ASTM B887-03(2008)e1
(Test Method)Standard Test Method for Determination of Coercivity (Hcs) of Cemented Carbides
Standard Test Method for Determination of Coercivity (Hcs) of Cemented Carbides
SIGNIFICANCE AND USE
Measurement of coercivity provides a relative comparison of carbide grain size, binder content, and possibly carbon deficiency for a given graded carbide material or product, and may be employed as a non-destructive measurement indicating deviation from a specified norm.
This test method allows the non-destructive estimate of average carbide grain size in sintered cemented carbide hardmetals. It is appropriate for a wide range of compositions and tungsten carbide (WC) WC grain sizes, and can be used for acceptance of material or product to specification.
SCOPE
1.1 This test method covers the determination of magnetization coercivity (Hcs) of cemented carbide materials and products using coercive force instrumentation. It is patterned after ISO 3326.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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Designation: B887 − 03(Reapproved 2008)
Standard Test Method for
Determination of Coercivity (Hcs) of Cemented Carbides
This standard is issued under the fixed designation B887; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
´ NOTE—The units statement in subsection 1.2 was corrected editorially in April 2008.
1. Scope 4. Summary of Test Method
1.1 This test method covers the determination of magneti-
4.1 A test sample is positioned in the dc magnetic field of
zation coercivity (Hcs) of cemented carbide materials and
the test apparatus and magnetized to technical saturation. The
products using coercive force instrumentation. It is patterned
magnetic field polarity is then reversed and the test sample is
after ISO 3326.
demagnetized by increasing the energy of the reversed mag-
netic field until the test sample reaches zero magnetism. The
1.2 The values stated in SI units are to be regarded as
coercive force (Hc) is the magnetizing force required to return
standard. No other units of measurement are included in this
the saturated magnetic induction to zero.
standard.
1.3 This standard does not purport to address all of the
5. Significance and Use
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appro-
5.1 Measurement of coercivity provides a relative compari-
priate safety and health practices and determine the applica- son of carbide grain size, binder content, and possibly carbon
bility of regulatory limitations prior to use.
deficiency for a given graded carbide material or product, and
may be employed as a non-destructive measurement indicating
2. Referenced Documents deviation from a specified norm.
2.1 ASTM Standards:
5.2 This test method allows the non-destructive estimate of
A340 Terminology of Symbols and Definitions Relating to
average carbide grain size in sintered cemented carbide hard-
Magnetic Testing
metals. It is appropriate for a wide range of compositions and
B243 Terminology of Powder Metallurgy
tungsten carbide (WC) WC grain sizes, and can be used for
acceptance of material or product to specification.
2.2 ISO Standard:Available from American National Stan-
dards Institute (ANSI), 25 W. 43rd St., 4th Floor, New York, NY
6. Interferences
10036, http://www.ansi.org.
ISO 3326 Hardmetals - Determination of (the Magnetiza-
6.1 Hcs measurement is a non-destructive “bulk” measure-
tion) Coercivity
ment that is averaged over the specimen volume. Bi-modal
grain size distributions will give approximately the same Hc
3. Terminology
value as would be obtained from a normal grain size distribu-
tion about the same mean value.
3.1 Definitions:
3.1.1 For definition of terms used in this procedure refer to
6.2 Large test specimens must be sized to fit within the
Terminology A340 and Terminology B243.
magnetic field coil spacing available for the apparatus em-
3.1.2 dc—direct current.
ployed.
6.3 Small test specimens may be immeasurable if their size
prohibits detection by the magnetic field coils for the apparatus
This test method is under the jurisdiction of ASTM Committee B09 on Metal
employed.
Powders and Metal Powder Products and is the direct responsibility of Subcom-
mittee B09.06 on Cemented Carbides.
6.4 Specimen shape, that is, symmetry and aspect ratio,
Current edition approved April 1, 2008. Published April 2008. Originally
influence Hc measurement values and repeatability of results.
approved in 1998. Last previous edition approved in 2003 as B887–03. DOI:
10.1520/B0887-03R08E01.
Test specimens should be positioned with their long axis in the
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
direction of the magnetic field. Asymmetrically shaped test
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
specimens should be tested in several positions, the
...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
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Designation:B887–98 Designation:B887–03 (Reapproved 2008)
Standard Test Method for
Determination of Coercivity (Hcs) of Cemented Carbides
This standard is issued under the fixed designation B 887; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
e NOTE—The units statement in subsection 1.2 was corrected editorially in April 2008.
1. Scope
1.1 This test method covers the determination of magnetization coercivity (Hcs) of cemented carbide materials and products
using coercive force instrumentation. It is patterned after ISO 3326.
1.2
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2.1 ASTM Standards:
A 340Terminology of Symbols and Definitions Relating to Magnetic Testing Specification for Reagent Water
B 243Terminology of Powder Metallurgy Specification for Reagent Water
2.2 ISO Standard:
ISO 3326 Hardmetals - Determination of (the Magnetization) Coercivity
3. Terminology
3.1 Definitions:
3.1.1 For definition of terms used in this procedure refer to Terminology A 340 and Terminology B 243.
3.1.2 dc—direct current —direct current.
4. Summary of Test Method
4.1 A test sample is positioned in the dc magnetic field of the test apparatus and magnetized to technical saturation. The
magnetic field polarity is then reversed and the test sample is demagnetized by increasing the energy of the reversed magnetic field
until the test sample reaches zero magnetism. The coercive force (Hc) is the magnetizing force required to return the saturated
magnetic induction to zero.
5. Significance and Use
5.1 Measurement of coercivity provides a relative comparison of carbide grain size, binder content, and possibly carbon
deficiency for a given graded carbide material or product, and may be employed as a non-destructive measurement indicating
deviation from a specified norm.
5.2 This test method allows the non-destructive estimate of average carbide grain size in sintered cemented carbide hardmetals.
It is appropriate for a wide range of compositions and tungsten carbide (WC) WC grain sizes, and can be used for acceptance of
material or product to specification.
ThistestmethodisunderthejurisdictionofASTMCommitteeB-9onMetalPowdersandMetalPowderProductsandisthedirectresponsibilityofSubcommitteeB09.06
on Cemented Carbides.
Current edition approved May 10, 1998. Published November 1998.
This test method is under the jurisdiction of ASTM Committee B09 on Metal Powders and Metal Powder Products and is the direct responsibility of Subcommittee
B09.06 on Cemented Carbides.
Current edition approved April 1, 2008. Published April 2008. Originally approved in 1998. Last previous edition approved in 2003 as B 887–03.
For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
, Vol 03.04.volume information, refer to the standard’s Document Summary page on the ASTM website.
Annual Book of ASTM Standards, Vol 02.05.
Available from American National Standards Institute (ANSI), 25 W. 43rd St., 4th Floor, New York, NY 10036, http://www.ansi.org.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
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B887–03 (2008)
6. Interferences
6.1 Hcs measurement is a non-destructive “bulk” measurement that is averaged over the specimen volume. Bi-modal grain size
distributions will give approximately the same Hc value as would be obtained from a normal grain size distribution about the same
mean value.
6.2 Large test specimens m
...
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