMS Chapter 10.3 (Test Method D 4007), supersedes the previous edition of Test Method D 1796 (API Standard D 2548, IP 75).
Note 1—With some types of fuel oils such as residual fuel oils or distillate fuel oils containing residual components, it is difficult to obtain water or sediment contents with this test method. When this situation is encountered, Test Method D 95 (API MPMS Chapter 10.5) or Test Method D 473 (API MPMS Chapter 10.1) may be used.
1.2 contains a procedure for saturating toluene with water.
1.3 The values stated in SI units are to be regarded as the standard. The values in parentheses are for information only.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For a specific precautionary statement see 6.1.

General Information

Status
Historical
Publication Date
09-Jan-1997
Technical Committee
D02 - Petroleum Products, Liquid Fuels, and Lubricants
Drafting Committee
D02.02 - Hydrocarbon Measurement for Custody Transfer (Joint ASTM-API)
Current Stage
Ref Project

Relations

Replaces
ASTM D1796-97 - Standard Test Method for Water and Sediment in Fuel Oils by the Centrifuge Method (Laboratory Procedure)
Effective Date
10-Jan-1997
Replaced By
ASTM D1796-97(2002) - Standard Test Method for Water and Sediment in Fuel Oils by the Centrifuge Method (Laboratory Procedure)
Effective Date
10-Dec-2002
Referred By
ASTM D6750-23 - Standard Test Methods for Evaluation of Engine Oils in a High-Speed, Single-Cylinder Diesel Engine—1K Procedure (0.4 % Fuel Sulfur) and 1N Procedure (0.04 % Fuel Sulfur)
Effective Date
10-Jan-1997
Referred By
ASTM D7666-12(2019) - Standard Specification for Triglyceride Burner Fuel
Effective Date
10-Jan-1997
Referred By
ASTM D975-23 - Standard Specification for Diesel Fuel
Effective Date
10-Jan-1997
Referred By
ASTM D6751-23a - Standard Specification for Biodiesel Fuel Blendstock (B100) for Middle Distillate Fuels
Effective Date
10-Jan-1997
Referred By
ASTM D2709-22 - Standard Test Method for Water and Sediment in Middle Distillate Fuels by Centrifuge
Effective Date
10-Jan-1997
Referred By
ASTM D2880-23 - Standard Specification for Gas Turbine Fuel Oils
Effective Date
10-Jan-1997
Referred By
ASTM F1084-08(2018) - Standard Guide for Sampling Oil/Water Mixtures for Oil Spill Recovery Equipment
Effective Date
10-Jan-1997
Referred By
ASTM D2711-22 - Standard Test Method for Demulsibility Characteristics of Lubricating Oils
Effective Date
10-Jan-1997
Referred By
ASTM D2158-21 - Standard Test Method for Residues in Liquefied Petroleum (LP) Gases
Effective Date
10-Jan-1997
Referred By
ASTM D6448-16(2022) - Standard Specification for Industrial Burner Fuels from Used Lubricating Oils
Effective Date
10-Jan-1997
Referred By
ASTM D6823-08(2021) - Standard Specification for Commercial Boiler Fuels With Used Lubricating Oils
Effective Date
10-Jan-1997
Referred By
ASTM F2084/F2084M-01(2018) - Standard Guide for Collecting Containment Boom Performance Data in Controlled Environments
Effective Date
10-Jan-1997
Referred By
ASTM D6666-20 - Standard Guide for Evaluation of Aqueous Polymer Quenchants
Effective Date
10-Jan-1997

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ASTM D1796-97e1 - Standard Test Method for Water and Sediment in Fuel Oils by the Centrifuge Method (Laboratory Procedure)ASTM D1796-97e1 - Standard Test Method for Water and Sediment in Fuel Oils by the Centrifuge Method (Laboratory Procedure)
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ASTM D1796-97e1 - Standard Test Method for Water and Sediment in Fuel Oils by the Centrifuge Method (Laboratory Procedure)
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Standards Content (Sample)

NOTICE: This standard has either been superceded and replaced by a new version or discontinued.
Contact ASTM International (www.astm.org) for the latest information.
An American National Standard
e1
Designation: D 1796 – 97
Designation: Manual of Petroleum Measurement Standards (MPMS), Chapter 10.6
Standard Test Method for
Water and Sediment in Fuel Oils by the Centrifuge Method
1
(Laboratory Procedure)
This standard is issued under the fixed designation D 1796; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1
e NOTE—Footnote 1 and the Referenced Documents were corrected editorially to comply with the ASTM-API joint standard
contract in October 2002. Warning notes were editorially moved into the standard text in October 2002.
3
1. Scope D 362 Specification for Industrial Grade Toluene
D 473 Test Method for Sediment in Crude Oils and Fuel
1.1 This test method covers the laboratory test for determi-
2
Oils by the Extraction Method (API MPMS Chapter 10.1)
nation of water and sediment in fuel oils by using the
D 4006 Test Method for Water in Crude Oil by Distillation
centrifuge method in the range from 0 to 30 % volume. This
4
(API MPMS Chapter 10.2)
chapter, along with API MPMS Chapter 10.3 (Test Method
D 4007 Test Method for Water and Sediment in Crude Oil
D 4007), supersedes the previous edition of Test Method
by the Centrifuge Method (Laboratory Procedure) (API
D 1796 (API Standard D 2548, IP 75).
4
MPMS Chapter 10.3)
NOTE 1—With some types of fuel oils such as residual fuel oils or
D 4057 Practice for Manual Sampling of Petroleum and
distillate fuel oils containing residual components, it is difficult to obtain
4
Petroleum Products (API MPMS Chapter 8.1)
water or sediment contents with this test method. When this situation is
D 4177 Practice for Automatic Sampling of Petroleum and
encountered, Test Method D 95 (API MPMS Chapter 10.5) or Test Method
4
Petroleum Products (API MPMS Chapter 8.2)
D 473 (API MPMS Chapter 10.1) may be used.
D 4377 Test Method for Water in Crude Oils by Potentio-
1.2 Annex A2 contains a procedure for saturating toluene
4
metric Karl Fischer Titration (API MPMS Chapter 10.7)
with water.
D 4928 Test Method for Water in Crude Oils by Coulom-
1.3 The values stated in SI units are to be regarded as the
4
etric Karl Fischer Titration (API MPMS Chapter 10.9)
standard. The values in parentheses are for information only.
D 5854 Practice for Mixing and Handling Liquid Samples
1.4 This standard does not purport to address all of the
of Petroleum and Petroleum Products (API MPMS Chapter
safety concerns, if any, associated with its use. It is the
5
8.3)
responsibility of the user of this standard to establish appro-
E 542 Practice for Calibration of Laboratory Volumetric
priate safety and health practices and determine the applica-
6
Apparatus
bility of regulatory limitations prior to use. For a specific
7
2.2 API Standards:
precautionary statement see 6.1.
MPMS Chapter 8.1 Manual Sampling of Petroleum and
Petroleum Products (ASTM Practice D 4057)
2. Referenced Documents
MPMS Chapter 8.2 Automatic Sampling of Petroleum and
2.1 ASTM Standards:
Petroleum Products (ASTM Practice D 4177)
D 95 Test Method for Water in Petroleum Products and
MPMS Chapter 8.3 Mixing and Handling Liquid Samples of
Bituminous Materials by Distillation (API MPMS Chapter
Petroleum and Petroleum Products (ASTM Practice
2
10.5)
D 5854)
MPMS Chapter 10.1 Test Method for Sediment in Crude
1
This test method is under the jurisdiction of ASTM Committee D02 on
Petroleum Products and Lubricants and the API Committee on Petroleum Measure-
3
ment, and is the direct responsibility of Subcommittee D02.02/COMQ, the joint Discontinued—See 1988 Annual Book of ASTM Standards, Vol 06.03.
4
ASTM-API committee on Static Petroleum Measurement. Annual Book of ASTM Standards, Vol 05.02.
5
Current edition approved Jan. 10, 1997. Published October 1997. Originally Annual Book of ASTM Standards, Vol 05.03.
e1 6
published as D 1796–60. Last previous edition D 1796–83 (1990). Annual Book of ASTM Standards, Vol 14.02.
2 7
Annual Book of ASTM Standards, Vol 05.01. Published as Manual of Petroleum Measurement Standards. Available from the
American Petroleum Institute, 1220 L St., N.W., Washington, DC 20005.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
NOTICE: This standard has either been superceded and replaced by a new version or discontinued.
Contact ASTM International (www.astm.org) for the latest information.
e1
D1796–97
Oils and Fuel Oils by the Extraction Method (ASTM Test
Method
...

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1.1 These test methods cover the physical properties associated with preformed expansion joint fillers. The test methods include:    
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7.5  
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Note 1: Specific test methods are applicable only to certain types of joint fillers, as stated herein.  
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1.1 This specification covers asphalt plank used for bridge decks as well as for industrial floors.  
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