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ASTM D3270-00(2006)

(Test Method)

Standard Test Methods for Analysis for Fluoride Content of the Atmosphere and Plant Tissues (Semiautomated Method)

Standard Test Methods for Analysis for Fluoride Content of the Atmosphere and Plant Tissues (Semiautomated Method)

SIGNIFICANCE AND USE
These test methods may be used for determining the fluoride content of particulate matter and gases collected from the atmosphere by passive and active means, including plant tissues. The user is warned that the fluoride content of passive collectors (including plants) give only qualitative or semiquantitative measurement of atmospheric fluoride content.
SCOPE
1.1 These test methods describe the semiautomated procedure for the analyses of various types of samples for the purpose of determining total fluoride. Since the test methods incorporate microdistillation of the sample, they may be applied to any fluoride-containing solution where standards of identical composition have been carried through the same sample preparation procedures and have proven to provide quantitative recovery when analyzed by the semiautomated system. Conversely, the methods shall not be applied for analyses until the applicability has been demonstrated.
1.2 In normal use, the procedure can detect 0.1 g/mL of F. The normal range of analysis is from 0.1 to 1.6 g/mL of F. Higher concentrations can be analyzed by careful dilution of samples with reagent water. If digested samples routinely exceed 1.6 g/mL of F, the analytical portion of the pump manifold can be modified to reduce sensitivity. However, the best procedure is to analyze a smaller aliquot of the sample. Most accurate results are obtained when the fluoride concentration falls in the middle or upper part of the calibration curve.
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See 8.3, 10.2.4, and 10.2.5 for additional precautions.

General Information

Status
Historical
Publication Date
31-Mar-2006
ICS
13.040.20 - Ambient atmospheres
Technical Committee
D22 - Air Quality
Drafting Committee
D22.03 - Ambient Atmospheres and Source Emissions
Current Stage
Ref Project

Relations

Replaces
ASTM D3270-00 - Standard Test Methods for Analysis for Fluoride Content of the Atmosphere and Plant Tissues (Semiautomated Method)
Effective Date
01-Apr-2006
Referred By
ASTM D3268-91(2018) - Standard Test Method for Separation and Collection of Particulate and Gaseous Fluorides in the Atmosphere (Sodium Bicarbonate-Coated Glass Tube and Particulate Filter Method)
Effective Date
01-Apr-2006
Referred By
ASTM D3267-20 - Standard Test Method for Separation and Collection of Particulate and Water-Soluble Gaseous Fluorides in the Atmosphere (Filter and Impinger Method)
Effective Date
01-Apr-2006
Referred By
ASTM D3266-91(2018) - Standard Test Method for Automated Separation and Collection of Particulate and Acidic Gaseous Fluoride in the Atmosphere (Double Paper Tape Sampler Method)
Effective Date
01-Apr-2006

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ASTM D3270-00(2006) - Standard Test Methods for Analysis for Fluoride Content of the Atmosphere and Plant Tissues (Semiautomated Method)ASTM D3270-00(2006) - Standard Test Methods for Analysis for Fluoride Content of the Atmosphere and Plant Tissues (Semiautomated Method)
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ASTM D3270-00(2006) - Standard Test Methods for Analysis for Fluoride Content of the Atmosphere and Plant Tissues (Semiautomated Method)
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D3270 − 00(Reapproved 2006)
Standard Test Methods for
Analysis for Fluoride Content of the Atmosphere and Plant
1
Tissues (Semiautomated Method)
This standard is issued under the fixed designation D3270; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D1356Terminology Relating to Sampling and Analysis of
Atmospheres
1.1 These test methods describe the semiautomated proce-
D3266Test Method for Automated Separation and Collec-
dure for the analyses of various types of samples for the
tion of Particulate and Acidic Gaseous Fluoride in the
purpose of determining total fluoride. Since the test methods
Atmosphere (Double Paper Tape Sampler Method)
incorporate microdistillation of the sample, they may be
D3267Test Method for Separation and Collection of Par-
applied to any fluoride-containing solution where standards of
ticulate and Water-Soluble Gaseous Fluorides in the At-
identical composition have been carried through the same
mosphere (Filter and Impinger Method)
sample preparation procedures and have proven to provide
D3268Test Method for Separation and Collection of Par-
quantitative recovery when analyzed by the semiautomated
ticulate and Gaseous Fluorides in the Atmosphere (So-
system. Conversely, the methods shall not be applied for
dium Bicarbonate-Coated Glass Tube and Particulate
analyses until the applicability has been demonstrated.
Filter Method)
1.2 In normal use, the procedure can detect 0.1 µg/mLof F.
D3269Test Methods for Analysis for Fluoride Content of
The normal range of analysis is from 0.1 to 1.6 µg/mL of F.
the Atmosphere and Plant Tissues (Manual Procedures)
Higher concentrations can be analyzed by careful dilution of 3
(Withdrawn 2010)
samples with reagent water. If digested samples routinely
D3614Guide for Laboratories Engaged in Sampling and
exceed 1.6 µg/mL of F, the analytical portion of the pump
Analysis of Atmospheres and Emissions
manifold can be modified to reduce sensitivity. However, the
best procedure is to analyze a smaller aliquot of the sample.
3. Terminology
Most accurate results are obtained when the fluoride concen-
3.1 Definitions—For definitions of terms used in these
trationfallsinthemiddleorupperpartofthecalibrationcurve.
methods, see Terminology D1356.
1.3 The values stated in SI units are to be regarded as the
standard. The values given in parentheses are for information
4. Summary of Test Methods
only.
4.1 These semiautomated methods are based on the distil-
1.4 This standard does not purport to address all of the
lation of hydrogen fluoride (HF) from the sample and subse-
safety concerns, if any, associated with its use. It is the
quent reaction of the distillate with alizarin fluorine blue-
responsibility of the user of this standard to establish appro-
lanthanum nitrate reagent, to form a blue complex which is
priate safety and health practices and determine the applica-
4
measured colorimetrically at 624 nm (1) , or the subsequent
bility of regulatory limitations prior to use.See8.3,10.2.4,and
measurement with a specific ion probe.
10.2.5 for additional precautions.
4.2 General, Plant Material:
2. Referenced Documents
4.2.1 The plant material including leaf samples, washed or
2
2.1 ASTM Standards:
unwashed, is dried, and ground, then dissolved with perchloric
D1193Specification for Reagent Water
acid and diluted to 50 mL with water. In the case of leaf
samples, an appreciable amount of fluoride may be deposited
1
These test methods are under the jurisdiction ofASTM Committee D22 on Air
on the external leaf surfaces. This fluoride behaves differently
Quality and are the direct responsibility of Subcommittee D22.03 on Ambient
physiologically from fluoride absorbed into the leaf and it is
Atmospheres and Source Emissions.
Current edition approved April 1, 2006. Published May 2006. Originally
approved in 1991. Last previous edition approved in 2000 as D3270-00. DOI:
10.1520/D3270-00R06.
2 3
For referenced ASTM standards, visit the ASTM website, www.astm.org, or The last approved version of this historical standard is referenced on
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM www.astm.org.
4
Standards volume information, refer to the standard’s Document Summary page on The boldface numbers in parentheses refer to the references at the end of this
the ASTM website. method.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D3270 − 00 (2006)
oftendesirabletowashitfromthesurfaceasapreliminarystep 4.5
...

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1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D1914-95(2022)(Practice)
Standard Practice for Conversion Units and Factors Relating to Sampling and Analysis of Atmospheres

SIGNIFICANCE AND USE
3.1 ASTM requires the use of SI units in all its publications and their use in reporting atmospheric measurement data. However, there are historic data and even data currently reported that are based on a variety of units of measurement. This practice tabulates factors that are necessary to convert such data to SI and other units of measurement.  
3.2 IEEE/ASTM SI-10 does not list all the conversion factors commonly used in air pollution and meteorological fields. This practice supplements IEEE/ASTM SI-10.  
3.3 The values reported here were obtained from a number of standard publications. They were adjusted to five figures and organized in a rational order. All values reflect the latest information from the 16th General Conference on Weights and Measurements held in 1979.  
3.4 The factors in Table 1 are provided to change units of measurement from one system to related units in other systems, as well as to smaller or larger units in the same system.  
3.5 Values of units in the left column may be converted to values of units in the right column merely by multiplying by the conversion factor provided in the center column.  (A) For specific applications and exceptions, see Terminology D1356.
SCOPE
1.1 This practice provides units and factors useful for members of the air pollution and meteorological communities.  
1.2 This practice is used together with IEEE/ASTM SI-10, which discusses SI units and contains selected conversion factors for inter-relation of SI units and some commonly used non-metric units.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D2914-15(2022)(Test Method)
Standard Test Methods for Sulfur Dioxide Content of the Atmosphere (West-Gaeke Method)

SIGNIFICANCE AND USE
5.1 Sulfur dioxide is a major air pollutant, commonly formed by the combustion of sulfur-bearing fuels. The Environmental Protection Agency (EPA) has set primary and secondary air quality standards (7) that are designed to protect the public health and welfare.  
5.2 The Occupational Safety and Health Administration (OSHA) has promulgated exposure limits for sulfur dioxide in workplace atmospheres (8).  
5.3 These methods have been found satisfactory for measuring sulfur dioxide in ambient and workplace atmospheres over the ranges pertinent in 5.1 and 5.2.  
5.4 Method A has been designed to correspond to the EPA-Designated Reference Method (7) for the determination of sulfur dioxide.
SCOPE
1.1 These test methods cover the bubbler collection and colorimetric determination of sulfur dioxide (SO2) in the ambient or workplace atmosphere.  
1.2 These test methods are applicable for determining SO2 over the range from approximately 25 μg/m3 (0.01 ppm(v)) to 1000 μg/m3 (0.4 ppm(v)), corresponding to a solution concentration of 0.03 μg SO2/mL to 1.3 μg SO2/mL. Beer's law is followed through the working analytical range from 0.02 μg SO2/mL to 1.4 μg SO2/mL.  
1.3 The lower limit of detection is 0.075 μg SO2/mL (1),2 representing an air concentration of 25 μg SO2/m3 (0.01 ppm(v)) in a 30-min sample, or 13 μg SO2/m3 (0.005 ppm(v)) in a 24-h sample.  
1.4 These test methods incorporate sampling for periods between 30 min and 24 h.  
1.5 These test methods describe the determination of the collected (impinged) samples. A Method A and a Method B are described.  
1.6 Method A is preferred over Method B, as it gives the higher sensitivity, but it has a higher blank. Manual Method B is pH-dependent, but is more suitable with spectrometers having a spectral band width greater than 20 nm.
Note 1: These test methods are applicable at concentrations below 25 μg/m3 by sampling larger volumes of air if the absorption efficiency of the particular system is first determined, as described in Annex A4.
Note 2: Concentrations higher than 1000 μg/m3 can be determined by using smaller gas volumes, larger collection volumes, or by suitable dilution of the collected sample with absorbing solution prior to analysis.  
1.7 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.8 Warning—Mercury has been designated by many regulatory agencies as a hazardous material that can cause serious medical issues. Mercury, or its vapor, has been demonstrated to be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury containing products. See the applicable product Safety Data Sheet (SDS) for additional information. Users should be aware that selling mercury and/or mercury containing products into your state or country may be prohibited by law.  
1.9 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific precautionary statements, see 8.3.1, Section 9, and A3.1.3.  
1.10 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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