ASTM D2397/D2397M-13

Standard Specification for Cationic Emulsified Asphalt

SCOPE
1.1 This specification covers seven grades of cationic emulsified asphalt for use in pavement construction in the manner designated.  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.

General Information

• Status: Historical
• Publication Date: 30-Nov-2013
• ICS: 91.100.50 - Binders. Sealing materials
• ICS: 93.080.20 - Road construction materials
• Technical Committee: D04 - Road and Paving Materials
• Drafting Committee: D04.41 - Emulsified Asphalt Specifications

Relations

• Replaces: ASTM D2397-12 - Standard Specification for Cationic Emulsified Asphalt
• Effective Date: 01-Dec-2013
• Replaced By: ASTM D2397/D2397M-17 - Standard Specification for Cationic Emulsified Asphalt
• Effective Date: 01-Jun-2017
• Referred By: ASTM D3628-15(2021) - Standard Practice for Selection and Use of Emulsified Asphalts
• Effective Date: 01-Dec-2013
• Referred By: ASTM D4215-21 - Standard Specification for Cold-Mixed, Cold-Laid Asphalt Paving Mixtures
• Effective Date: 01-Dec-2013
• Referred By: ASTM D7196-23 - Standard Test Method for Raveling Test of Cold-Mixed Emulsified Asphalt Samples
• Effective Date: 01-Dec-2013
• Referred By: ASTM D7404-19 - Standard Test Method for Determination of Emulsified Asphalt Residue by Moisture Balance Analyzer
• Effective Date: 01-Dec-2013
• Referred By: ASTM D5505-14(2020) - Standard Practice for Classifying Emulsified Recycling Agents
• Effective Date: 01-Dec-2013
• Referred By: ASTM D7226-13(2023) - Standard Test Method for Determining the Viscosity of Emulsified Asphalts Using a Rotational Paddle Viscometer
• Effective Date: 01-Dec-2013
• Referred By: ASTM D6372-23 - Standard Practice for Design, Testing, and Construction of Microsurfacing
• Effective Date: 01-Dec-2013
• Referred By: ASTM D3910-21 - Standard Practices for Design, Testing, and Construction of Slurry Seal
• Effective Date: 01-Dec-2013
• Referred By: ASTM D7497-21 - Standard Practice for Recovering Residue from Emulsified Asphalt Using Low-Temperature Evaporative Technique
• Effective Date: 01-Dec-2013
• Referred By: ASTM D1369-19 - Standard Practice for Quantities of Materials for Asphalt-Aggregate Surface Treatments
• Effective Date: 01-Dec-2013
• Referred By: ASTM D7496-18 - Standard Test Method for Viscosity of Emulsified Asphalt by Saybolt Furol Viscometer
• Effective Date: 01-Dec-2013

Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D2397/D2397M −13
Standard Specification for
1
Cationic Emulsified Asphalt
This standard is issued under the fixed designation D2397/D2397M; the number immediately following the designation indicates the
year of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last
reapproval. A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope D7402 Practice for Identifying Cationic EmulsifiedAsphalts
D7496 Test Method for Viscosity of Emulsified Asphalt by
1.1 This specification covers seven grades of cationic emul-
Saybolt Furol Viscometer
sified asphalt for use in pavement construction in the manner
D7553 Test Method for Solubility of Asphalt Materials in
designated.
N-Propyl Bromide
1.2 The values stated in either SI units or inch-pound units
are to be regarded separately as standard. The values stated in
3. Requirements
each system may not be exact equivalents; therefore, each
3.1 The emulsified asphalt shall be tested within 14 days of
system shall be used independently of the other. Combining
delivery. The emulsified asphalt shall be homogeneous after
values from the two systems may result in non-conformance
thorough mixing provided separation has not been caused by
with the standard.
freezing. Emulsions separated by freezing shall not be tested.
2. Referenced Documents
3.2 Emulsified asphalt shall conform to the requirements
2
2.1 ASTM Standards:
prescribed in Table 1 or Table 2. If no table is specified, the
D5 Test Method for Penetration of Bituminous Materials
default is Table 1.
D113 Test Method for Ductility of Bituminous Materials
D140 Practice for Sampling Bituminous Materials
4. Sampling
D244 Test Methods and Practices for Emulsified Asphalts
4.1 Samples of emulsified asphalt shall be taken in accor-
D2042 Test Method for Solubility of Asphalt Materials in
dance with Practice D140.
Trichloroethylene
D3910 Practices for Design, Testing, and Construction of
4.2 Samples shall be stored in clean, airtight sealed contain-
Slurry Seal
ers at a temperature of not less than 4°C [39.2°F] until tested.
D6930 Test Method for Settlement and Storage Stability of
Emulsified Asphalts
5. Test Methods
D6933 Test Method for Oversized Particles in Emulsified
5.1 The properties of the emulsified asphalts given in Table
Asphalts (Sieve Test)
1 or Table 2 shall be determined in accordance with the
D6935 Test Method for Determining Cement Mixing of
following ASTM test methods:
Emulsified Asphalt
5.1.1 Viscosity—Test Method D7496 for Table 1 or Test
D6936 Test Method for Determining Demulsibility of Emul-
Method D7226 for Table 2.
sified Asphalt
5.1.2 Storage Stability—Test Method D6930.
D6997 Test Method for Distillation of Emulsified Asphalt
D7226 Test Method for Determining the Viscosity of Emul-
5.1.3 Demulsibility—Test Method D6936.
sified Asphalts Using a Rotational Paddle Viscometer
5.1.4 Coating Ability and Water Resistance—Test Methods
D244.
5.1.5 Particle Charge—Test Method D7402.
1
This specification is under the jurisdiction of ASTM Committee D04 on Road
5.1.6 Sieve Test—Test Method D6933, except use distilled
and Paving Materials and is the direct responsibility of Subcommittee D04.41 on
Emulsified Asphalt Specifications. water in all wetting and washing operations in place of the
Current edition approved Dec. 1, 2013. Published January 2014. Originally
nonionic surfactant solution (1 %).
approved in 1965. Last previous edition approved in 2012 as D2397 – 12. DOI:
5.1.7 Cement Mixing—Test Method D6935.
10.1520/D2397_D2397M-13.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
5.1.8 Distillation—Test Method D6997.
contact ASTM Customer Service at [e-mail]. For Annual Book of ASTM
5.1.9 Tests on Residue from Distillation—Test Methods D5,
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. D113, D2042, and D7553.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

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D2397/D2397M−13
2
TABLE 1 Requirements for Cationic Emulsified Asphalt
Type Rapid-Setting Medium-Setting Slow-Setting Quick Setting
A
CRS-1 CRS-2 CMS-2 CMS-2h CSS-1 CSS-1h CQS-1h
Grade
min max min max min max min max min max min max min max
Test on emulsions:
Viscosity, Saybolt Furol at 25°C [77°F] SFS 20 100 20 100 20 100
Viscosity, Saybolt Furol at 50°C [122°F] SFS 20 100 100 400 50 450 50 450
B
Storage stability test, 24-h, % 11 1 1 1 1
Demulsibility, 35 mL, 0.8 % dioctyl sodium 40 . 40 .
sulfosuccinate, %
Coating ability and water resistance:
Coating, dry aggregate good good
Coating, after spraying fair
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D2397 − 12 D2397/D2397M − 13
Standard Specification for
1
Cationic Emulsified Asphalt
This standard is issued under the fixed designation D2397;D2397/D2397M; the number immediately following the designation indicates
the year of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last
reapproval. A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope
1.1 This specification covers seven grades of cationic emulsified asphalt for use in pavement construction in the manner
designated.
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each
system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the
two systems may result in non-conformance with the standard.
2. Referenced Documents
2
2.1 ASTM Standards:
D5 Test Method for Penetration of Bituminous Materials
D113 Test Method for Ductility of Bituminous Materials
D140 Practice for Sampling Bituminous Materials
D244 Test Methods and Practices for Emulsified Asphalts
D2042 Test Method for Solubility of Asphalt Materials in Trichloroethylene
D3910 Practices for Design, Testing, and Construction of Slurry Seal
D6930 Test Method for Settlement and Storage Stability of Emulsified Asphalts
D6933 Test Method for Oversized Particles in Emulsified Asphalts (Sieve Test)
D6935 Test Method for Determining Cement Mixing of Emulsified Asphalt
D6936 Test Method for Determining Demulsibility of Emulsified Asphalt
D6997 Test Method for Distillation of Emulsified Asphalt
D7226 Test Method for Determining the Viscosity of Emulsified Asphalts Using a Rotational Paddle Viscometer
D7402 Practice for Identifying Cationic Emulsified Asphalts
D7496 Test Method for Viscosity of Emulsified Asphalt by Saybolt Furol Viscometer
D7553 Test Method for Solubility of Asphalt Materials in N-Propyl Bromide
3. Requirements
3.1 The emulsified asphalt shall be tested within 14 days of delivery. The emulsified asphalt shall be homogeneous after
thorough mixing provided separation has not been caused by freezing. Emulsions separated by freezing shall not be tested.
3.2 Emulsified asphalt shall conform to the requirements prescribed in Table 1 or Table 2. If no table is specified, the default
is Table 1.
4. Sampling
4.1 Samples of emulsified asphalt shall be taken in accordance with Practice D140.
4.2 Samples shall be stored in clean, airtight sealed containers at a temperature of not less than 4°C (39.2°F)[39.2°F] until tested.
1
This specification is under the jurisdiction of ASTM Committee D04 on Road and Paving Materials and is the direct responsibility of Subcommittee D04.41 on Emulsified
Asphalt Specifications.
Current edition approved July 1, 2012Dec. 1, 2013. Published July 2012January 2014. Originally approved in 1965. Last previous edition approved in 20052012 as
D2397D2397 – 12.–05. DOI: 10.1520/D2397-12.10.1520/D2397_D2397M-13.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at [e-mail]. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D2397/D2397M − 13
2
TABLE 1 Requirements for Cationic Emulsified Asphalt
NOTE 1—CQS–1H emulsions shall meet the requirements outlined in Practices D3910.
NOTE 2—CQS-1h is used for Quick Set Slurry Seal systems.
Type Rapid-Setting Medium-Setting Slow-Setting Quick Setting
A
CRS-1 CRS-2 CMS-2 CMS-2h CSS-1 CSS-1h CQS-1HCQS-1h
Grade
min max min max min max min max min max min max min max
Test on emulsions:
Viscosity, Saybolt Furol at 25°C (77°F) SFS 20 100 20 100 20 100
Viscosity, Saybolt Furol at 25°C [77°F] SFS 20 100 20 100 20 100
Viscosity, Saybolt Furol at 50°C (122°F) SFS 20 100 100 400 50 450 50 450
Viscosity, Saybolt Furol at 50°C [122°F] SFS 20 100 100 400 50 450 50 450
A
Storage stability test, 24-h, % 1 1 1 1 1 1
B
Storage stability test, 24-h, % 1 1 1 1 1 1
Demulsibility, 35 mL, 0.8 % dioctyl sodium 40 . 40 .
sulfosuccinate, %
Coating ability and water resistance:
Coating, dry aggregate good good
Coating, after spraying fair fair
Coating, wet aggregate fair fair
Coating, after spra
...