Standard Specification for Expanded or Exfoliated Vermiculite Thermal Insulating Cement

ABSTRACT
This specification covers expanded or exfoliated vermiculite thermal insulating material in the form of dry cement or plaster, intended to be mixed with a suitable proportion of water, applied as a plastic mass, and dried in place, for use as insulation on surfaces. The cement shall be composed predominantly of expanded or exfoliated vermiculite, with a suitable proportion of heat-resistant binder. The following requirements are employed for purposes of initial material or product qualification: consistency, compressive strength, linear shrinkage, apparent thermal conductivity, and dry adhesion to steel. The consistency of the material, dry converting capacity and volume change upon drying, compressive strength, linear shrinkage, apparent thermal conductivity, and dry adhesion to steel shall be tested to meet the requirements prescribed.
SCOPE
1.1 This specification covers expanded or exfoliated vermiculite thermal insulating material in the form of dry cement or plaster, intended to be mixed with a suitable proportion of water, applied as a plastic mass, and dried in place, for use as insulation on surfaces operating at temperatures between 100°F (38°C) and 1800°F (982°C). The cement shall not be used where it will be exposed to combustion conditions, such as the hot face lining of a furnace.  
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.3 The following safety hazards caveat pertains only to the test method portion, Section 10, of this specification. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 When the installation or use of thermal insulation materials, accessories and systems, may pose safety or health problems, the manufacturer shall provide the user with appropriate current information regarding any known problems associated with the recommended use of the company’s products. The manufacturer shall also recommend protective measures to be employed in the safe utilization of said products.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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31-Mar-2019
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ASTM C196-00(2019) - Standard Specification for Expanded or Exfoliated Vermiculite Thermal Insulating Cement
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: C196 −00 (Reapproved 2019)
Standard Specification for
Expanded or Exfoliated Vermiculite Thermal Insulating
Cement
This standard is issued under the fixed designation C196; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope 2. Referenced Documents
2.1 ASTM Standards:
1.1 This specification covers expanded or exfoliated ver-
miculite thermal insulating material in the form of dry cement C163 Practice for Mixing Thermal Insulating Cement
Samples
or plaster, intended to be mixed with a suitable proportion of
water, applied as a plastic mass, and dried in place, for use as C166 Test Method for Covering Capacity and Volume
Change Upon Drying of Thermal Insulating Cement
insulation on surfaces operating at temperatures between
100°F (38°C) and 1800°F (982°C). The cement shall not be C168 Terminology Relating to Thermal Insulation
used where it will be exposed to combustion conditions, such C177 Test Method for Steady-State Heat Flux Measure-
as the hot face lining of a furnace. ments and Thermal Transmission Properties by Means of
the Guarded-Hot-Plate Apparatus
1.2 The values stated in inch-pound units are to be regarded
C353 Test Method forAdhesion of DriedThermal Insulating
as standard. The values given in parentheses are mathematical
or Finishing Cement (Withdrawn 2002)
conversions to SI units that are provided for information only
C354 Test Method for Compressive Strength of Thermal
and are not considered standard.
Insulating or Finishing Cement (Withdrawn 2002)
1.3 The following safety hazards caveat pertains only to the
C356 Test Method for Linear Shrinkage of Preformed High-
test method portion, Section 10, of this specification. This
Temperature Thermal Insulation Subjected to Soaking
standard does not purport to address all of the safety concerns,
Heat
if any, associated with its use. It is the responsibility of the user
C390 Practice for Sampling and Acceptance of Thermal
of this standard to establish appropriate safety, health, and
Insulation Lots
environmental practices and determine the applicability of
C405 Practice for Estimating Consistency of Wet-Mixed
regulatory limitations prior to use.
Thermal Insulating Cement (Withdrawn 2006)
1.4 When the installation or use of thermal insulation
C518 Test Method for Steady-State Thermal Transmission
materials, accessories and systems, may pose safety or health
Properties by Means of the Heat Flow Meter Apparatus
problems, the manufacturer shall provide the user with appro-
C1058 Practice for Selecting Temperatures for Evaluating
priate current information regarding any known problems
and Reporting Thermal Properties of Thermal Insulation
associated with the recommended use of the company’s prod-
ucts. The manufacturer shall also recommend protective mea-
3. Terminology
sures to be employed in the safe utilization of said products.
3.1 Definitions:
1.5 This international standard was developed in accor-
3.2 Terminology C168 shall be considered as applying to
dance with internationally recognized principles on standard-
the terms used in this specification.
ization established in the Decision on Principles for the
Development of International Standards, Guides and Recom-
4. Materials and Manufacture
mendations issued by the World Trade Organization Technical
4.1 The cement shall be composed predominantly of ex-
Barriers to Trade (TBT) Committee.
panded or exfoliated vermiculite, with a suitable proportion of
1 2
This specification is under the jurisdiction of ASTM Committee C16 on For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Thermal Insulation and is the direct responsibility of Subcommittee C16.20 on contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Homogeneous Inorganic Thermal Insulations. Standards volume information, refer to the standard’s Document Summary page on
Current edition approved April 1, 2019. Published May 2019. Originally the ASTM website.
approved in 1944. Last previous edition approved in 2016 as C196 – 00 (2016). The last approved version of this historical standard is referenced on
DOI: 10.1520/C0196-00R19. www.astm.org.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
C196 − 00 (2019)
heat-resistant binder. Asbestos shall not be used as an ingredi- sample shall be taken from the lot. Average the results of the
ent or component part of the product. retest with the results of the original test to determine compli-
ance with this specification.
5. Other Requirements
9. Specimen Preparation
5.1 The cement shall conform to the requirements given in
9.1 Mix specimens for testing in accordance with Practice
Table 1. Conformance shall be based on results of tests on
C163.
specimens first mixed with water, according to the ratio for
proper troweling consistency determined in accordance with
9.2 The amount of water to be used in preparing samples for
Section 10.
all tests shall be that amount which results in the specified
consistency, determined in accordance with Practice C405.
6. Qualification Requirements
10. Test Methods
6.1 The following requirements are employed for purposes
10.1 Consistency— Practice C405.
of initial material or product qualification:
6.1.1 Consistency,
10.2 Dry Covering Capacity—Test Method C166.
6.1.2 Compressive strength,
10.3 Volume Change upon Drying—Test Method C166.
6.1.3 Linear shrinkage,
10.4 Compressive Strength—Test Method C354.
6.1.4 Apparent thermal conductivity, and
6.1.5 Dry adhesion to steel.
10.5 Linear Shrinkage— Test Method C356.
10.6 Apparent Thermal Conductivity—Test Method C177 or
7. Sampling
Test Method C518, except prepare the test specimens as
7.1 The cement shall be sampled, for the purpose of tests
follows:
using one of the following procedures.
10.6.1 Mold test specimens in a
...

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