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ASTM D4339-01(2007)

(Test Method)

Standard Test Method for Determination of the Odor of Adhesives

Standard Test Method for Determination of the Odor of Adhesives

SIGNIFICANCE AND USE
The results from this determination are useful in determining the suitability of adhesives in applications where the odor level associated with the end use is critical.
SCOPE
1.1 This test method describes a procedure for evaluating the odor of adhesives. It is intended to replace Federal Standard 175A, Method 4051.
1.2 This test method provides a means of comparing the odor of an adhesive sample to a reference sample. It is not intended to give an absolute value for the odor of a sample. It can be used for wet or dry samples.
1.3 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.
Note 1—Warning: Do not use this test method with adhesives containing hazardous components such as solvent residues and unreacted monomeric materials.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See Note 1 for specific precautionary statements.

General Information

Status
Historical
Publication Date
30-Apr-2007
ICS
83.180 - Adhesives
Technical Committee
D14 - Adhesives
Drafting Committee
D14.10 - Working Properties
Current Stage
Ref Project

Relations

Replaces
ASTM D4339-01 - Standard Test Method for Determination of the Odor of Adhesives
Effective Date
01-May-2007
Replaced By
ASTM D4339-01(2013) - Standard Test Method for Determination of the Odor of Adhesives
Effective Date
01-Oct-2013
Referred By
ASTM C647-19 - Standard Guide to Properties and Tests of Mastics and Coating Finishes for Thermal Insulation
Effective Date
01-May-2007
Referred By
ASTM D6465-99(2016) - Standard Guide for Selecting Aerospace and General Purpose Adhesives and Sealants
Effective Date
01-May-2007

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ASTM D4339-01(2007) - Standard Test Method for Determination of the Odor of Adhesives
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D4339 − 01 (Reapproved2007)
Standard Test Method for
Determination of the Odor of Adhesives
This standard is issued under the fixed designation D4339; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope 3.2 Definitions of Terms Specific to This Standard:
3.2.1 odor, n—that property of a substance which affects the
1.1 This test method describes a procedure for evaluating
sense of smell.
the odor of adhesives. It is intended to replace Federal
Standard 175A, Method 4051.
4. Significance and Use
1.2 This test method provides a means of comparing the
4.1 The results from this determination are useful in deter-
odor of an adhesive sample to a reference sample. It is not
mining the suitability of adhesives in applications where the
intended to give an absolute value for the odor of a sample. It
odor level associated with the end use is critical.
can be used for wet or dry samples.
5. Apparatus
1.3 The values stated in inch-pound units are to be regarded
as the standard. The values given in parentheses are for
5.1 Glass Bottles, 1-qt (1-L), wide-mouth, straight sided,
information only.
with screw caps.
NOTE 1—Warning: Do not use this test method with adhesives
NOTE 2—It is important that the bottles and caps be kept clean and
containing hazardous components such as solvent residues and unreacted
odor-free. Discard any bottle which cannot be made visibly clean or
monomeric materials.
odor-free. Wash bottles and caps with a suitable cleaning powder, rinse
thoroughly with tap water, then rinse with distilled water, drain, and dry
1.4 This standard does not purport to address all of the
in an oven. Do all cleaning in an odor-free atmosphere.
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appro- 5.2 Oven or Incubator, for aging samples at elevated tem-
priate safety and health practices and determine the applica- peratures.
bility of regulatory limitations prior to use. See Note 1 for
5.3 Aluminum Foil.
specific precautionary statements.
5.4 Balance, capable of measuring to nearest 0.1 g.
2. Referenced Documents
6. Test Sample and Test Specimen
2.1 ASTM Standards:
6.1 Select a test sample representative of the adhesive being
D907 Terminology of Adhesives
tested. It may be liquid or solid. Keep in a tightly closed
D1391 Method for Measurement of Odor in Atmospheres
3 container until used (5.1).
(Dilution Method) (Withdrawn 1986)
6.2 For the test specimen, place 20.0 6 0.1 g of the test
3. Terminology
sample into the glass bottle (5.1), cover with aluminum foil,
place the cap on the bottle and tighten.
3.1 Definitions—Several terms in this test method are de-
fined in accordance with Terminology D907.
NOTE 3—Always use new aluminum foil, never reuse it.
7. Reference Sample and Reference Specimen
This test method is under the jurisdiction of ASTM Committee D14 on
7.1 Select a reference sample, that from prior experience or
Adhesives and is the direct responsibility of Subcommittee D14.10 on Working
Properties.
knowledge,orbyagreementbetweensupplierandpurchaserof
Current edition approved May 1, 2007. Published May 2007. Originally
adhesive, has acceptable odor.
approved in 1984. Last previous edition approved in 2001 as D4339 – 01. DOI:
7.1.1 Store the reference sample in a tightly closed
10.1520/D4339-01R07.
container, specified in 5.1, in a reasonably odor-free atmo-
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
sphere.
Standards volume information, refer to the standard’s Document Summary page on
7.1.2 Take care against contamination of the reference
the ASTM website.
sample. If it is suspected that the reference sample has been
The last approved version of this historical standard is referenced on
www.astm.org. contaminated, discard it and obtain a new reference sample.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
D4339 − 01 (2007)
7.2 For the reference specimen, transfer 20.0 6 0.1 g of the 10.4 Observe the following conditions when conducting the
reference sample into the glass bottle (5.1), cover with alumi- tests:
num foil, place the cap on the bottle, and tighten.
10.4.1 Allpan
...

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SCOPE
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SCOPE
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This specification provides the means to measure and evaluate the performance of adhesives for structural or semistructural bonding of wood-to-wood in manufactured homes. Wood as used in this specification includes lumber, plywood, particleboard, gypsum board, and all materials having woodbased surfaces at the bondline. The adhesives can be classified according to resistance to deformation: Group A or structural, and Group B or semistructural. Also, the adhesives may be designated into three types, according to their recommended use based on their resistance to water and water vapor: Type 1 for interior and exterior use, Type 2 for weather-protected interior use, and Type 3 for interior use only. Different tests shall be performed in order to determine the following properties of adhesives: shear strength, gap-filling ability, total deformation resistance, moisture and temperature limitation during fabrication, high-temperature resistance, low-temperature resistance, moisture resistance, aging, oxidation resistance, and mold resistance.
SCOPE
1.1 This specification provides the means to measure and evaluate the performance of adhesives for structural or semi-structural bonding of wood-to-wood in manufactured homes. Wood as used in this specification includes lumber, plywood, particleboard, gypsum board, and all materials having wood-based surfaces at the bondline. This specification does not cover other adhesives used in manufactured homes such as adhesives for carpet, floor tile, ceramic fixtures, plastic laminates, trim and millwork, and similar nonstructural applications.  
1.1.1 The performance of the adhesives is measured in the following tests:    
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ASTM D907-15(2023)(Terminology)
Standard Terminology of Adhesives

SCOPE
1.1 This terminology standard is a compilation of definitions used in the science and technology of the adhesives industry. Terms that are generally understood or adequately defined in other readily available sources are not included.  
1.2 Any changes in this standard since 1988 are documented as follows:  
1.2.1 Appendix X1 gives a history of revisions made since 1988. Table X1.1 lists the terms that are affected as: (1) Terms Added, (2) Terms Revised, and (3) Terms Deleted.
1.2.1.1 In Table X1.1, the year of publication in Volume 15.06 is shown in parentheses following the term.  
1.2.2 In the text of the standard, the year of publication is shown following each definition. Also, the following codes are included after the year of publication to describe the type change that was made: (A) Addition, (R) Revision, or (E) Edited.  
1.2.3 Deletions are shown in Appendix X1, suitably footnoted. The deleted terms do not appear in the text of the standard.  
1.2.4 Any special circumstances not covered by 1.2.2 and 1.2.3 are documented in Table X1.1, suitably footnoted.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Standard Test Method for Resistance to Creep of Adhesives in Static Shear by Compression Loading (Wood-to-Wood)

SIGNIFICANCE AND USE
5.1 This test method evaluates the performance of the adhesive in laminated wood as measured by resistance to creep under static load.  
5.2 Test results from the evaluation of adhesive creep resistance, under designated environmental conditions of the test, provide a measure of the adhesive’s ability to withstand constant loading over a relatively long period of time.  
5.3 Creep measured with this test method is normally used in conjunction with specifications such as, but not limited to Specification D2559 and CSA O112.9 to confirm suitability of an adhesive to resist creep under designed loads when subjected to specific levels of stress, load duration and environmental conditions.
SCOPE
1.1 This test method covers the determination of creep properties of structural adhesives in wood-to-wood bonds when a standardized specimen is subjected to shearing stresses at various levels of static load, constant temperature, and relative humidity. Apparatus and procedures are provided for shear deformation (creep) of adhesive bonds under static load. This test method is used under the indicated conditions to evaluate resistance to creep properties of a structural wood adhesive.  
1.2 The test method is used to evaluate creep performance of adhesives suitable for the bonding of wood, including treated wood, into structural wood products for general construction, marine use, or for other uses where a high-strength general construction, creep-resistant, durable adhesive bond is required. Individual block shear specimens are prepared from adhesively bonded laminations, subjected to a constant load under various combinations of temperature and relative humidity, and the amount of creep measured.  
1.3 Creep of structural wood adhesives as measured by this test method may not be comparative to other ASTM methods and is limited to the conditions of the test and procedures contained herein.  
1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
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Standard Guide for Classifying and Specifying Adhesives

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4.1 The purpose of this classification system is to provide a method of identifying adhesives in order to give industry a system that can be used universally for materials. It further provides a means for specifying these materials by the use of the standards that are developed using this guide.  
4.2 This classification system was developed to permit the addition of future adhesives.
SCOPE
1.1 This guide provides a classification system for tabulating the properties of adhesives suitable for holding parts or assemblies together. The use of this guide also provides information necessary for the development of standard specifications for adhesives.  
Note 1: This classification system may serve many of the needs of industries using adhesives. This guide is subject to revision as the need requires; therefore, the latest revision should always be used.  
1.2 Limitations—This classification system is intended to be a means of identifying adhesives. It is not intended for the selection of materials. Material selection should be made by those having expertise in the adhesives field after careful consideration of the design and the performance required of the part, the environment to which it will be exposed, the attachment process to be employed, the inherent properties of the material not covered in this document, and the economic factors.  
1.3 This classification system is based on the premise that adhesives can be arranged into broad generic families using basic properties to arrange the materials into groups, classes, and grades.  
1.4 In all cases where the provisions of this classification system would conflict with the referenced ASTM specification for a particular material, the latter shall take precedence.  
1.5 The values stated in SI units, as detailed in IEEE/ASTM SI 10, are to be regarded as the standard.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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