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ASTM D3333-01

(Practice)

Standard Practice for Sampling Manufactured Staple Fibers, Sliver, or Tow for Testing

Standard Practice for Sampling Manufactured Staple Fibers, Sliver, or Tow for Testing

SCOPE
1.1 This practice covers a procedure for the division of shipments of man-made staple fiber, sliver (or top) or tow into lots and the sampling of such lots for testing.
Note 1--For sampling yarns, refer to Practice D2258.
Note 2--This practice differs from BISFA rules for staple fibers in the lot sampling, by the elimination of separate sampling of outer versus inner container areas, in the reduction of number of strata from 6 to 5, and by the elimination of compositing to obtain a single laboratory sample for the lot when testing properties which do not depend on as-received moisture content.
1.2  This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
09-Apr-2001
ICS
59.060.20 - Man-made fibres
Technical Committee
D13 - Textiles
Drafting Committee
D13.58 - Yarns and Fibers
Current Stage
Ref Project

Relations

Replaces
ASTM D3333-95 - Standard Practice for Sampling Manufactured Staple Fibers, Sliver, or Tow for Testing
Effective Date
10-Apr-2001
Replaced By
ASTM D3333-07 - Standard Practice for Sampling Manufactured Staple Fibers, Sliver, or Tow for Testing
Effective Date
01-Jan-2007
Referred By
ASTM D3937-12(2018) - Standard Test Method for Crimp Frequency of Manufactured Staple Fibers
Effective Date
10-Apr-2001
Referred By
ASTM D3217/D3217M-20 - Standard Test Methods for Breaking Tenacity of Manufactured Textile Fibers in Loop or Knot Configurations
Effective Date
10-Apr-2001
Referred By
ASTM D5103-07(2018) - Standard Test Method for Length and Length Distribution of Manufactured Staple Fibers (Single-Fiber Test)
Effective Date
10-Apr-2001
Referred By
ASTM D2612-99(2018) - Standard Test Method for Fiber Cohesion in Sliver and Top (Static Tests)
Effective Date
10-Apr-2001
Referred By
ASTM D2462-22 - Standard Test Method for Moisture in Wool by Distillation With Toluene
Effective Date
10-Apr-2001
Referred By
ASTM D2402-07(2018) - Standard Test Method for Water Retention of Textile Fibers (Centrifuge Procedure)
Effective Date
10-Apr-2001
Referred By
ASTM D2257-20 - Standard Test Method for Extractable Matter in Textiles
Effective Date
10-Apr-2001
Referred By
ASTM D7138-16 - Standard Test Method to Determine Melting Temperature of Synthetic Fibers
Effective Date
10-Apr-2001
Referred By
ASTM D1577-07(2018) - Standard Test Methods for Linear Density of Textile Fibers
Effective Date
10-Apr-2001
Referred By
ASTM D4120-07(2018) - Standard Test Method for Fiber Cohesion in Roving, Sliver, and Top in Dynamic Tests
Effective Date
10-Apr-2001
Referred By
ASTM D2102-02(2018) - Standard Test Method for Shrinkage of Textile Fibers (Bundle Test)
Effective Date
10-Apr-2001
Referred By
ASTM D3513-02(2018) - Standard Test Method for Overlength Fiber Content of Manufactured Staple Fiber
Effective Date
10-Apr-2001
Referred By
ASTM D4849-21 - Standard Terminology Related to Yarns and Fibers
Effective Date
10-Apr-2001

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ASTM D3333-01 - Standard Practice for Sampling Manufactured Staple Fibers, Sliver, or Tow for TestingASTM D3333-01 - Standard Practice for Sampling Manufactured Staple Fibers, Sliver, or Tow for Testing
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ASTM D3333-01 - Standard Practice for Sampling Manufactured Staple Fibers, Sliver, or Tow for Testing
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D3333–01
Standard Practice for
Sampling Manufactured Staple Fibers, Sliver, or Tow for
1
Testing
This standard is issued under the fixed designation D 3333; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope 3.1.1.1 Discussion—for the purposes of this standard, the
term container includes bales, cartons and other shipping units.
1.1 This practice covers a procedure for the division of
3.1.2 laboratory sample, n—a portion of material taken to
shipments of manufactured staple fiber, sliver (or top) or tow
represent the lot sample, or the original material, and used in
into lots and the sampling of such lots for testing.
the laboratory as a source of test specimens.
NOTE 1—For sampling yarns, refer to Practice D 2258.
3.1.3 lot, n—in acceptance testing, that part of a consign-
2
NOTE 2—This practice differs from BISFA rules for staple fibers in the
ment or shipment consisting of material from one production
lot sampling, by the elimination of separate sampling of outer versus inner
lot.
container areas, in the reduction of number of strata from 6 to 5, and by
3.1.4 lot sample, n—one or more shipping units taken at
the elimination of compositing to obtain a single laboratory sample for the
random to represent an acceptance sampling lot and used as a
lot when testing properties which do not depend on as-received moisture
content.
source of laboratory samples.
3.1.5 man-made staple fiber, n—fiber of spinnable length
1.2 This standard does not purport to address all of the
manufactured directly or by cutting filaments.
safety concerns, if any, associated with its use. It is the
3.1.6 primary sampling unit, n—the sampling unit contain-
responsibility of the user of this standard to establish appro-
ing all of the sources of variability which should be considered
priate safety and health practices and determine the applica-
in acceptance testing; the sampling unit taken in the first stage
bility of regulatory limitations prior to use.
of selection in any procedure for sampling a lot or shipment.
2. Referenced Documents
3.1.7 sample, n—(1) a portion of a lot of material which is
3
taken for testing or for record purposes. (2) a group of
2.1 ASTM Standards:
specimens used, or observations made, which provide infor-
D 123 Terminology Relating to Textiles
mation that can be used for making statistical inferences about
D 2258 Practice for Sampling Yarn for Testing
the population(s) from which the specimens were drawn. (See
D 2494 TestMethodforCommercialMassofaShipmentof
also lot sample, laboratory sample, and specimen.)
Yarn or Man-Made Staple Fiber or Tow
3.1.8 sampling unit, n—an identifiable, discrete unit or
D 4271 PracticeforWritingStatementsonSamplinginTest
subunit of material that could be taken as part of a sample.
Methods for Textiles
3.1.9 shipping unit, n—in textiles, any type of packaging
3. Terminology
used to facilitate the handling and shipping of fibers, yarns and
fabrics.
3.1 Definitions:
3.1.9.1 Discussion—For the purposes of this practice, pack-
3.1.1 container, n—areceptacledesignedtoholdamaterial,
aging includes bales, cartons, and other such containers.
or to give integrity to the material.
3.1.10 specimen, n—a specific portion of a material or a
laboratory sample upon which a test is performed or which is
1
ThispracticeisunderthejurisdictionofASTMCommitteeD13onTextilesand
selected for that purpose. (Syn. test specimen.)
is the direct responsibility of Subcommittee D13.58 onYarnTest Methods, General.
3.1.11 For definitions of other textile terms used in this
Current edition approved April 10, 2001. Published June 2001. Originally
practice, refer to Terminology D 123.
published as D 3333 – 74 T. Last previous edition D 3333 – 95.
2
BISFA Internationally Agreed Methods for Testing Polyamide Staple Fibers,
1974 edition, BISFA Internationally Agreed Methods for Testing Polyester Staple
4. Summary of Practice
Fibers, 1972 edition, and BISFA Rules for Testing Regenerated Cellulose and
4.1 Instructions are given for dividing containers into lots,
Acetate Staple Fibers, 1970 edition, available from the Bureau International pour la
Standardisation de la Rayonne et des Fibres Synthetiques. for determining the number of containers to be selected from
3
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
each lot as the lot sample, and for determining the number of
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
containers taken from the lot sample as a laboratory sample.
Standards volume information, refer to the standard’s Document Summary page on
...

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ASTM D3217/D3217M-20(Test Method)
Standard Test Methods for Breaking Tenacity of Manufactured Textile Fibers in Loop or Knot Configurations

SIGNIFICANCE AND USE
5.1 Both the loop breaking tenacity and the knot breaking tenacity, calculated from the breaking force measured under the conditions specified herein and the linear density of the fiber, are fundamental properties that are used to establish limitations on fiber-processing and upon their end-use applications. Physical properties, such as brittleness, not well defined by tests for breaking force and elongation can be estimated from the ratio of breaking tenacity measured in loop or knot tests, or both, and the normal tenacity as measured by Test Method D3822 provided both methods use the same gauge length and strain rate.  
5.2 This test method is not recommended for acceptance testing of commercial shipments in the absence of reliable information on between-laboratory precision (see Note 3). In some cases the purchaser and the supplier may have to test a commercial shipment of one or more specific materials by the best available method, even though the method has not been recommended for acceptance testing of commercial shipments. In such a case, if there is a disagreement arising from differences in values reported by the purchaser and the supplier when using this test method for acceptance testing, the statistical bias, if any, between the laboratory of the purchaser and the laboratory of the supplier should be determined with each comparison being based on testing specimens randomly drawn from one sample of material of the type being evaluated.
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1.1 These test methods cover the measurement of the breaking tenacity of manufactured textile fibers taken from filament yarns, staple, or tow fiber, either crimped or uncrimped, and tested in either a double loop or as a strand formed into a single overhand knot.  
1.2 Methods for measuring the breaking tenacity of conditioned and wet (immersed) fibers in loop and knot form are included.  
1.3 Elongation in loop or knot tests has no known significance, and is usually not recorded.  
1.4 The basic distinction between the procedures described in these test methods and those included in Test Methods D2101 is the configuration of the specimen, that is, either as a double loop or in the configuration of a single overhand knot.  
1.5 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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ASTM D3218-07(2018)(Specification)
Standard Specification for Polyolefin Monofilaments

ABSTRACT
This specification covers polyolefin monofilament yarn materials, and test methods for standard polyolefin monofilaments. The direct yarn number in tex or in denier, tensile properties in terms of breaking force, breaking tenacity, elongation at break and initial modulus shall be determined from a sample material. The width, thickness, gloss, hot water shrinkage, resistance to ultraviolet radiation, stability to thermal oxidation and cleanliness of the material shall also be analyzed.
SIGNIFICANCE AND USE
6.1 Acceptance Testing—The test methods in Specification D3218 for the determination of the properties of polyolefin monofilaments are considered satisfactory for acceptance testing of commercial shipments of polyolefin monofilaments, unless specified in the individual test method. These test methods are the best available and are used extensively in the trade.  
6.1.1 If there are differences or practical significance between reported test results for two laboratories (or more) comparative test should be performed to determine if there is a statistical bias between them, using competent statistical assistance. As a minimum, test samples that are as homogeneous as possible, drawn from the material from which the disparate test results were obtained, and randomly assigned in equal numbers to each laboratory for testing. The test results from the two laboratories should be compared using a statistical test for unpaired data, at a probability level chosen prior to the testing series. If a bias is found either its cause must be found and corrected or future test results for that material must be adjusted in consideration of the known bias.
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1.1 This specification covers polyolefin monofilament yarn materials, and test methods for standard polyolefin monofilaments. While designed primarily for testing standard polyolefin monofilaments, many of the procedures can be used, with little or no modification, for other polyolefin monofilaments. However, testing on non-standard polyolefin monofilaments should be conducted with caution. See 3.1 for a definition of standard polyolefin monofilament.  
1.2 Only on condition that interlaboratory precision data are available for the specific procedure is any test method described, or referenced in this specification, recommended for acceptance testing of commercial shipments of polyolefin monofilaments.  
1.3 The specification for polyolefin raw materials appears in Section 4.  
1.4 The test methods for individual properties appear in the following sections:    
Property  
Section  
Breaking Force  
10    
Breaking Tenacity  
10    
Elongation  
10    
Gloss  
13    
Hot Water Shrinkage  
14    
Initial Modulus  
10    
Polyolefin-Material Cleanliness  
17    
Resistance to Ultraviolet Radiation  
15    
Stability to Thermal Oxidation  
16    
Tensile Properties  
10    
Thickness  
12    
Width  
11    
Yarn Number  
9
Note 1: In most instances, the suitability of these procedures for polymeric yarns in general, and polyolefin monofilaments in particular, is already accepted in commercial transactions (see 6.1).  
1.5 The values stated in SI units are to be regarded as standard; the values in English units are provided as information only and are not exact equivalents.  
1.6 The following safety hazards caveat pertains only to the test methods described in this specification: This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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ASTM D5103-07(2018)(Test Method)
Standard Test Method for Length and Length Distribution of Manufactured Staple Fibers (Single-Fiber Test)

SIGNIFICANCE AND USE
5.1 This test method is used for research, development, quality control, product specifications, and may be used for acceptance testing of commercial shipments of textile fibers. However, caution is advised since information on between-laboratory precision is lacking. Comparative tests as directed in 5.1.1 may be advisable.  
5.1.1 If there are differences of practical significance between reported test results for two laboratories (or more), comparative tests should be performed to determine if there is a statistical bias between them, using competent statistical assistance. As a minimum, test samples that are as homogenous as possible, drawn from the material from which the disparate test results were obtained, and randomly assigned in equal numbers to each laboratory for testing. The test results from the two laboratories should be compared using a statistical test for upaired data, at a probability level chosen prior to the testing series. If a bias is found, either its cause must be found and corrected, or future test results for that material must be adjusted in consideration of the known bias.  
5.2 This test method provides objective measurements for determining the average fiber length and length distribution in a sample of fiber.  
5.3 The staple length diagram of a fiber sample can be used to determine the relative number of fibers above and below a specified length. If a fiber is too long, it will not process well in spinning, and if there is a preponderance of short fibers, the yarn might have lower than normal breaking strength.
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1.1 This test method covers the determination of average staple length and staple length distribution of both manufactured and natural fibers by manually measuring single fiber lengths. This test method is also used to measure the length of fibers removed from a staple yarn, but such a measurement may not represent the fiber's staple length, as manufactured.  
1.2 Because this test method requires measuring the length of only 50 fibers, it is not suitable for use in determining the number of long fibers that occur infrequently in a sample.  
Note 1: For determination for overlength fibers, refer to Test Method D3513.
Note 2: For methods covering the determination of the average length and length distribution of natural fibers, refer to the following methods: for cotton, Test Method D1440, and Test Method D1447, for wool, Test Method D519, Test Method D1234, and Test Method D1575.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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ASTM D3937-12(2018)(Test Method)
Standard Test Method for Crimp Frequency of Manufactured Staple Fibers

SIGNIFICANCE AND USE
5.1 This test method for the determination of crimp frequency of manufactured staple fibers may be used for the acceptance testing of commercial shipments but caution is advised since between-laboratory precision is known to be poor. Comparative tests conducted as directed in 5.1.1 may be advisable.  
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5.3 Crimp in fiber affects the carding and subsequent processing of the fiber into either a yarn or a nonwoven fabric.  
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1.1 This test method covers the determination of the crimp frequency of manufactured staple fibers. This test method is applicable to all crimped staple fibers provided the crimp can be viewed two-dimensionally as a sine-wave configuration.  
1.1.1 It should be recognized that yarn manufacturing processes or treatments to manufactured yarns can influence or modify crimp in fiber. Hence, the value for crimp of fibers taken from spun yarns may be different than that of the same fiber prior to the manufacturing or treatment processes.  
1.2 Three options are provided for preparation of the specimens. Option One (preferred) uses single fibers for the specimens with a low magnification available, Option Two (optional for staple or tow samples) uses fiber chips as the specimens, and Option Three uses projected images of single fibers.  
1.3 The values stated in SI units are to be regarded as the standard. The inch-pound units in parentheses are for information only.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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ASTM D3333-07(2018)(Practice)
Standard Practice for Sampling Manufactured Staple Fibers, Sliver, or Tow for Testing

SIGNIFICANCE AND USE
5.1 Assigning a value to any property of the material in a container or in a lot, consignment, or delivery involves a measurement process that includes both sampling and testing procedures. The correctness of the value assigned depends upon the variability due to testing. Even when the variability due to testing is minimized by carefully developed procedures, correct and consistent estimates of the true value of the property are possible only when the sampling procedure avoids systematic bias, minimizes variations due to sampling, and provides a laboratory sample of adequate size.  
5.2 This practice may not give the most efficient sampling plan that might be devised in special situations but it does present a general procedure that gives satisfactory precision with an economical amount of sampling and one which does not require elaborate statistical computation based on previous knowledge of the amount of variation between lot samples, between laboratory samples, and between test specimens.  
5.3 The smallest number of specimens required for a given variability in the average result will usually be obtained by (1) minimizing the number of shipping units in the lot sample, (2) taking one of the shipping units in the laboratory sample, and (3) taking the prescribed specimen(s) from the selected laboratory sample shipping unit. (See 7.3 and 7.4.)  
5.4 To minimize the cost of sampling a lot of material, it is necessary to agree on the required variance for the reported average for a lot of material:  
5.4.1 Estimate the variance due to lot samples, the variance due to laboratory samples, and the variance due to test specimens.  
5.4.2 Calculate the total variance for the average test results for several combinations of the number of lot samples, the number of laboratory samples per lot sample, and the number of test specimens per laboratory sample.  
5.4.3 Calculate the cost of performing each of the sampling schemes considered in 5.4.2.  
5.4.4 Select the samp...
SCOPE
1.1 This practice covers a procedure for the division of shipments of manufactured staple fiber, sliver (or top) or tow into lots and the sampling of such lots for testing.  
Note 1: For sampling yarns, refer to Practice D2258.
Note 2: This practice differs from BISFA2 rules for staple fibers in the lot sampling, by the elimination of separate sampling of outer versus inner container areas, in the reduction of number of strata from 6 to 5, and by the elimination of compositing to obtain a single laboratory sample for the lot when testing properties which do not depend on as-received moisture content.  
1.2 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D3513-02(2018)(Test Method)
Standard Test Method for Overlength Fiber Content of Manufactured Staple Fiber

SIGNIFICANCE AND USE
5.1 The existence of overlength fiber in manufactured staple can cause serious problems in the spinning of these fibers into yarn. Overlength fibers may create problems in carding, but more especially high-strength multiple cut fibers may cause cockling in spinning.  
5.2 Since the overlength fibers are caused by dull or damaged cutting knives or by uneven flow of tow to the staple cutter, their existence within the fiber population is not uniform and their occurrence in the population follows a highly skewed distribution.  
5.3 Manual methods of determining overlength fiber require much more operator time, and the standard deviations of the test between laboratories and operators are high. Use of the Fibrosampler method greatly reduces both operator time and standard deviation of testing.  
5.4 In manufacturing it is important to know if fibers are overlength due to looping of the tow or multiple length due to damaged cutters.  
5.5 This method for testing staple fiber for overlength fiber is not recommended for acceptance testing (see 13.1).  
5.5.1 In some cases the purchaser and the supplier may have to test a commercial shipment of one or more specific materials by the best available method, even though the method has not been recommended for acceptance testing of commercial shipments. If there are differences of practical significance between reported test results for two laboratories (or more), comparative test should be performed to determine if there is a statistical bias between them, using competent statistical assistance. As a minimum, use the samples for such a comparative tests that are as homogeneous as possible, drawn from the same lot of material as the samples that resulted in disparate results during initial testing and randomly assigned in equal numbers to each laboratory. The test results from the laboratories involved should be compared using a statistical test for unpaired data, a probability level chosen prior to the testing series. If a...
SCOPE
1.1 This test method covers the determination of the percent by number of overlength or multiple length fibers in a sample of manufactured cut staple. The method is applicable to fiber taken immediately after manufacturing, from the bale, or from partially processed stock.  
Note 1: For measurement of length and length distribution of manufactured staple fibers, refer to Test Method D5103.  
1.2 This test method covers procedures using the Fibrosampler Model 335A (inch-pound units), the Fibrosampler Model 335B (SI units), and Fibrosampler combs Model 336.  
1.2.1 The Fibrosampler Model 335A is equipped with a sample plate that has 15.8-mm (5/8-in.) diameter sample holes and is recommended for use on blended staple taken from the fiber blender or from a carding machine.  
1.2.2 The Fibrosampler Model 335B is equipped with a sample plate that has 10-mm (0.4-in.) diameter sample holes and is recommended for use on unblended staple as may be taken from the fiber cutter or from a bale of staple fiber.  
1.3 The values stated in either SI units or inch-pound units are to be regarded separately as the standard. The values stated in each unit are not exact equivalents; therefore, each unit must be used independently of the other.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D7138-16(Test Method)
Standard Test Method to Determine Melting Temperature of Synthetic Fibers

SIGNIFICANCE AND USE
5.1 Either of these two test methods is used to determine the temperature at which a synthetic fiber specimen changes from a solid to a liquid-like state.  
5.1.1 Synthetic fibers may be either amorphous or semi-crystalline thermoplastics or thermosets. Synthetic fibers may change from the solid to a liquid-like state on heating because of the glass transition of amorphous polymers, the melting of crystalline regions of semi-crystalline polymers, or at the onset of degradation. Thermoplastic fibers consist of crystalline and amorphous regions and may be manufactured with a range of molecular weights. The amorphous and crystalline fiber structure and variable molecular weight can lead to a melting temperature range instead of a discreet melting point (see Table X1.1).  
5.2 This test method is considered satisfactory for acceptance testing of commercial shipments.  
5.2.1 If there are differences of practical significance between reported test results for two or more laboratories, perform comparative testing to determine if there is a statistical bias between them, using competent statistical assistance. As a minimum, use the samples for such a comparative test that are as homogeneous as possible, drawn from the same lot of material as the samples that resulted in disparate results during initial testing and randomly assigned in equal numbers to each laboratory. Compare the test results from the laboratories involved using a statistical test for unpaired data, at a probability level chosen prior to the testing series. If bias is found, either its cause must be found and corrected, or future test results for that material must be adjusted in consideration of the known bias.  
5.3 This test method is suitable for quality control testing of synthetic fibers and product comparisons of different fibers by manufacturers, retailers, and users.  
5.4 If the test method is used to identify fiber material type, it is important to test a known reference material at the s...
SCOPE
1.1 Either of two test methods are used to determine the melting temperature of thermoplastic fibers, yarns, or threads.  
1.2 Method 1 can be used to determine melting temperatures for blends of multiple fiber material types. Method 2 can only be used to determine the melting temperature of a single fiber material type.  
1.2.1 Method 1, Differential Scanning Calorimetry (DSC), measures changes in heat capacity and will detect the glass transition, the crystalline melting and endothermic thermal degradation.  
1.2.2 Method 2, a visual determination of melting, determines any change that visually appears as a transition from a solid to a liquid state.  
1.2.3 Due to the differences in what each test method measures, the results from Method 1 and Method 2 cannot be compared.  
1.3 The values stated in either SI units or other units are to be regarded separately. The values stated in each system are not exact equivalents; therefore, each system shall be used independently without combining values.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

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ASTM D3217/D3217M-20(Test Method)
Standard Test Methods for Breaking Tenacity of Manufactured Textile Fibers in Loop or Knot Configurations

SIGNIFICANCE AND USE
5.1 Both the loop breaking tenacity and the knot breaking tenacity, calculated from the breaking force measured under the conditions specified herein and the linear density of the fiber, are fundamental properties that are used to establish limitations on fiber-processing and upon their end-use applications. Physical properties, such as brittleness, not well defined by tests for breaking force and elongation can be estimated from the ratio of breaking tenacity measured in loop or knot tests, or both, and the normal tenacity as measured by Test Method D3822 provided both methods use the same gauge length and strain rate.  
5.2 This test method is not recommended for acceptance testing of commercial shipments in the absence of reliable information on between-laboratory precision (see Note 3). In some cases the purchaser and the supplier may have to test a commercial shipment of one or more specific materials by the best available method, even though the method has not been recommended for acceptance testing of commercial shipments. In such a case, if there is a disagreement arising from differences in values reported by the purchaser and the supplier when using this test method for acceptance testing, the statistical bias, if any, between the laboratory of the purchaser and the laboratory of the supplier should be determined with each comparison being based on testing specimens randomly drawn from one sample of material of the type being evaluated.
SCOPE
1.1 These test methods cover the measurement of the breaking tenacity of manufactured textile fibers taken from filament yarns, staple, or tow fiber, either crimped or uncrimped, and tested in either a double loop or as a strand formed into a single overhand knot.  
1.2 Methods for measuring the breaking tenacity of conditioned and wet (immersed) fibers in loop and knot form are included.  
1.3 Elongation in loop or knot tests has no known significance, and is usually not recorded.  
1.4 The basic distinction between the procedures described in these test methods and those included in Test Methods D2101 is the configuration of the specimen, that is, either as a double loop or in the configuration of a single overhand knot.  
1.5 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM E2058-19(Test Method)
Standard Test Methods for Measurement of Material Flammability Using a Fire Propagation Apparatus (FPA)

SIGNIFICANCE AND USE
5.1 These test methods are an integral part of existing test standards for cable fire propagation and clean room material flammability, as well as, in an approval standard for conveyor belting (1-3).3 Refs (1-3) use these test methods because fire-test-response results obtained from the test methods correlate with fire behavior during real-scale fire propagation tests, as discussed in X1.4.  
5.2 The Ignition, Combustion, or Fire Propagation test method, or a combination thereof, have been performed with materials and products containing a wide range of polymer compositions and structures, as described in X1.7.  
5.3 The Fire Propagation test method is different from the test methods in the ASTM standards listed in 2.1 by virtue of producing laboratory measurements of the chemical heat release rate during upward fire propagation and burning on a vertical test specimen in normal air, oxygen-enriched air, or in oxygen-vitiated air. Test methods from other standards, for example, Test Method E1321, which yields measurements during lateral/horizontal or downward flame spread on materials and Test Methods E906, E1354, and E1623, which yield measurements of the rate of heat release from materials fully involved in flaming combustion, generally use an external radiant flux, rather than the flames from the burning material itself, to characterize fire behavior.  
5.4 These test methods are not intended to be routine quality control tests. They are intended for evaluation of specific flammability characteristics of materials. Materials to be analyzed consist of specimens from an end-use product or the various components used in the end-use product. Results from the laboratory procedures provide input to fire propagation and fire growth models, risk analysis studies, building and product designs, and materials research and development.
SCOPE
1.1 This fire-test-response standard determines and quantifies material flammability characteristics, related to the propensity of materials to support fire propagation, by means of a fire propagation apparatus (FPA). Material flammability characteristics that are quantified include time to ignition (tign), chemical ( Q˙chem), and convective ( Q˙c) heat release rates, mass loss rate ( m˙) and effective heat of combustion (EHC).  
1.2 The following test methods, capable of being performed separately and independently, are included herein:  
1.2.1 Ignition Test, to determine tign  for a horizontal specimen;  
1.2.2 Combustion Test, to determine  Q˙chem,  Q˙c,  m˙, and EHC from burning of a horizontal specimen; and,  
1.2.3 Fire Propagation Test, to determine  Q˙chem  from burning of a vertical specimen.  
1.3 Distinguishing features of the FPA include tungsten-quartz external, isolated heaters to provide a radiant flux of up to 110 kW/m2 to the test specimen, which remains constant whether the surface regresses or expands; provision for combustion or upward fire propagation in prescribed flows of normal air, air enriched with up to 40 % oxygen, air oxygen vitiated, pure nitrogen or mixtures of gaseous suppression agents with the preceding air mixtures; and, the capability of measuring heat release rates and exhaust product flows generated during upward fire propagation on a vertical test specimen 0.305 m high.  
1.4 The FPA is used to evaluate the flammability of materials and products. It is also designed to obtain the transient response of such materials and products to prescribed heat fluxes in specified inert or oxidizing environments and to obtain laboratory measurements of generation rates of fire products (CO2, CO, and, if desired, gaseous hydrocarbons) for use in fire safety engineering.  
1.5 Ignition of the specimen is by means of a pilot flame at a prescribed location with respect to the specimen surface.  
1.6 The Fire Propagation test of vertical specimens is not suitable for materials that, on heating, melt sufficiently to form a liquid pool...

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ASTM
ASTM D3218-07(2018)(Specification)
Standard Specification for Polyolefin Monofilaments

ABSTRACT
This specification covers polyolefin monofilament yarn materials, and test methods for standard polyolefin monofilaments. The direct yarn number in tex or in denier, tensile properties in terms of breaking force, breaking tenacity, elongation at break and initial modulus shall be determined from a sample material. The width, thickness, gloss, hot water shrinkage, resistance to ultraviolet radiation, stability to thermal oxidation and cleanliness of the material shall also be analyzed.
SIGNIFICANCE AND USE
6.1 Acceptance Testing—The test methods in Specification D3218 for the determination of the properties of polyolefin monofilaments are considered satisfactory for acceptance testing of commercial shipments of polyolefin monofilaments, unless specified in the individual test method. These test methods are the best available and are used extensively in the trade.  
6.1.1 If there are differences or practical significance between reported test results for two laboratories (or more) comparative test should be performed to determine if there is a statistical bias between them, using competent statistical assistance. As a minimum, test samples that are as homogeneous as possible, drawn from the material from which the disparate test results were obtained, and randomly assigned in equal numbers to each laboratory for testing. The test results from the two laboratories should be compared using a statistical test for unpaired data, at a probability level chosen prior to the testing series. If a bias is found either its cause must be found and corrected or future test results for that material must be adjusted in consideration of the known bias.
SCOPE
1.1 This specification covers polyolefin monofilament yarn materials, and test methods for standard polyolefin monofilaments. While designed primarily for testing standard polyolefin monofilaments, many of the procedures can be used, with little or no modification, for other polyolefin monofilaments. However, testing on non-standard polyolefin monofilaments should be conducted with caution. See 3.1 for a definition of standard polyolefin monofilament.  
1.2 Only on condition that interlaboratory precision data are available for the specific procedure is any test method described, or referenced in this specification, recommended for acceptance testing of commercial shipments of polyolefin monofilaments.  
1.3 The specification for polyolefin raw materials appears in Section 4.  
1.4 The test methods for individual properties appear in the following sections:    
Property  
Section  
Breaking Force  
10    
Breaking Tenacity  
10    
Elongation  
10    
Gloss  
13    
Hot Water Shrinkage  
14    
Initial Modulus  
10    
Polyolefin-Material Cleanliness  
17    
Resistance to Ultraviolet Radiation  
15    
Stability to Thermal Oxidation  
16    
Tensile Properties  
10    
Thickness  
12    
Width  
11    
Yarn Number  
9
Note 1: In most instances, the suitability of these procedures for polymeric yarns in general, and polyolefin monofilaments in particular, is already accepted in commercial transactions (see 6.1).  
1.5 The values stated in SI units are to be regarded as standard; the values in English units are provided as information only and are not exact equivalents.  
1.6 The following safety hazards caveat pertains only to the test methods described in this specification: This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.7 This international standard was developed in accordance with internationally recognized principles on ...

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