ASTM E1775-20
(Guide)Standard Guide for Evaluating Performance of On-Site Extraction and Field-Portable Electrochemical or Spectrophotometric Analysis for Lead
Standard Guide for Evaluating Performance of On-Site Extraction and Field-Portable Electrochemical or Spectrophotometric Analysis for Lead
SIGNIFICANCE AND USE
4.1 This guide is intended for use in evaluating the performance of field-portable electroanalytical or spectrophotometric devices for lead determination, or both.
4.2 Desired performance criteria for field-based extraction procedures are provided.
4.3 Performance parameters of concern may be determined using protocols that are referenced in this guide.
4.4 Example reference materials to be used in assessing the performance of field-portable lead analyzers are listed.
4.5 Exhaustive details regarding quality assurance issues are outside the scope of this guide. Applicable quality assurance aspects are dealt with extensively in references that are cited in this guide.
SCOPE
1.1 This guide provides guidelines for determining the performance of field-portable quantitative lead analysis instruments.
1.2 This guide applies to field-portable electroanalytical and spectrophotometric (including reflectance and colorimetric) analyzers.
1.3 Sample matrices of concern herein include paint, dust, soil, and airborne particles.
1.4 This guide addresses the desired performance characteristics of field-based sample extraction procedures for lead, as well as on-site extraction followed by field-portable analysis.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
General Information
Relations
Buy Standard
Standards Content (Sample)
This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: E1775 − 20
Standard Guide for
Evaluating Performance of On-Site Extraction and Field-
Portable Electrochemical or Spectrophotometric Analysis
1
for Lead
This standard is issued under the fixed designation E1775; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D5438 Practice for Collection of Floor Dust for Chemical
Analysis
1.1 This guide provides guidelines for determining the
D6785 TestMethodforDeterminationofLeadinWorkplace
performance of field-portable quantitative lead analysis instru-
Air Using Flame or Graphite Furnace Atomic Absorption
ments.
Spectrometry
1.2 This guide applies to field-portable electroanalytical and
D6966 Practice for Collection of Settled Dust Samples
spectrophotometric (including reflectance and colorimetric)
Using Wipe Sampling Methods for Subsequent Determi-
analyzers.
nation of Metals
1.3 Sample matrices of concern herein include paint, dust,
D7035 Test Method for Determination of Metals and Met-
soil, and airborne particles.
alloids in Airborne Particulate Matter by Inductively
1.4 This guide addresses the desired performance character- Coupled Plasma Atomic Emission Spectrometry (ICP-
istics of field-based sample extraction procedures for lead, as AES)
well as on-site extraction followed by field-portable analysis. D7144 Practice for Collection of Surface Dust by Micro-
vacuum Sampling for Subsequent Metals Determination
1.5 This standard does not purport to address all of the
D7439 Test Method for Determination of Elements in Air-
safety concerns, if any, associated with its use. It is the
borne Particulate Matter by Inductively Coupled Plasma-
responsibility of the user of this standard to establish appro-
–Mass Spectrometry
priate safety, health, and environmental practices and deter-
E1583 Practice for Evaluating Laboratories Engaged in De-
mine the applicability of regulatory limitations prior to use.
termination of Lead in Paint, Dust, Airborne Particulates,
1.6 This international standard was developed in accor-
dance with internationally recognized principles on standard- and Soil Taken From and Around Buildings and Related
ization established in the Decision on Principles for the Structures
Development of International Standards, Guides and Recom-
E1605 Terminology Relating to Lead in Buildings
mendations issued by the World Trade Organization Technical E1644 Practice for Hot Plate Digestion of Dust Wipe
Barriers to Trade (TBT) Committee.
Samples for the Determination of Lead
E1645 Practice for Preparation of Dried Paint Samples by
2. Referenced Documents
Hotplate or Microwave Digestion for Subsequent Lead
2
2.1 ASTM Standards:
Analysis
D1356 Terminology Relating to Sampling and Analysis of
E1726 Practice for Preparation of Soil Samples by Hotplate
Atmospheres
Digestion for Subsequent Lead Analysis
E1728/E1728M Practice for Collection of Settled Dust
1
Samples Using Wipe Sampling Methods for Subsequent
This guide is under the jurisdiction of ASTM Committee D22 on Air Quality
and is the direct responsibility of Subcommittee D22.12 on Sampling andAnalysis
Lead Determination
of Lead for Exposure and Risk Assessment.
E1727 Practice for Field Collection of Soil Samples for
Current edition approved Sept. 1, 2020. Published September 2020. Originally
Subsequent Lead Determination
approved in 1996. Last previous edition approved in 2016 as E1775 – 16. DOI:
10.1520/E1775-20.
E1729 Practice for Field Collection of Dried Paint Samples
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
for Subsequent Lead Determination
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
E1792 Specification for Wipe Sampling Materials for Lead
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. in Surface Dust
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
E1775 − 20
E3193 Test Method for Measurement of Lead (Pb) in Dust wavelengths is measured by a detector. The amount of ab-
by Wipe, Paint, and Soil by Flame Atomic Absorption sorbed light is a function of the concentration of analyte
Spectrophotometry (FAAS) species.
E3203 Test Method for Determination of Lead in Dried
Paint, Soil, and Wipe Samples by Inductively Coupled 4. Significance and Use
Plasma-Optical Emission Spectroscopy (ICP-OES)
4.1 This
...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: E1775 − 16 E1775 − 20
Standard Guide for
Evaluating Performance of On-Site Extraction and Field-
Portable Electrochemical or Spectrophotometric Analysis
1
for Lead
This standard is issued under the fixed designation E1775; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This guide provides guidelines for determining the performance of field-portable quantitative lead analysis instruments.
1.2 This guide applies to field-portable electroanalytical and spectrophotometric (including reflectance and colorimetric)
analyzers.
1.3 Sample matrices of concern herein include paint, dust, soil, and airborne particles.
1.4 This guide addresses the desired performance characteristics of field-based sample extraction procedures for lead, as well as
on-site extraction followed by field-portable analysis.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety safety, health, and healthenvironmental practices and determine the
applicability of regulatory limitations prior to use.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
D1356 Terminology Relating to Sampling and Analysis of Atmospheres
D5438 Practice for Collection of Floor Dust for Chemical Analysis
D6785 Test Method for Determination of Lead in Workplace Air Using Flame or Graphite Furnace Atomic Absorption
Spectrometry
D6966 Practice for Collection of Settled Dust Samples Using Wipe Sampling Methods for Subsequent Determination of Metals
D7035 Test Method for Determination of Metals and Metalloids in Airborne Particulate Matter by Inductively Coupled Plasma
Atomic Emission Spectrometry (ICP-AES)
D7144 Practice for Collection of Surface Dust by Micro-vacuum Sampling for Subsequent Metals Determination
1
This guide is under the jurisdiction of ASTM Committee D22 on Air Quality and is the direct responsibility of Subcommittee D22.12 on Sampling and Analysis,Analysis
of Lead,Lead for Exposure and Risk Assessment.
Current edition approved March 1, 2016Sept. 1, 2020. Published April 2016September 2020. Originally approved in 1996. Last previous edition approved in 2016 as
E1775 – 07 (2016).E1775 – 16. DOI: 10.1520/E1775-16.10.1520/E1775-20.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’sstandard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
E1775 − 20
D7439 Test Method for Determination of Elements in Airborne Particulate Matter by Inductively Coupled Plasma–Mass
Spectrometry
E1583 Practice for Evaluating Laboratories Engaged in Determination of Lead in Paint, Dust, Airborne Particulates, and Soil
Taken From and Around Buildings and Related Structures
E1605 Terminology Relating to Lead in Buildings
E1613 Test Method for Determination of Lead by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES),
Flame Atomic Absorption Spectrometry (FAAS), or Graphite Furnace Atomic Absorption Spectrometry (GFAAS) Techniques
E1644 Practice for Hot Plate Digestion of Dust Wipe Samples for the Determination of Lead
E1645 Practice for Preparation of Dried Paint Samples by Hotplate or Microwave Digestion for Subsequent Lead Analysis
E1726 Practice for Preparation of Soil Samples by Hotplate Digestion for Subsequent Lead Analysis
E1728/E1728M Practice for Collection of Settled Dust Samples Using Wipe Sampling Methods for Subsequent Lead
Determination
E1727 Practice for Field Collection of Soil Samples for Subsequent Lead Determination
E1729 Practice for Field Collection of Dried Paint Samples for Subsequent Lead Determination
E1792 Specification for Wipe Sampling Materials for Lead in Surface Dust
E31
...
Questions, Comments and Discussion
Ask us and Technical Secretary will try to provide an answer. You can facilitate discussion about the standard in here.