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ASTM D2359-10

(Specification)

Standard Specification for Refined Benzene-535

Standard Specification for Refined Benzene-535

ABSTRACT
This specification covers a grade of benzene known as refined benzene-535. Different tests shall be performed in order to determine the following properties of refined benzene-535: minimum purity, maximum toluene content, maximum sulfur content, maximum thiophene content, maximum nonaromatic hydrocarbon content, maximum nitrogen content, water content, maximum acid wash color, appearance, maximum color, 1,4 dioxane content, and minimum solidification point with anhydrous basis.
SCOPE
1.1 This specification covers a grade of benzene known as refined benzene-535.
1.2 The following applies to all specified limits in this standard: for purposes of determining conformance with this standard, an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 Consult current OSHA regulations, supplier's Material Safety Data Sheets, and local regulations for all materials used in this specification.

General Information

Status
Historical
Publication Date
31-Jul-2010
ICS
87.060.30 - Solvents
Technical Committee
D16 - Aromatic, Industrial, Specialty and Related Chemicals
Drafting Committee
D16.01 - Benzene, Toluene, Xylenes, Cyclohexane and Their Derivatives
Current Stage
Ref Project

Relations

Replaces
ASTM D2359-09 - Standard Specification for Refined Benzene-535
Effective Date
01-Aug-2010
Replaced By
ASTM D2359-12 - Standard Specification for Refined Benzene-535
Effective Date
01-Nov-2012
Referred By
ASTM D4735-19 - Standard Test Method for Determination of Trace Thiophene in Refined Benzene by Gas Chromatography
Effective Date
01-Aug-2010
Referred By
ASTM D4790-23 - Standard Terminology of Aromatic Hydrocarbons and Related Chemicals
Effective Date
01-Aug-2010
Referred By
ASTM D7011-15(2019) - Standard Test Method for Determination of Trace Thiophene in Refined Benzene by Gas Chromatography and Sulfur Selective Detection
Effective Date
01-Aug-2010

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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D2359 −10
StandardSpecification for
1
Refined Benzene-535
This standard is issued under the fixed designation D2359; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope* D4492 Test Method for Analysis of Benzene by Gas Chro-
matography
1.1 This specification covers a grade of benzene known as
D4735 Test Method for Determination of Trace Thiophene
refined benzene-535.
in Refined Benzene by Gas Chromatography
1.2 The following applies to all specified limits in this
D5194 Test Method for Trace Chloride in Liquid Aromatic
standard: for purposes of determining conformance with this
Hydrocarbons
standard, an observed value or a calculated value shall be
D5386 Test Method for Color of Liquids Using Tristimulus
rounded off “to the nearest unit” in the last right-hand digit
Colorimetry
used in expressing the specification limit, in accordance with
D5808 Test Method for Determining Chloride in Aromatic
the rounding-off method of Practice E29.
Hydrocarbons and Related Chemicals by Microcoulom-
1.3 The values stated in SI units are to be regarded as
etry
standard. No other units of measurement are included in this D6069 Test Method for Trace Nitrogen in Aromatic Hydro-
standard.
carbons by Oxidative Combustion and Reduced Pressure
Chemiluminescence Detection
1.4 Consult current OSHA regulations, supplier’s Material
D6304 Test Method for Determination of Water in Petro-
Safety Data Sheets, and local regulations for all materials used
leum Products, Lubricating Oils, and Additives by Cou-
in this specification.
lometric Karl Fischer Titration
D6875 Test Method for Solidification Point of Industrial
2. Referenced Documents
Organic Chemicals by Thermistor
2
2.1 ASTM Standards:
D7011 Test Method for Determination of Trace Thiophene
D848 Test Method for Acid Wash Color of Industrial Aro-
in Refined Benzene by Gas Chromatography and Sulfur
matic Hydrocarbons
Selective Detection
D852 Test Method for Solidification Point of Benzene
D7183 Test Method for Determination of Total Sulfur in
D1209 Test Method for Color of Clear Liquids (Platinum-
Aromatic Hydrocarbons and Related Chemicals by Ultra-
Cobalt Scale)
violet Fluorescence
D1685 Test Method for Traces of Thiophene in Benzene by
D7184 Test Method for Ultra Low Nitrogen in Aromatic
3
Spectrophotometry (Withdrawn 2009)
Hydrocarbons by Oxidative Combustion and Reduced
D3437 Practice for Sampling and Handling Liquid Cyclic
Pressure Chemiluminescence Detection
Products
D7359 Test Method for Total Fluorine, Chlorine and Sulfur
in Aromatic Hydrocarbons and Their Mixtures by Oxida-
tive Pyrohydrolytic Combustion followed by Ion Chroma-
1
This specification is under the jurisdiction of ASTM Committee D16 on
tography Detection (Combustion Ion Chromatography-
Aromatic Hydrocarbons and Related Chemicals and is the direct responsibility of
CIC)
Subcommittee D16.01 on Benzene, Toluene, Xylenes, Cyclohexane and Their
Derivatives.
D7375 Test Method for Trace Quantities of Water in Aro-
Current edition approved Aug. 1, 2010. Published September 2010. Originally
matic Hydrocarbons and Their Mixtures by Coulometric
approved in 1966. Last previous edition approved in 2009 as D2359 – 09. DOI:
Karl Fischer Titration
10.1520/D2359-10.
2
D7536 Test Method for Chlorine in Aromatics by Mono-
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
chromatic Wavelength Dispersive X-ray Fluorescence
Standards volume information, refer to the standard’s Document Summary page on
Spectrometry
the ASTM website.
3 E29 Practice for Using Significant Digits in Test Data to
The last approved version of this historical standard is referenced on
www.astm.org. Determine Conformance with Specifications
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D2359 − 10
E1064 Test Method for Water in Organic Liquids by Coulo-
Nitrogen, max, mg/kg (if needed) D6069 or D7184
Water (if needed) D6304 or E1064 or
metric Karl Fischer Titration
D7375
2.2 Other Document:
Acid wash color, max pass with 1 D848
B
OSHA Regulations, 29 CFR paragraphs 1910.1000 and
Appearance .
4
Color, max, Pt–Co scale 20 D1209 or D5386
1910.1200
1,4 Dioxane (if needed) D4492
Solidification point, anhydrous 5.35 D852 or
3. Properties
basis, min, °C D6875
Chloride, max, mg/kg as needed D5194 or D5808 or
3.1 Refined benzene-535 shall conform to the following
D735
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation:D2359–09 Designation: D2359 – 10
Standard Specification for
1
Refined Benzene-535
This standard is issued under the fixed designation D2359; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope*
1.1 This specification covers a grade of benzene known as refined benzene-535.
1.2 The following applies to all specified limits in this standard: for purposes of determining conformance with this standard,
an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing
the specification limit, in accordance with the rounding-off method of Practice E29.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 Consult current OSHA regulations, supplier’s Material Safety Data Sheets, and local regulations for all materials used in
this specification.
2. Referenced Documents
2
2.1 ASTM Standards:
D848 Test Method for Acid Wash Color of Industrial Aromatic Hydrocarbons
D852 Test Method for Solidification Point of Benzene
D1209 Test Method for Color of Clear Liquids (Platinum-Cobalt Scale)
D1685 Test Method for Traces of Thiophene in Benzene by Spectrophotometry
D3437 Practice for Sampling and Handling Liquid Cyclic Products
D4492 Test Method for Analysis of Benzene by Gas Chromatography
D4735 Test Method for Determination of Trace Thiophene in Refined Benzene by Gas Chromatography
D5194 Test Method for Trace Chloride in Liquid Aromatic Hydrocarbons
D5386 Test Method for Color of Liquids Using Tristimulus Colorimetry
D5808 Test Method for Determining Chloride in Aromatic Hydrocarbons and Related Chemicals by Microcoulometry
D6069 Test Method for Trace Nitrogen in Aromatic Hydrocarbons by Oxidative Combustion and Reduced Pressure
Chemiluminescence Detection
D6304 Test Method for Determination of Water in Petroleum Products, Lubricating Oils, and Additives by Coulometric Karl
Fischer Titration
D6875 Test Method for Solidification Point of Industrial Organic Chemicals by Thermistor
D7011 Test Method for Determination of Trace Thiophene in Refined Benzene by Gas Chromatography and Sulfur Selective
Detection
D7183 Test Method for Determination of Total Sulfur in Aromatic Hydrocarbons and Related Chemicals by Ultraviolet
Fluorescence
D7184 Test Method for Ultra Low Nitrogen in Aromatic Hydrocarbons by Oxidative Combustion and Reduced Pressure
Chemiluminescence Detection
D7359 Test Method for Total Fluorine, Chlorine and Sulfur in Aromatic Hydrocarbons and Their Mixtures by Oxidative
Pyrohydrolytic Combustion followed by Ion Chromatography Detection (Combustion Ion Chromatography-CIC)
D7375 Test Method for Trace Quantities of Water inAromatic Hydrocarbons and Their Mixtures by Coulometric Karl Fischer
Titration
D7536 Test Method for Chlorine in Aromatics by Monochromatic Wavelength Dispersive X-ray Fluorescence Spectrometry
E29 Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
E1064 Test Method for Water in Organic Liquids by Coulometric Karl Fischer Titration
2.2 Other Document:
1
This specification is under the jurisdiction ofASTM Committee D16 onAromatic Hydrocarbons and Related Chemicals and is the direct responsibility of Subcommittee
D16.01 on Benzene, Toluene, Xylenes, Cyclohexane and Their Derivatives.
Current edition approved JuneAug. 1, 2009.2010. Published July 2009.September 2010. Originally approved in 1966. Last previous edition approved in 20082009 as
D2359 – 089. DOI: 10.1520/D2359-109.
2
For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at service@astm.org. ForAnnualBookofASTMStandards
volume information, refer to the standard’s Document Summary page on the ASTM website.
*ASummary of Changes section appears at the end of this standard.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D2359 – 10
3
OSHA Regulations, 29 CFR paragraphs 1910.1000 and 1910.1200
3
Available from U.S. Government Printing Office Superintendent of Documents, 732 N. Capitol St., NW, Mail Stop: SDE, Washington, DC 20401, http://
www.access.gpo.gov.
2

---------------------- Page: 2 --------------
...

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