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ASTM E1979-21

(Practice)

Standard Practice for Ultrasonic Extraction of Paint, Dust, Soil, and Air Samples for Subsequent Determination of Lead

Standard Practice for Ultrasonic Extraction of Paint, Dust, Soil, and Air Samples for Subsequent Determination of Lead

SIGNIFICANCE AND USE
5.1 Ultrasonic extraction using dilute nitric acid is a simpler and easier method for extracting lead from environmental samples than are traditional digestion methods that employ hot plate or microwave digestion with concentrated acids (3), (5), (7), (8). Hence, ultrasonic extraction may be used in lieu of the more rigorous strong acid/high temperature digestion methods (for example, see Ref (3) and Test Method E1613), provided that the performance is demonstrated using accepted criteria as delineated in Guide E1775.  
5.2 In contrast with hot plate or microwave digestion techniques, ultrasonic extraction is field-portable, which allows for on-site sample analysis.
SCOPE
1.1 This practice covers an ultrasonic extraction procedure for the extraction of lead from environmental samples of interest in lead abatement and renovation (or related) work, for analytical purposes.  
1.2 Environmental matrices of concern include dry paint films, settled dusts, soils, and air particulates.  
1.3 Samples subjected to ultrasonic extraction are prepared for subsequent determination of lead by laboratory analytical methods.  
1.4 This practice includes, where applicable, descriptions of procedures for sample homogenization and weighing prior to ultrasonic extraction.  
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
31-Oct-2021
ICS
17.140.99 - Other standards related to acoustics
71.040.50 - Physicochemical methods of analysis
Technical Committee
D22 - Air Quality
Drafting Committee
D22.12 - Sampling and Analysis of Lead for Exposure and Risk Assessment
Current Stage
Ref Project

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ASTM E1979-21 - Standard Practice for Ultrasonic Extraction of Paint, Dust, Soil, and Air Samples for Subsequent Determination of LeadASTM E1979-21 - Standard Practice for Ultrasonic Extraction of Paint, Dust, Soil, and Air Samples for Subsequent Determination of Lead
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REDLINE ASTM E1979-21 - Standard Practice for Ultrasonic Extraction of Paint, Dust, Soil, and Air Samples for Subsequent Determination of LeadREDLINE ASTM E1979-21 - Standard Practice for Ultrasonic Extraction of Paint, Dust, Soil, and Air Samples for Subsequent Determination of Lead
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Standards Content (Sample)

This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: E1979 − 21
Standard Practice for
Ultrasonic Extraction of Paint, Dust, Soil, and Air Samples
1
for Subsequent Determination of Lead
This standard is issued under the fixed designation E1979; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D5438 Practice for Collection of Floor Dust for Chemical
Analysis
1.1 This practice covers an ultrasonic extraction procedure
D6785 Test Method for Determination of Lead inWorkplace
for the extraction of lead from environmental samples of
Air Using Flame or Graphite Furnace Atomic Absorption
interest in lead abatement and renovation (or related) work, for
Spectrometry
analytical purposes.
D7144 Practice for Collection of Surface Dust by Micro-
1.2 Environmental matrices of concern include dry paint
vacuum Sampling for Subsequent Determination of Met-
films, settled dusts, soils, and air particulates.
als and Metalloids
1.3 Samples subjected to ultrasonic extraction are prepared D8358 GuideforAssessmentandInclusionofWallDeposits
in the Analysis of Single-Stage Samplers for Airborne
for subsequent determination of lead by laboratory analytical
methods. Particulate Matter
E631 Terminology of Building Constructions
1.4 This practice includes, where applicable, descriptions of
E1605 Terminology Relating to Lead in Buildings
procedures for sample homogenization and weighing prior to
E1613 Test Method for Determination of Lead by Induc-
ultrasonic extraction.
tively Coupled Plasma Atomic Emission Spectrometry
1.5 The values stated in SI units are to be regarded as
(ICP-AES), Flame Atomic Absorption Spectrometry
standard. No other units of measurement are included in this
(FAAS), or Graphite Furnace Atomic Absorption Spec-
3
standard.
trometry (GFAAS) Techniques (Withdrawn 2021)
1.6 This standard does not purport to address all of the E1726 Practice for Preparation of Soil Samples by Hotplate
safety concerns, if any, associated with its use. It is the Digestion for Subsequent Lead Analysis
responsibility of the user of this standard to establish appro- E1727 Practice for Field Collection of Soil Samples for
priate safety, health, and environmental practices and deter- Subsequent Lead Determination
mine the applicability of regulatory limitations prior to use. E1728 PracticeforCollectionofSettledDustSamplesUsing
1.7 This international standard was developed in accor- Wipe Sampling Methods for Subsequent Lead Determi-
dance with internationally recognized principles on standard- nation
ization established in the Decision on Principles for the E1729 Practice for Field Collection of Dried Paint Samples
Development of International Standards, Guides and Recom- for Subsequent Lead Determination
mendations issued by the World Trade Organization Technical E1775 Guide for Evaluating Performance of On-Site Extrac-
Barriers to Trade (TBT) Committee. tion and Field-Portable Electrochemical or Spectrophoto-
metric Analysis for Lead
2. Referenced Documents
E1792 Specification for Wipe Sampling Materials for Lead
2
in Surface Dust
2.1 ASTM Standards:
D1193 Specification for Reagent Water
3. Terminology
3.1 Definitions—For definitions of terms relating to this
1
This practice is under the jurisdiction ofASTM Committee D22 on Air Quality
practice that do not appear in this section, refer to Terminolo-
and is the direct responsibility of Subcommittee D22.12 on Sampling and Analysis
gies E631 and E1605.
of Lead for Exposure and Risk Assessment.
Current edition approved Nov. 1, 2021. Published January 2023. Formerly PS 3.1.1 extraction, n—the dissolution of target analytes from a
87–97. Originally adopted by Committee E06 in 1998. Last previous edition
solid matrix into a liquid form.
approved in 2017 as E1979 – 17. DOI: 10.1520/E1979-21.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
3
Standards volume information, refer to the standard’s Document Summary page on The last approved version of this historical standard is referenced on
the ASTM website. www.astm.org.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
E1979 − 21
3.1.1.1 Discussion—During sample digestion or extraction, 5.2 In contrast with hot plate or microwave digestion
target analytes are extracted (solubilized) into solution to te
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: E1979 − 17 E1979 − 21
Standard Practice for
Ultrasonic Extraction of Paint, Dust, Soil, and Air Samples
1
for Subsequent Determination of Lead
This standard is issued under the fixed designation E1979; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This practice covers an ultrasonic extraction procedure for the extraction of lead from environmental samples of interest in
lead abatement and renovation (or related) work, for analytical purposes.
1.2 Environmental matrices of concern include dry paint films, settled dusts, soils, and air particulates.
1.3 Samples subjected to ultrasonic extraction are prepared for subsequent determination of lead by laboratory analytical methods.
1.4 This practice includes, where applicable, descriptions of procedures for sample homogenization and weighing prior to
ultrasonic extraction.
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.6 This practicestandard does not purport to address all of the safety concerns, if any, associated with its use. It is the
responsibility of the user of this practicestandard to establish appropriate safety safety, health, and healthenvironmental practices
and determine the applicability of regulatory limitationlimitations prior to use.
1.7 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
D1193 Specification for Reagent Water
D5438 Practice for Collection of Floor Dust for Chemical Analysis
D6785 Test Method for Determination of Lead in Workplace Air Using Flame or Graphite Furnace Atomic Absorption
Spectrometry
D7144 Practice for Collection of Surface Dust by Micro-vacuum Sampling for Subsequent Determination of Metals and
Metalloids
D8358 Guide for Assessment and Inclusion of Wall Deposits in the Analysis of Single-Stage Samplers for Airborne Particulate
Matter
1
This practice is under the jurisdiction of ASTM Committee D22 on Air Quality and is the direct responsibility of Subcommittee D22.12 on Sampling and
Analysis,Analysis of Lead,Lead for Exposure and Risk Assessment.
Current edition approved March 1, 2017Nov. 1, 2021. Published March 2017January 2023. Formerly PS 87–97. Originally adopted by Committee E06 in 1998. Last
previous edition approved in 20162017 as E1979-12(2016).E1979 – 17. DOI: 10.1520/E1979-17.10.1520/E1979-21.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
E1979 − 21
E631 Terminology of Building Constructions
E1605 Terminology Relating to Lead in Buildings
E1613 Test Method for Determination of Lead by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES),
Flame Atomic Absorption Spectrometry (FAAS), or Graphite Furnace Atomic Absorption Spectrometry (GFAAS) Techniques
3
(Withdrawn 2021)
E1726 Practice for Preparation of Soil Samples by Hotplate Digestion for Subsequent Lead Analysis
E1727 Practice for Field Collection of Soil Samples for Subsequent Lead Determination
E1728 Practice for Collection of Settled Dust Samples Using Wipe Sampling Methods for Subsequent Lead Determination
E1729 Practice for Field Collection of Dried Paint Samples for Subsequent Lead Determination
E1775 Guide for Evaluating Performance of On-Site Extraction and Field-Portable Electrochemical or Spectrophotometric
Analysis for Lead
E1792 Specification for Wipe Sampling Materials for Lead in Surface Dust
3. Terminology
3.1 Definitions:Definitions For —For definitions of terms relating to this practice that do not appear in this section, refer to
Terminologies E631 and E1605.
3.1.1 extraction—extraction, n—the dissolution of target analytes from a solid matrix into a liquid form.
...

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5.1 This test method is designed to determine the temperature at which the Wet Blue or Wet White specimen experiences shrinkage. In this test method, shrinkage occurs as a result of hydrothermal denaturation of the collagen protein molecules which make up the fiber structure of the Wet Blue or Wet White. The shrinkage temperature of Wet Blue or Wet White is influenced by many different factors, most of which appear to affect the number and nature of crosslinking interactions between adjacent polypeptide chains of the collagen protein molecules. The value of the shrinkage temperature of Wet Blue or Wet White is commonly used as an indicator of the type of tannage or the degree of tannage, or both, of that particular Wet Blue or Wet White (especially for the more hydrothermally stable tannages such as chrome tannage).
SCOPE
1.1 This test method covers the determination of the shrinkage temperature of all types of Wet Blue and Wet White. The heating medium is water when the shrinkage temperature is at or below 98 °C. The heating medium is a glycerine-water solution when the shrinkage temperature is above 98 °C.  
1.2 The values stated in SI units are to be regarded as the standard. The values in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D8530/D8530M-23(Guide)
Standard Guide for the Selection and Use of Waterstops

SIGNIFICANCE AND USE
4.1 This guide is intended to be used in the selection and installation of waterstops in cast-in-place concrete construction. This guide is intended to assist the building owner, owner’s representative, architect, engineer, contractor, and/or authorized inspector during the specification and installation of waterstops.  
4.2 This guide is applicable to cast-in-place concrete construction. The use of this guide may not be appropriate for installation of waterstops in other types of concrete construction, including but not limited to, pneumatically applied (that is, shotcrete) and precast concrete construction.
SCOPE
1.1 This guide covers the use of waterstops within cast-in-place concrete construction. Waterstops are generally placed within static, non-moving construction joints in concrete to close off the joint to water, which may be under significant hydrostatic pressure. They are used as part of the overall waterproofing strategy for a building or other structure. Expansion and other types of moving joints may require the use of waterstops, which can accommodate the anticipated movement of the structure and are beyond the scope of this guide.  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents: therefore, each system shall be used independently of the other. Combining values from the two systems may result in nonconformance with the standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM E2956-23(Guide)
Standard Guide for Monitoring the Neutron Exposure of LWR Reactor Pressure Vessels

SIGNIFICANCE AND USE
4.1 Regulatory Requirements—The USA Code of Federal Regulations (10CFR Part 50, Appendix H) requires the implementation of a reactor vessel materials surveillance program for all operating LWRs. Other countries have similar regulations. The purpose of the program is to (1) monitor changes in the fracture toughness properties of ferritic materials in the reactor vessel beltline6 resulting from exposure to neutron irradiation and the thermal environment, and (2) make use of the data obtained from surveillance programs to determine the conditions under which the vessel can be operated with adequate margins of safety throughout its service life. Practice E185, derived mechanical property data, and (r, θ, z) physics-dosimetry data (derived from the calculations and reactor cavity and surveillance capsule measurements (1) using physics-dosimetry standards) can be used together with information in Guide E900 and Refs. 4, 11-18 to provide a relation between property degradation and neutron exposure, commonly called a “trend curve.” To obtain this trend curve at all points in the pressure vessel wall requires that the selected trend curve be used together with the appropriate (r, θ, z) neutron field information derived by use of this guide to accomplish the necessary interpolations and extrapolations in space and time.  
4.2 Neutron Field Characterization—The tasks required to satisfy the second part of the objective of 4.1 are complex and are summarized in Practice E853. In doing this, it is necessary to describe the neutron field at selected (r, θ, z) points within the pressure vessel wall. The description can be either time dependent or time averaged over the reactor service period of interest. This description can best be obtained by combining neutron transport calculations with plant measurements such as reactor cavity (ex-vessel) and surveillance capsule or RPV cladding (in-vessel) measurements, benchmark irradiations of dosimeter sensor materials, and knowledge of th...
SCOPE
1.1 This guide establishes the means and frequency of monitoring the neutron exposure of the LWR reactor pressure vessel throughout its operating life.  
1.2 The physics-dosimetry relationships determined from this guide may be used to estimate reactor pressure vessel damage through the application of Practice E693 and Guide E900, using fast neutron fluence (E > 1.0 MeV and E > 0.1 MeV), displacements per atom (dpa), or damage-function-correlated exposure parameters as independent exposure variables. Supporting the application of these standards are the E853, E944, E1005, and E1018 standards, identified in 2.1.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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    12 pages
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  • Guide
    12 pages
    English language
    sale 15% off