iTeh StandardsiTeh Standards
EURUSD
Your shopping cart is empty.
ASTM

ASTM D4541-09e1

(Test Method)

Standard Test Method for Pull-Off Strength of Coatings Using Portable Adhesion Testers

Standard Test Method for Pull-Off Strength of Coatings Using Portable Adhesion Testers

SIGNIFICANCE AND USE
The pull-off strength of a coating is an important performance property that has been used in specifications. This test method serves as a means for uniformly preparing and testing coated surfaces, and evaluating and reporting the results. This test method is applicable to any portable apparatus meeting the basic requirements for determining the pull-off strength of a coating.
Variations in results obtained using different devices or different substrates with the same coating are possible (see Section 11). Therefore, it is recommended that the type of apparatus and the substrate be mutually agreed upon between the interested parties.
The purchaser or specifier shall designate a specific test method, that is, B, C, D, E, or F when calling out this standard.
SCOPE
1.1 This test method covers a procedure for evaluating the pull-off strength (commonly referred to as adhesion) of a coating system from metal substrates. Pull-off strength of coatings from concrete is described in Test Method D7234. The test determines either the greatest perpendicular force (in tension) that a surface area can bear before a plug of material is detached, or whether the surface remains intact at a prescribed force (pass/fail). Failure will occur along the weakest plane within the system comprised of the test fixture, adhesive, coating system, and substrate, and will be exposed by the fracture surface. This test method maximizes tensile stress as compared to the shear stress applied by other methods, such as scratch or knife adhesion, and results may not be comparable.
Note 1—The procedure in this standard was developed for metal substrates, but may be appropriate for other rigid substrates such as plastic and wood. Factors such as loading rate and flexibility of the substrate must be addressed by the user/specifier.
1.2 Pull-off strength measurements depend upon both material and instrumental parameters. Results obtained by each test method may give different results. Results should only be assessed for each test method and not be compared with other instruments. There are five instrument types, identified as Test Methods B-F. It is imperative to identify the test method used when reporting results.
Note 2—Method A, which appeared in previous versions of this standard, has been eliminated as its main use is for testing on concrete substrates (see Test Method D7234).
1.3 This test method uses a class of apparatus known as portable pull-off adhesion testers. They are capable of applying a concentric load and counter load to a single surface so that coatings can be tested even though only one side is accessible. Measurements are limited by the strength of adhesion bonds between the loading fixture and the specimen surface or the cohesive strengths of the adhesive, coating layers, and substrate.
1.4 This test can be destructive and spot repairs may be necessary.
1.5 The values stated in MPa (inch-pound) units are to be regarded as the standard. The values given in parentheses are for information only.
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
31-Jan-2009
ICS
87.040 - Paints and varnishes
Technical Committee
D01 - Paint and Related Coatings, Materials, and Applications
Drafting Committee
D01.46 - Industrial Protective Coatings
Current Stage
Ref Project

Buy Standard

ASTM D4541-09e1 - Standard Test Method for Pull-Off Strength of Coatings Using Portable Adhesion TestersASTM D4541-09e1 - Standard Test Method for Pull-Off Strength of Coatings Using Portable Adhesion Testers
PreviousNext
Standard
ASTM D4541-09e1 - Standard Test Method for Pull-Off Strength of Coatings Using Portable Adhesion Testers
English language
16 pages
sale 15% off
Preview
sale 15% off
Preview

Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
´1
Designation: D4541 − 09
Standard Test Method for
Pull-Off Strength of Coatings Using Portable Adhesion
1
Testers
This standard is issued under the fixed designation D4541; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1
ε NOTE—Practice D3980 was deleted from Section 2 in August 2010.
1. Scope* sion bonds between the loading fixture and the specimen
surface or the cohesive strengths of the adhesive, coating
1.1 This test method covers a procedure for evaluating the
layers, and substrate.
pull-off strength (commonly referred to as adhesion) of a
coating system from metal substrates. Pull-off strength of 1.4 This test can be destructive and spot repairs may be
coatingsfromconcreteisdescribedinTestMethodD7234.The necessary.
test determines either the greatest perpendicular force (in
1.5 The values stated in MPa (inch-pound) units are to be
tension) that a surface area can bear before a plug of material
regarded as the standard. The values given in parentheses are
is detached, or whether the surface remains intact at a pre-
for information only.
scribed force (pass/fail). Failure will occur along the weakest
1.6 This standard does not purport to address all of the
plane within the system comprised of the test fixture, adhesive,
safety concerns, if any, associated with its use. It is the
coating system, and substrate, and will be exposed by the
responsibility of the user of this standard to establish appro-
fracture surface. This test method maximizes tensile stress as
priate safety and health practices and determine the applica-
compared to the shear stress applied by other methods, such as
bility of regulatory limitations prior to use.
scratch or knife adhesion, and results may not be comparable.
NOTE 1—The procedure in this standard was developed for metal
2. Referenced Documents
substrates,butmaybeappropriateforotherrigidsubstratessuchasplastic
3
andwood.Factorssuchasloadingrateandflexibilityofthesubstratemust 2.1 ASTM Standards:
be addressed by the user/specifier.
D2651 GuideforPreparationofMetalSurfacesforAdhesive
Bonding
1.2 Pull-off strength measurements depend upon both ma-
terial and instrumental parameters. Results obtained by each D3933 Guide for Preparation of Aluminum Surfaces for
test method may give different results. Results should only be Structural Adhesives Bonding (Phosphoric Acid Anodiz-
assessed for each test method and not be compared with other ing)
instruments. There are five instrument types, identified as Test D7234 Test Method for Pull-OffAdhesion Strength of Coat-
Methods B-F. It is imperative to identify the test method used ings on Concrete Using Portable Pull-Off Adhesion Tes-
when reporting results. ters
NOTE 2—Method A, which appeared in previous versions of this
E691 Practice for Conducting an Interlaboratory Study to
standard, has been eliminated as its main use is for testing on concrete
Determine the Precision of a Test Method
substrates (see Test Method D7234).
2.2 ANSI Standard:
4
1.3 This test method uses a class of apparatus known as
N512 Protective Coatings (Paints) for the Nuclear Industry
2
portable pull-off adhesion testers. They are capable of apply-
2.3 ISO Standard:
4
ing a concentric load and counter load to a single surface so
ISO 4624 Paints and Varnish—Pull-Off Test for Adhesion
that coatings can be tested even though only one side is
3. Summary of Test Method
accessible. Measurements are limited by the strength of adhe-
3.1 The general pull-off test is performed by securing a
loading fixture (dolly, stud) normal (perpendicular) to the
1
This test method is under the jurisdiction of ASTM Committee D01 on Paint
and Related Coatings, Materials, andApplications and is the direct responsibility of
3
Subcommittee D01.46 on Industrial Protective Coatings. For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Current edition approved Feb. 1, 2009. Published April 2009. Originally contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
approved in 1993. Last previous edition approved in 2002 as D4541 – 02. DOI: Standards volume information, refer to the standar’s Document Summary page on
10.1520/D4541-09E01. the ASTM website.
2
4
The term adhesion tester may be somewhat of a misnomer, but its adoption by Available fromAmerican National Standards Institute (ANSI), 25 W. 43rd St.,
two manufacturers and at least two patents indicates continued usage. 4th Floor, New York, NY 10036, http://www.ansi.org.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box
...

Questions, Comments and Discussion

Ask us and Technical Secretary will try to provide an answer. You can facilitate discussion about the standard in here.

This May Also Interest You

ASTM
ASTM D7190-10(2023)(Practice)
Standard Practice to Evaluate Leaching of Water-Soluble Materials from Latex Paint Films

SIGNIFICANCE AND USE
4.1 Surfactant staining is a common problem with exterior house paints, particularly when subjected to humid environments (such as morning dew) shortly after application.  
4.2 Interior paints used in humid areas such as kitchens and bathrooms may also experience surfactant staining.  
4.3 Leaching of water-soluble materials may be dependent on colorant dispersions that are mixed into tint base paints. Other paint components may also affect the leaching of water-soluble materials.
SCOPE
1.1 This practice covers the ability of a latex paint film to resist staining caused by the leaching of water-soluble materials when contacted with water shortly after application.  
1.2 Water staining is attributed to the leaching of surfactants or other water-soluble materials from a paint film.  
1.3 The values stated in SI units are to be regarded as standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    2 pages
    English language
    sale 15% off
ASTM
ASTM D4287-00(2023)(Test Method)
Standard Test Method for High-Shear Viscosity Using a Cone/Plate Viscometer

SIGNIFICANCE AND USE
4.1 The viscosity value obtained by this test method gives information about the flow properties of the material under high-shear conditions similar to those encountered during application: brushing (see Test Method D4958), spraying, electrostatic disk, or roll coating.  
4.2 This test method is suitable for all paints and varnishes whether they are Newtonian in behavior or not. However, due to the narrow gap between the stationary and rotary parts of high-shear viscometers, this test method is more reproducible for paints having finer pigment dispersions as determined by Test Method D1210.
SCOPE
1.1 This test method covers the determination of the viscosity of paints, varnishes, and related products at a rate of shear of 12 000 s−1.  
1.2 Paints and varnishes that dry very rapidly may not give reproducible results with this test method. Measurements made at elevated temperatures may also give poor precision due to loss of volatiles and to drying.  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    4 pages
    English language
    sale 15% off
ASTM
ASTM D4214-23(Test Method)
Standard Test Methods for Evaluating the Degree of Chalking of Exterior Paint Films

SIGNIFICANCE AND USE
4.1 The procedures provide a broad range of techniques and photographic references to evaluate chalking of exterior paints.
SCOPE
1.1 These test methods cover the evaluation of the degree of chalking on white or tinted exterior paint films. These test methods describe the procedures recommended for transferring the chalk to a fabric or fingertip, which is then compared to photographic reference standards, or in the case of adhesive tapes, compared to a reflectance table or photographic reference standards, to determine the degree of chalking.  
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    7 pages
    English language
    sale 15% off
  • Standard
    7 pages
    English language
    sale 15% off
ASTM
ASTM D4147-18(2023)(Practice)
Standard Practice for Applying Coil Coatings Using Wire-Wound Drawdown Bars

SIGNIFICANCE AND USE
3.1 This practice is useful in the laboratory to simulate roll-coated films.
SCOPE
1.1 This practice covers a procedure for applying a coil coating film of uniform thickness on a flat metal panel using wire-wound drawdown bars.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    2 pages
    English language
    sale 15% off
ASTM
ASTM D16-23(Terminology)
Standard Terminology for Paint, Related Coatings, Materials, and Applications

SCOPE
1.1 This standard consists of technical terms used in standards under the jurisdiction of ASTM Committee D01 (on Paint and Related Coatings, Materials, and Applications), and of definitions suitable for use in these standards.
Note 1: When any definition in this standards is quoted or published out of the context of this standard, editorially insert the following delimiting statement “for paints and related coatings, materials, and applications” after the dash following the term (in the absence of an existing delimiting statement). This will limit the filed of application of the term and definition to that approved by this committee.  
1.2 In this terminology standard, definitions used in other ASTM standards are indicated by following the definition with the designation of that standard. In some cases, a relevant D01 subcommittee is also listed. Definitions influenced by those used by other organizations are indicated by the acronym of the organization. Primary terms are given in bold, while narrower and unapproved terms are given in italics.  
1.3 There are several specialized terminology standards under the jurisdiction of Committee D01, as follows: D804, D1695, D6440, D6488, and D7188. Few definitions from those standards are included in Terminology D16. Therefore, in searches for definitions of paints and coatings terms, these standards should be included where appropriate.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    10 pages
    English language
    sale 15% off
  • Standard
    10 pages
    English language
    sale 15% off
ASTM
ASTM D3732-23(Practice)
Standard Practice for Reporting Cure Times of Ultraviolet-Cured Coatings

SIGNIFICANCE AND USE
4.1 This practice provides a guide whereby all pertinent variables relating to the ultraviolet cure of a coating are described.
SCOPE
1.1 This practice applies to all coatings cured by ultraviolet energy.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    2 pages
    English language
    sale 15% off
  • Standard
    2 pages
    English language
    sale 15% off
ASTM
ASTM D1644-01(2023)(Test Method)
Standard Test Methods for Nonvolatile Content of Varnishes

SIGNIFICANCE AND USE
2.1 These test methods are applicable to varnish and are useful to producers and users in determining nonvolatile content and are sometimes an appropriate measure of the film-forming matter in varnish.
SCOPE
1.1 These test methods determine the fraction of a varnish that is nonvolatile at the temperature of the test while volatile solvents are driven off. It is sometimes an approximate measure of the film-forming matter in a varnish.  
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For a specific statement, see Section 3.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    2 pages
    English language
    sale 15% off
ASTM
ASTM D6486-23(Practice)
Standard Practice for Short Term Vehicle Service Exposure of Automotive Coatings

SIGNIFICANCE AND USE
4.1 Since the exposure of automotive coatings to the various mechanical and chemical stresses encountered in actual operations, is very opportunistic, obtaining statistically significant data from which valid conclusions can be drawn, requires rigorous attention to the experimental designs and conditions of exposure.
SCOPE
1.1 This practice covers the protocol for vehicle service exposure testing of automotive coatings. Such exposure testing is valuable for the verification of the performance of automotive coatings and correlation with laboratory test data. Vehicle service exposure is intended to provide short term (2 to 20 weeks) exposure to the stress factors associated with vehicle operation. Factors included are scratch, mar, impact, stone chipping, insect impact, bird dropping, tree sap and staining, environmental fallout, etc.
Note 1: Vehicle service exposure is not intended to provide the conditions that are needed for characterizing the long term effects of weathering or corrosion exposure.  
1.2 The exposure conditions are produced by the placement of multiple test panels of automotive finishes on automotive test fleets that traverse a defined road course. Exposure to the operating environment can be 20 h/day, 7 days/week allowing for accumulation of over 100 000 miles in 10 weeks of exposure.  
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    3 pages
    English language
    sale 15% off
  • Standard
    3 pages
    English language
    sale 15% off
ASTM
ASTM D2805-11(2023)(Test Method)
Standard Test Method for Hiding Power of Paints by Reflectometry

SIGNIFICANCE AND USE
5.1 This is a precise instrumental method giving results having an absolute physical significance without reference to a comparison paint. It should be used when maximum precision and minimum subjectivity are required, as in testing specification coatings or evaluating the hiding efficiency of pigments.  
5.2 Hiding power Test Method D344 is visual instead of instrumental, and gives results that are relative to a material standard instead of absolute. It is less precise than Test Method D2805 but more closely aligned with practical painting procedures.
SCOPE
1.1 This test method covers the determination, without reference to a material paint standard, of the hiding power of air dry coatings with Y tristimulus values greater than 15 %. With appropriate modification, it can also be used to test baking finishes.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    6 pages
    English language
    sale 15% off
ASTM
ASTM D6762-18(2023)(Test Method)
Standard Test Method for Determining the Hiding Power of Paint by Visual Evaluation of Spray Applied Coatings

SIGNIFICANCE AND USE
5.1 This test method determines hiding power of a test paint by visual evaluation of a spray applied coating.
Note 1: Test Method D2805 describes an instrumental method for determining hiding power. The paint film is applied at a uniform thickness (for example with a doctor blade), the film thickness is measured rigorously, and the opacity is determined photometrically. Hiding power is thereby determined with a high degree of precision.  
5.2 Test Method D6762 is less precise than Test Method D2805, but is commonly used since it is more closely related to the application characteristics of the paint and is simpler in concept and evaluation.
SCOPE
1.1 This test method provides for the quantitative visual determination of the film thickness required to achieve full hiding. This film thickness is considered to be the hiding power of a test paint.  
1.2 This method applies only to spray applied coatings but its concepts are valid for other methods of application as well.  
1.3 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    4 pages
    English language
    sale 15% off