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ASTM C87-04

(Test Method)

Standard Test Method for Effect of Organic Impurities in Fine Aggregate on Strength of Mortar

Standard Test Method for Effect of Organic Impurities in Fine Aggregate on Strength of Mortar

SCOPE
1.1 This test method covers the determination of the effect on mortar strength of the organic impurities in fine aggregate, whose presence is indicated using Test Method C 40. Comparison is made between compressive strengths of mortar made with washed and unwashed fine aggregate.
1.2 The SI values shown are to be regarded as the standard. The inch-pound values shown in parentheses are provided for information purposes only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.(Warning—Fresh hydraulic cementitous mixtures are caustic and may cause chemical burns to exposed skin and tissue upon prolonged exposure.)

General Information

Status
Historical
Publication Date
31-Jul-2004
ICS
91.100.10 - Cement. Gypsum. Lime. Mortar
Technical Committee
C09 - Concrete and Concrete Aggregates
Drafting Committee
C09.20 - Aggregates
Current Stage
Ref Project

Relations

Replaces
ASTM C87-03 - Standard Test Method for Effect of Organic Impurities in Fine Aggregate on Strength of Mortar
Effective Date
01-Aug-2004
Replaced By
ASTM C87-05 - Standard Test Method for Effect of Organic Impurities in Fine Aggregate on Strength of Mortar
Effective Date
01-Jul-2005
Referred By
ASTM C156-20 - Standard Test Method for Water Loss [from a Mortar Specimen] Through Liquid Membrane-Forming Curing Compounds for Concrete
Effective Date
01-Aug-2004

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ASTM C87-04 - Standard Test Method for Effect of Organic Impurities in Fine Aggregate on Strength of MortarASTM C87-04 - Standard Test Method for Effect of Organic Impurities in Fine Aggregate on Strength of Mortar
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ASTM C87-04 - Standard Test Method for Effect of Organic Impurities in Fine Aggregate on Strength of Mortar
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:C87–04
Standard Test Method for
Effect of Organic Impurities in Fine Aggregate on Strength
1
of Mortar
ThisstandardisissuedunderthefixeddesignationC 87;thenumberimmediatelyfollowingthedesignationindicatestheyearoforiginal
adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.Asuperscript
epsilon (e) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope* C 230 Specification for Flow Table for Use in Tests of
Hydraulic Cement
1.1 This test method covers the determination of the effect
C 305 PracticeforMechanicalMixingofHydraulicCement
on mortar strength of the organic impurities in fine aggregate,
Pastes and Mortars of Plastic Consistency
whose presence is indicated usingTest MethodC40. Compari-
C511 Specification for Mixing Rooms, Moist Cabinets,
son is made between compressive strengths of mortar made
Moist Rooms, and Water Storage Tanks Used in the
with washed and unwashed fine aggregate.
Testing of Hydraulic Cements and Concretes
1.2 The SI values shown are to be regarded as the standard.
C 670 Practice for Preparing Precision and Bias Statements
The inch-pound values shown in parentheses are provided for
for Test Methods for Construction Materials
information purposes only.
C 702 Practice for Reducing Samples of Aggregate to
1.3 This standard does not purport to address all of the
Testing Size
safety concerns, if any, associated with its use. It is the
D75 Practice for Sampling Aggregates
responsibility of the user of this standard to establish appro-
D 3665 Practice for Random Sampling of Construction
priate safety and health practices and determine the applica-
Materials
bility of regulatory limitations prior to use.(Warning—Fresh
hydraulic cementitous mixtures are caustic and may cause
3. Significance and Use
chemical burns to exposed skin and tissue upon prolonged
2 3.1 This test method is of significance in making a final
exposure.)
determination of the acceptability of fine aggregates with
2. Referenced Documents respect to the requirements of Specification C33 concerning
3 organic impurities.
2.1 ASTM Standards:
3.2 This test method is applicable to those samples which,
C33 Specification for Concrete Aggregates
when tested in accordance with Test Method C40, have
C40 Test Method for Organic Impurities in Fine Aggre-
produced a supernatant liquid with a color darker than standard
gates for Concrete
color plate No. 3 or color solution.
C 109/C 109M Test Method for Compressive Strength of
3.3 Many specifications provide for the acceptance of fine
Hydraulic Cement Mortars (Using 2-in. or [50-mm] Cube
aggregate producing a darker color in the Test Method C40
Specimens)
test, when testing by this test method indicates the strength of
C 128 Test Method for Density, Relative Density, (Specific
the mortar cubes prepared with the unwashed fine aggregate is
Gravity), and Absorption of Fine Aggregate
comparable to the strength of mortar cubes made with the
C 150 Specification for Portland Cement
washed fine aggregate.
4. Summary of Test Method
1
This test method is under the jurisdiction of ASTM Committee C09 on
Concretes and Concrete Aggregates and is the direct responsibility of Subcommit- 4.1 A portion of the fine aggregate that produced a color
tee C09.20 on Normal Weight Aggregates.
darker than the standard inTest MethodC40 is used to prepare
Current edition approved Aug. 1, 2004. Published December 2004. Originally
mortar cube specimens. A separate portion of the same fine
approved in 1931. Last previous edition approved in 2003 as C 87 – 03.
2
aggregate is washed in sodium hydroxide solution to remove
See section on Safety Precautions, Manual of Aggregate and Concrete Testing,
Annual Book of ASTM Standards, Vol 04.02.
the organic impurities that caused the failing result when tested
3
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
in accordance with Test Method C40, and that washed fine
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
aggregate is used to prepare another set of mortar cube
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. specimens.
*A Summary of Changes section appears at the end of this standard.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
C87–04
4.2 After curing for a stated period, the compressive 7.4.2 Establishing a Standard for Thoroughness of
strengths of the two sets of cube specimens are determined and Rinsing—Place a small amount of the water to be used for
compared. washing and rinsing in a clean, clear container, and det
...

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4.1 The results of mortar mixture tests can be suitable for comparing the relative performance of combinations of concrete-making materials such as fine aggregate, chemical admixtures, supplementary cementitious materials (SCMs), water, and hydraulic cement. Furthermore, this guide can be useful to identify unexpected performances due to combination of various materials. The relative trends in performance observed with the mortar method may suggest relative performance in concrete mixtures batched with the same materials and relative mixture proportions.  
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1.1 This guide provides information on how to compare the relative performance and potential incompatibility of combinations of concrete-making materials. Performance tests on fresh and early-age properties of mortar mixtures can be useful indicators of concrete performance using similar materials. The performance tests described in this guide include mortar-slump, mortar spread, mortar-workability retention, early stiffening of mortar, time of setting, air entrainment, and hydration kinetics.  
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SCOPE
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This specification covers the production, properties, packaging, and testing of packaged, dry, combined materials for concrete and mortars. Concrete mixtures covered by this specification includes high-early strength concrete, normal strength concrete, normal weight concrete, high-strength mortar, and mortars for unit masonry. The purchaser shall specify the material desired as concrete, high strength mortar, or mortar for use with unit masonry, and the respective physical requirements. Materials used as ingredients in packaged, dry, combined materials for mortar and concrete shall be composed of aggregates, air-entraining admixtures, blended cement, chemical admixtures, fly ash, ground granulated blast-furnace slag, hydrated lime, latex and powder polymer modifiers, masonry cement, mortar cement, Portland cement, and silica fume. All aggregates shall be dried, without disintegration, to specific moisture content The proportions of cementitious material and aggregate shall be such that the strength requirements will be met. Packaged, dry, combined materials for concrete, high strength mortar and mortar for use with unit masonry shall conform to the respective compressive strength requirements. Scales conforming to the standards will be used for sampling concretes from a single batch using a sufficient quantity. A slump test will be performed to check if additional water is required. In sampling mortar, the contents of an entire package of dry, combined material for mortar for unit masonry or for concrete mortar shall be used. Mortar mixing equipment, which must be provided with a bowl positioning adapter, shall be used to ensure clearance for the largest size aggregate in the mix being tested. The specification includes the following testing methods for mortar: compressive strength, density and yield, air content, and water retention.
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1.1 This specification covers the production, properties, packaging, and testing of packaged, dry, combined materials for concrete and high strength mortar. The classifications of concrete and mortar covered are defined in Section 3.
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Standard Test Method for Effect of Organic Impurities in Fine Aggregate on Strength of Mortar

SIGNIFICANCE AND USE
5.1 This test method is of significance in making a final determination of the acceptability of fine aggregates with respect to the requirements of Specification C33/C33M concerning organic impurities.  
5.2 This test method is applicable to those samples which, when tested in accordance with Test MethodC40/C40M, have produced a supernatant liquid with a color darker than the standard listed in Table 1 of C40/C40M (Organic plate No. 3, Gardner Color Standard No. 14, Circular Disk No. 14 or prepared color solution).  
5.3 Many specifications provide for the acceptance of fine aggregate producing a darker color in the Test Method C40/C40M test, if testing by this test method indicates the strength of the mortar cubes prepared with the unwashed fine aggregate is comparable to the strength of mortar cubes made with the washed fine aggregate.
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1.1 This test method covers the determination of the effect on mortar strength of the organic impurities in fine aggregate, whose presence is indicated using Test Method C40/C40M. Comparison is made between compressive strengths of mortar made with washed and unwashed fine aggregate.  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. Some values have only SI units because the inch-pound equivalents are not used in the practice.
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1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.(Warning—Fresh hydraulic cementitous mixtures are caustic and may cause chemical burns to exposed skin and tissue upon prolonged exposure.)2  
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Standard Practice for Measuring Hydration Kinetics of Hydraulic Cementitious Mixtures Using Isothermal Calorimetry

SIGNIFICANCE AND USE
5.1 Thermal power curves are used to evaluate the isothermal hydration kinetics of the combined mixture of different materials during the early period after being mixed with water. These isothermal power curves, or hydration profiles, may provide indications relative to setting characteristics, compatibility of different materials, sulfate balance and early strength development. The isothermal hydration profiles can also be used to evaluate the effects of compositions, proportions, and time of addition of materials as well as curing temperature. Special care must be used in evaluating extended retardation with paste specimens, which have been shown to overestimate the retardation of some mixtures containing cement, SCM, and admixtures.  
5.2 This procedure can be used to measure the effect of chemical admixtures on the cement hydration profile. In many cases, the addition of chemical admixture changes the kinetics of cement hydration.  
5.3 Although this technique has been used historically to understand issues related to setting and slump loss, it must be emphasized that isothermal calorimetry results cannot predict concrete performance definitely, either positively or negatively. Extensive verification in concrete at planned dosages and temperatures, and at higher dosages, is needed. Isothermal calorimetry is an effective tool to identify sensitivities, so that concrete testing can be efficiently planned and performed.  
5.4 This practice provides a means of assessing the relative hydration performance of various test mixtures compared with control mixtures that are prepared in a similar manner.  
5.5 The procedure and apparatus can be used to monitor the thermal power from pastes and mortars alone or in combination with chemical admixtures.  
5.6 The isothermal calorimeter described here can be used to measure the thermal power and heat of hydration of mortars prepared independently or obtained by wet sieving from concrete in accordance with Practice C172/C1...
SCOPE
1.1 This practice describes the apparatus and procedure for measuring relative differences in hydration kinetics of hydraulic cementitious mixtures, either in paste or mortar (see Note 1), including those containing admixtures, various supplementary cementitious materials (SCM), and other fine materials by measuring the thermal power using an isothermal calorimeter.
Note 1: Paste specimens are often preferred for mechanistic research when details of individual reaction peaks are important or for particular calorimetry configurations. Mortar specimens may give results that have better correlation with concrete setting and early strength development and are often preferred to evaluate different mixture proportions for concrete. Both paste and mortar studies have been found to be effective in evaluating concrete field problems due to incompatibility of materials used in concrete mixtures.  
1.2 This practice does not cover the measurement of heat of hydration. Heat of hydration can be determined according to Test Method C1702.  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. (Warning—Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure.2)  
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SIGNIFICANCE AND USE
4.1 Supplementary cementitious materials (SCM) covered under existing ASTM specifications are fly ash, slag cement, raw and calcined natural pozzolans including calcined clays, silica fume, and ground-glass pozzolan. The use of these materials, and limits established in existing specifications, are based on data obtained from research programs, field testing, and long term performance monitoring. Performance of SCM in specific concrete mixtures is commonly verified through preconstruction testing. This guide provides an approach to assessing the properties of materials that are not covered under existing specifications, and for assessing the performance of those materials in concrete.  
4.2 If an ASCM does not yet have a significant record of performance in concrete, a comprehensive evaluation based on this Guide should be undertaken, and it should be recognized that this ASCM might be introduced for a specific project or into a limited marketplace to initially demonstrate its performance. The user should bear in mind the intended end use of the ASCM and use appropriate test methods to establish its suitability. An ASCM that demonstrates good performance through a comprehensive evaluation as outlined in this guide could then be considered to have access to broader markets and could be considered for inclusion in an ASTM standard for SCM. For this reason, the test program to demonstrate acceptable performance should include concrete mixtures with a range of characteristics specific to the ASCM’s intended use.  
4.3 In the absence of long-term durability or acceptable field performance, prospective users are advised to apply appropriate risk management and engineering practice in the use of an ASCM.
SCOPE
1.1 This guide is intended to provide a technical approach to the evaluation of alternative supplementary cementitious materials such as pozzolans and hydraulic materials that fall outside the scope of Specifications C618, C989/C989M, C1240, and C1866/C1866M. This guide provides the initial steps for a comprehensive evaluation of an ASCM that provides due diligence for its specific intended uses in concrete; however, it does not evaluate conformance to all possible performance criteria for all types of concrete mixtures.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 Performing the tests or meeting the test limits in this guide should not imply that the material tested meets the requirements of Specifications C618, C989/C989M, C1240, and C1866/C1866M. These materials should not be represented as such and each specific source is to be evaluated separately.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Standard Practice for Evaluating Early Hydration of Hydraulic Cementitious Mixtures Using Thermal Measurements

SIGNIFICANCE AND USE
5.1 This practice provides a means of assessing the relative early hydration performance of various test mixtures compared with control mixtures that are prepared in a similar manner.  
5.2 Thermal profiles are used to evaluate the hydration behavior of hydraulic cementitious mixtures after the addition of water. They may provide indications concerning setting characteristics, compatibility of different materials, sulfate balance, relative heat of hydration, and early strength development. They can be used to evaluate the effects of compositions, proportions, and time of addition of materials as well as the initial mixture and test temperatures. Thermal profile testing is an effective tool for identifying performance sensitivities or trends, and may help to reduce the number of concrete test mixtures required to develop and qualify mixtures, especially those to be subject to variable ambient environments. It may be used by concrete producers, materials suppliers, and other practitioners to support mixture development, selection of material types or sources, optimization of proportions, or troubleshooting of field problems.  
5.3 This practice can be used to understand concrete problems related to slump loss, setting, and early strength, but results may not predict field concrete performance. Performance verification with concrete is needed to quantify the trends identified using thermal testing.  
5.4 This practice can be used to evaluate the effects of chemical admixtures on the thermal profiles of cementitious mixtures. This can be especially useful in selecting dosages appropriate for different ambient conditions.  
5.5 Thermal measurement testing as described in this practice may have similar significance and use as isothermal calorimetry described by Practice C1679 or some types of near-adiabatic calorimetry. The selection of which practice or methods to use may depend on specific applications and circumstances. The thermal profiles obtained by this practic...
SCOPE
1.1 This practice describes the apparatus and procedure for evaluating relative differences in early hydration of hydraulic cementitious mixtures such as paste, mortar, or concrete, including those containing chemical admixtures, various supplementary cementitious materials (SCMs), and other finely divided materials, by measuring the temperature history of a specimen.  
1.2 Calorimetry is the measurement of heat lost or gained during a chemical reaction such as cement hydration; calorimetric measurements as a function of time can be used to describe and evaluate hydration and related early-age property development. Calorimetry may be performed under isothermal conditions (as described in Practice C1679) or under adiabatic or semi-adiabatic conditions. This practice cannot be described as calorimetry because no attempt is made to measure or compute the heat evolved from test specimens due to hydration, but it can in many cases be used for similar evaluations. Variables that should be considered in the application of this practice are discussed in the Appendix.  
1.3 Units—The values stated in either SI units or inch-pound units shall be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system must be used independently of the other. Combining values from the two systems may result in non-conformance with the standard. Some values have only SI units because the inch-pound equivalents are not used in practice.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.
Note 1: Warning: Fresh hydraulic cementitious mixtures are caustic and may cause chemical burns to skin and tissue upon prolonged exposure.2  
1.5 This...

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ASTM
ASTM C1697-21(Specification)
Standard Specification for Blended Supplementary Cementitious Materials

SCOPE
1.1 This specification covers blended supplementary cementitious materials that result from the blending or intergrinding of two or three ASTM compliant supplementary cementitious materials, for use in concrete or mortar where hydraulic or pozzolanic action, or both, is desired. The supplementary cementitious materials include slag cement conforming to Specification C989/C989M, natural pozzolans and coal fly ash conforming to Specification C618 and silica fume conforming to Specification C1240.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
Note 1: The incorporation of supplementary cementitious materials as separate additions or as a manufactured blend may significantly alter the properties of fresh and hardened concrete. The user should be aware of these changes and is referred to the ACI Manual of Concrete Practice2 for information and guidelines. Specific reference is made to:    
ACI 232.1R  
Use of Natural Pozzolans in Concrete  
ACI 232.2R  
Use of Fly Ash in Concrete  
ACI 233R  
Slag Cement in Concrete and Mortar  
ACI 234R  
Guide for the Use of Silica Fume in Concrete  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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