ASTM E2623-14(2021)
(Practice)Standard Practice for Reporting Thermometer Calibrations
Standard Practice for Reporting Thermometer Calibrations
SIGNIFICANCE AND USE
5.1 This practice is adequate for use with all ASTM Test Methods which require the reporting of temperature measurements.
5.2 The Report of Calibration, however named, is the physical output of the calibration laboratory. It shall be prepared so that both the results of the measurement(s) and the non-technical information necessary to support those results are conveyed in a manner that ensures accurate communication and justification of the results.
5.3 This practice is not meant to supersede requirements of other standards practice such as ISO/IEC 17025 or ANSI/NCSL Z540.3.
SCOPE
1.1 This practice contains reporting requirements for thermometer calibrations included in ASTM Committee E20 Test Methods.
1.2 This practice covers reports of calibration for radiation thermometers, liquid-in-glass thermometers, resistance thermometers, digital thermometers, and new thermocouples.
Note 1: This practice does not apply to used thermocouples.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
General Information
Relations
Standards Content (Sample)
This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: E2623 − 14 (Reapproved 2021)
Standard Practice for
Reporting Thermometer Calibrations
This standard is issued under the fixed designation E2623; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope ISO/IEC 17025:2005 General Requirements for the Compe-
tence of Testing and Calibration Laboratories
1.1 This practice contains reporting requirements for ther-
JCGM100:2008 Evaluation of Measurement Data—Guide
mometer calibrations included in ASTM Committee E20 Test
to the Expression of Uncertainty in Measurement
Methods.
ISO/IEC Guide 98-3 Uncertainty of Measurement—Part 3:
1.2 This practice covers reports of calibration for radiation
Guide to the Expression of Uncertainty in Measurement
thermometers, liquid-in-glass thermometers, resistance
(GUM:1995)
thermometers, digital thermometers, and new thermocouples.
NIST Technical Note 1297 Guidelines for Evaluating and
NOTE 1—This practice does not apply to used thermocouples.
Expressing the Uncertainty of NIST Measurement
1.3 This standard does not purport to address all of the
Results, 1994 Edition
safety concerns, if any, associated with its use. It is the
UKAS M3003 The Expression of Uncertainty and Confi-
responsibility of the user of this standard to establish appro-
dence in Measurement, Edition 2
priate safety, health, and environmental practices and deter-
ANSI/NCSL Z540.2-1997 (R2002) U.S. Guide to the Ex-
mine the applicability of regulatory limitations prior to use.
pression of Uncertainty in Measurement
1.4 This international standard was developed in accor-
dance with internationally recognized principles on standard-
3. Terminology
ization established in the Decision on Principles for the
3.1 Definitions—Definitions given in Terminology E344,
Development of International Standards, Guides and Recom-
unless otherwise defined herein, apply to terms as used in this
mendations issued by the World Trade Organization Technical
practice.
Barriers to Trade (TBT) Committee.
3.2 Definitions of Terms Specific to This Standard:
2. Referenced Documents
3.2.1 correction, n—numerical value added to the uncor-
rected result of a measurement to compensate for errors.
2.1 ASTM Standards:
3.2.1.1 Discussion—The correction is equal to the negative
E77 Test Method for Inspection and Verification of Ther-
of the estimated errors. Since the systematic error cannot be
mometers
known perfectly, the compensation cannot be complete.
E344 Terminology Relating to Thermometry and Hydrom-
etry
3.2.2 error, n—the indication of a thermometer or tempera-
E1137 SpecificationforIndustrialPlatinumResistanceTher-
ture measuring device minus the true value of the correspond-
mometers
ing input quantity.
2.2 Other Standards or Guides: 3.2.2.1 Discussion—Since the true value cannot be
ANSI/NCSL Z540.3-2006 American National Standard for determined, in practice a conventional true value is used. This
Calibration—Calibration Laboratories and Measuring and concept applies mainly when the instrument is compared to a
Test Equipment—General Requirements reference standard.
3.2.3 gradient zone, n—thesectionofathermocouplethatis
exposed during a measurement to temperatures in the range
ThispracticeisunderthejurisdictionofASTMCommitteeE20onTemperature
from t + 0.1(t – t )to t + 0.9(t – t ), where t is
Measurement and is the direct responsibility of Subcommittee E20.07 on Funda- amb m amb amb m amb amb
mentals in Thermometry.
ambienttemperatureand t isthetemperatureofthemeasuring
m
Current edition approved Nov. 1, 2021. Published November 2021. Originally
junction (all in °C).
approved in 2008. Last previous edition approved in 2014 as E2623 – 14. DOI:
3.2.3.1 Discussion—This term is used in thermocouple cali-
10.1520/E2623-14R21.
bration reports as part of the description of the thermal profile
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
along the length of the thermocouple. Although thermocouple
Standards volume information, refer to the standard’s Document Summary page on
emf is a function of the measuring and reference junction
the ASTM website.
temperatures, the emf is actually generated along the length of
Available fromAmerican National Standards Institute (ANSI), 25 W. 43rd St.,
4th Floor, New York, NY 10036, http://www.ansi.org. thethermocouple,whereverthethermoelementspassthrougha
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
E2623 − 14 (2021)
temperature gradient. The gradient zone definition is intended 6.1.6 Description of the thermometer or thermocouple, the
to describe, in an approximate way, the section of thermo- overall range, and, if different, the calibrated range. This shall
couple that created most of the emf during the calibration. also include the manufacturer, model number (as applicable),
identification or unique serial number, and the condition of the
3.2.4 half-maximum heated length, n—the distance between
thermometer or thermocouple upon receipt.
the tip of the temperature sensor and the position along the
6.1.7 Date of Calibration:
length of the sensor leads or sheath where the temperature
equals the average of the calibration-point and ambient tem-
6.1.7.1 Where applicable, additional dates, including date
peratures. received, date of report preparation and next due date may be
3.2.4.1 Discussion—This term is used in thermocouple cali-
included.
bration reports as part of the description of the thermal profile
6.1.8 Calibration Results—This can take the form of a table
along the length of the thermocouple.
with reading of standard temperature, reading of test
instrument, corrections to be applied and consistent units of
4. Summary of Practice
measureoranyformofreportingasrequestedbythecustomer.
4.1 This practice describes the required information neces-
6.1.8.1 When an instrument has been repaired or adjusted,
sary for reporting results of temperature calibrations included
the calibration results before and after repair or adjustment
in ASTM Test Methods.
shall be reported, if available.
6.1.9 Conditions (for example, environmental conditions)
5. Significance and Use
under which the calibrations were made that have an influence
on the measurement results.
5.1 This practice is adequate for use with all ASTM Test
Methods which require the reporting of temperature measure-
6.1.10 A statement of the estimated uncertainty(ies) of
ments.
measurement and the corresponding level of confidence.
6.1.10.1 Method for estimating uncertainties. Internation-
5.2 The Report of Calibration, however named, is the
ally the BIPM document JCGM100:2008 (“Guide to the
physical output of the calibration laboratory. It shall be
Expression of Uncertianty of Measurement”) is cited, ISO/IEC
prepared so that both the results of the measurement(s) and the
non-technical information necessary to support those results Guide 98-3, NIST Technical Note 1297, UKAS M3003 and
Z540.2-1997 (R2002) also meet this requirement.
areconveyedinamannerthatensuresaccuratecommunication
and justification of the results.
6.1.10.2 Coverage factor and estimated confidence interval.
Typically the coverage factor (k) is 2 for an approximate
5.3 This practice is not meant to supersede requirements of
confidence level of 95%.
other standards practice such as ISO/IEC 17025 or ANSI/
6.1.11 Traceability statement to the International System of
NCSL Z540.3.
Units (SI) through the National Institute of Standards and
6. Procedure Technology (NIST) or other National Metrological Institute
(NMI) of test equipment used in the test or calibration.
6.1 Requirements for Written Report— The requirements in
6.1.12 Signature or equivalent identification of the respon-
6.1.1 through 6.1.14 are mandatory for all written reports
sible party.
issued in compliance with this practice. Subsections 6.1.15
through 6.1.19 include general provisions for information that 6.1.12.1 Other signatures may be required, at the discretion
of the laboratory manager. Each signatory or named person
may be omitted if not required by a calibration procedure or
client/user. accepts responsibility for the contents of the report.
6.1.1 Title Examples—Report of Calibration, Calibration
6.1.13 Astatementspecifyingthatthecalibrationcertificate,
Certificate, Test Report or Test Certificate.
howevernamed,shallnotbereproducedexceptinfull,without
6.1.2 Name and address of the laboratory and location
written approval of the laboratory.
where the calibration was performed, if different from the
6.1.14 Statement of Temperature Scale (for example, Inter-
laboratory address.
national Temperature Scale of 1990 (ITS-90)).
6.1.3 Unique identification of the report or certificate, and
6.1.15 Where appropriate and needed, opinions and
on each page an identification in order to ensure that the page
interpretations, including additional information which may be
is recognized as part of the report or certificate, a clear
required by specific methods, clients or groups of clients.
identification of the end of the report or certificate, and the
6.1.16 Where relevant, a sampling plan and procedure and a
page number and total number of pages.
statement to the effect that the results relate only to the items
6.1.4 Name and address of the client.
calibrated.
6.1.5 Statement and concise description of the test method
6.1.17 Where relevant, a statement of compliance/non-
or calibration procedure used. This statement shall include
compliance with requirements or specification, or both.
revisions and the date of the test method or calibration
procedure. Test methods can consist of published standards 6.1.17.1 Compliancemayrefertoallcriteria,includingboth
(such as ASTM Test Methods), internally developed methods, specifications and maximum permissible error, of a referenced
or a combination of both. standard. When the scope of calibration is limited to only
6.1.5.1 Information describing deviations from previously certain portions of the standard, the statement of compliance
agreed-upon procedures. shall cite and be limited to those sections of the referenced
E2623 − 14 (2021)
standard with which the thermometer complies. If non- 6.4.7 Fitting equation or reference to fitting equation, if
compliance is to be noted, the statement should cite those applicable.
sections of the referenced standard for which the thermometer
6.4.8 Fitting residuals, if applicable.
fails to comply. 6.4.9 Repeatability results, if applicable.
6.1.18 Date of receipt of calibration item where this is
6.5 Additional Requirements for Reported Calibrations of
critical to the validity and application of the results.
Thermocouples—The requirements in 6.5.1 and 6.5.2 are
6.1.19 When applicable, customer purchase order or refer-
mandatory for all written reports for thermocouples issued in
ence number and date.
compliance with this practice. Subsections 6.5.3 – 6.5.6 in-
6.2 Additional Requirements for All Reported Calibrations
clude general provisions for information that may be omitted if
for Radiation Thermometers only: not required by a calibration procedure or the client/user.
6.2.1 Statement of source type (blackbody, filament lamp,
6.5.1 Mathematical description of any fitting equation used
and so forth).
in reporting the results of the calibration. The equation may
6.2.2 Statement of source aperture or diameter of flat type
consist of a deviation function modeling the difference in emf
sources.
from a reference function of a stated thermocouple type, or the
6.2.3 Statement of measuring distances between the objec-
equation may consist of a function giving emf-versus-
tive lens and the source aperture or cavity bottom, or both.
measuring junction temperature.
6.2.4 Statement of aperture distance, if an aperture is used.
6.5.2 Statement whether any allowance is included in the
6.2.5 Statement of field-of-view or size of source (as refer-
uncertainty for thermocouple drift and inhomogeneity.
enced to the thermometer under test).
6.5.3 Immersion depth used during the test.
6.2.6 Statement of emissivity of the thermometer under test
6.5.4 Gradient zone of the thermocouple during the test.
(emissivity setting of the thermometer under test).
6.5.5 Statement of calibration set up, if applicable.
6.2.7 Statement of source emissivity.
6.5.6 Reference junction temperature.
6.2.8 Statement of the spectral response of the thermometer
6.6 Additional Requirements for Reported Calibrations of
under test.
Digital Thermometers—The requirements in 6.6.1 – 6.6.3 are
6.2.9 Statement of traceability of the source through contact
mandatory for all written reports for digital thermometers
or radiation thermometry.
issued in compliance with this practice. Subsections 6.6.4 –
6.3 Additional Requirements for All Reported Calibrations
6.6.6 include general provisions for information that may be
of Liquid-in-Glass Thermometers:
omitted if not required by a calibration procedure or the
6.3.1 Statement of minimum length of time at test tempera-
client/user.
ture before reading.
6.6.1 For digital thermometers with multiple probes or
multiple channels, or both, the report shall identify each
NOTE 2—The time allowed for equilibrium of a liquid-in-glass ther-
mometer is dependent on the type of thermometric liquid used. For the
thermometer probe calibrated and each corresponding channel
purposes of this practice, the timing device for this measurement does not
used for the calibration.
need to be traceable to an National Metrology Institute (NMI).
6.6.2 For digital thermometers that include one or more
6.3.2 Statement of emergent stem temperature either in
algorithms for temperature conversion, the report shall include
chart or text form (for partial immersion thermometers or total
a method of conversion statement, identifying the method(s),
immersion thermometers calibrated with partial immersion
all relevant standards, and identify coefficients (if applicable)
only).
used for each thermometer channel and probe calibrated.
6.6.3 Where a digital thermometer is checked without a
6.4 Additional Requirements for Reported Calibrations of
thermometer probe using either resistance or voltage
Resistance Thermometers—The requirements in 6.4.1 – 6.4.4
simulation, each sensor type or curve, or both, shall be
are mandatory for al
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