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ASTM E367-02

(Test Method)

Standard Methods for Chemical Analysis of Ferrocolumbium

Standard Methods for Chemical Analysis of Ferrocolumbium

SCOPE
1.1 These methods cover the chemical analysis of ferrocolumbium having chemical compositions within the following limits:ElementConcentration, %Aluminum2.00 maxCarbon0.30 maxChromium2.00 maxCobalt0.25 maxNiobium40.00 to 75.00Lead0.01 maxManganese3.00 maxPhosphorus0.05 maxSilicon4.00 maxSulfur0.03 maxTantalum7.00 maxTin0.15 maxTitanium5.00 maxTungsten0.50 max
1.2 The methods appear in the following order:SectionsNiobium, Tantalum, and Titanium by theIon-Exchange Method9-30
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of whoever uses this standard to consult and establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 5.

General Information

Status
Historical
Publication Date
09-Oct-2002
ICS
77.040.30 - Chemical analysis of metals
Technical Committee
E01 - Analytical Chemistry for Metals, Ores, and Related Materials
Drafting Committee
E01.01 - Iron, Steel, and Ferroalloys
Current Stage
Ref Project

Relations

Replaces
ASTM E367-83(1997)e1 - Standard Methods for Chemical Analysis of Ferrocolumbium
Effective Date
10-Oct-2002
Replaced By
ASTM E367-03 - Standard Methods for Chemical Analysis of Ferroniobium
Effective Date
10-Jun-2003

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ASTM E367-02 - Standard Methods for Chemical Analysis of Ferrocolumbium
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NOTICE: This standard has either been superceded and replaced by a new version or discontinued.
Contact ASTM International (www.astm.org) for the latest information.
Designation: E 367 – 02
Standard Methods for
1
Chemical Analysis of Ferroniobium
This standard is issued under the fixed designation E 367; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope E 32 Practices for Sampling Ferroalloys and Steel Additives
4
for Determination of Chemical Composition
1.1 These methods cover the chemical analysis of ferro-
E 50 Practices for Apparatus, Reagents, and Safety Precau-
columbium having chemical compositions within the follow-
4
tions for Chemical Analysis of Metals
ing limits:
E 60 Practice for Photometric and Spectrophotometric
Element Concentration, %
4
Methods for Chemical Analysis of Metals
Aluminum 2.00 max
E 173 Practice for Conducting Interlaboratory Studies
Carbon 0.30 max
5
ofMethods for Chemical Analysis of Metals
Chromium 2.00 max
Cobalt 0.25 max
3. Significance and Use
Niobium 40.00 to 75.00
Lead 0.01 max
3.1 These methods for the chemical analysis of metals and
Manganese 3.00 max
alloys are primarily intended to test such materials for com-
Phosphorus 0.05 max
Silicon 4.00 max
pliance with compositional specifications. It is assumed that all
Sulfur 0.03 max
who use these methods will be trained analysts capable of
Tantalum 7.00 max
performing common laboratory procedures skillfully and
Tin 0.15 max
Titanium 5.00 max
safely. It is expected that work will be performed in a properly
Tungsten 0.50 max
equipped laboratory.
1.2 The methods appear in the following order:
4. Apparatus, Reagents, and Photometric Practice
Sections
4.1 Apparatus and reagents required for each determination
Niobium, Tantalum, and Titanium by the
are listed in separate sections preceding the procedure. The
Ion-Exchange Method 9-30
apparatus, standard solutions, and other reagents used in more
1.3 This standard does not purport to address all of the
than one procedure are referred to by number and shall
safety concerns, if any, associated with its use. It is the
conform to the requirements prescribed in Practices E 50.
responsibility of whoever uses this standard to consult and
Photometers shall conform to the requirements prescribed in
establish appropriate safety and health practices and deter-
Practice E 60.
mine the applicability of regulatory limitations prior to use.
4.2 Photometric practice prescribed in these methods shall
Specific precautionary statements are given in Section 5.
conform to Practice E 60.
2. Referenced Documents
5. Safety Precautions
2.1 ASTM Standards:
5.1 For precautions to be observed in the use of certain
2
A 550 Specification for Ferrocolumbium
reagents in these methods, refer to Practices E 50.
E 29 Practice for Using Significant Digits in Test Data to
3
Determine Conformance with Specifications 6. Sampling
6.1 For procedures for sampling the material, and for
particle size of the sample for chemical analysis, refer to
1
These methods are under the jurisdiction of ASTM Committee E01 on
Practices E 32.
Analytical Chemistry for Metals, Ores, and Related Materials and are the direct
responsibility of Subcommittee E01.01 on Iron, Steel, and Ferroalloys.
Current edition approved October 10, 2002. Published December 2002. Origi-
nally approved in 1970. Last previous edition approved in 1983 as
4
E 367 – 83 (1997). Annual Book of ASTM Standards, Vol 03.05.
2 5
Annual Book of ASTM Standards, Vol 01.02. Withdrawn from publication, see 1997 Annual Book of ASTM Standards,Vol
3
Annual Book of ASTM Standards, Vol 14.02. 03.05.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
NOTICE: This standard has either been superceded and replaced by a new version or discontinued.
Contact ASTM International (www.astm.org) for the latest information.
E367–02
6
7. Rounding Off Calculated Values length of polyvinyl tubing, and control the flow rate by a
hosecock on the polyvinyl tubing.
7.1 Calculated values shall be rounded off to the desired
12.1.1 If a number of determinations are to be made, it is
number of places as directed in 3.4 to 3.6 of Practice E 29.
convenient to arrange the columns so that they can be operated
with a minimum of attention. Plastic columns equipped with
8. Interlaboratory Studies
fittings of polystyrene have been developed for such an
8.1 These methods have been evaluated in accordance with
7
assembly. Inlet and outlet tubes are polyethylene; flexible
Practice E 173, unless otherwise noted in the precision and bias
connections, where necessary, are of polyvinyl tubing. The
section.
flow rate is controlled by hosecocks
...

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Zinc  
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Zirconium  
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5.1 This test method for the chemical analysis of metals and alloys is primarily intended to test such materials for compliance with compositional specifications. It is assumed that all who use these test methods will be trained analysts capable of performing common laboratory procedures skillfully and safely. It is expected that work will be performed in a properly equipped laboratory.
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1.3 Wrought products may be in the form of flat, pipe, tube, rod, bar, shape, or forging.  
1.4 This practice is not intended to supersede or replace existing specification requirements for the sampling of a particular material.  
1.5 The values stated in SI units are to be regarded as standard. The values in parentheses are given for information only.  
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1.1 This guide covers information for using Combustion, Inert Gas Fusion and Hot Extraction instruments to determine the mass fraction of the non-metallic elements Carbon, Sulfur, Nitrogen, Oxygen and Hydrogen in metals, ores and related materials.  
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1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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5.1 This test method is suitable for manufacturing control and for verifying that a product meets specifications. This test method provides rapid, multi-element determinations with sufficient accuracy to ensure product quality and to minimize production delays. The analytical performance data may be used as a benchmark to determine if similar X-ray spectrometers provide equivalent precision and accuracy, or if the performance of a particular X-ray spectrometer has changed.  
5.2 Calcium is sometimes added to steel to affect inclusion shape which enhances certain mechanical properties of steel. This test method is useful for determining the residual calcium in the steel after such treatment.  
5.2.1 Because calcium occurs primarily in inclusions, the precision of this test method is a function of the distribution of the calcium-bearing inclusions in the steel. The variation of determinations on freshly prepared surfaces will give some indication of the distribution of these inclusions.
SCOPE
1.1 This test method covers the wavelength dispersive X-ray fluorescence analysis of low-alloy steels for the following elements:    
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Mass Fraction
Range, %  
Calcium  
0.001 to 0.007  
Chromium  
0.04 to 2.5  
Cobalt  
0.03 to 0.2  
Copper  
0.03 to 0.6  
Manganese  
0.04 to 2.5  
Molybdenum  
0.005 to 1.5  
Nickel  
0.04 to 3.0  
Niobium  
0.002 to 0.1  
Phosphorus  
0.010 to 0.08  
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0.06 to 1.5  
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0.009 to 0.1  
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0.012 to 0.6  
1.1.1 Unless exceptions are noted, mass fraction ranges can be extended and additional elements can be included by the use of suitable reference materials and measurement conditions. Deviations from the published scope must be validated by experimental means. See Guide E2857 for information on validation options.  
1.2 The values stated in the International System of Units (SI) are to be regarded as standard. The values given in parentheses are mathematical conversions to other units that are provided for information only, because they may be used in older software and laboratory procedures.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in Section 10.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM E2209-22(Test Method)
Standard Test Method for Analysis of High Manganese Steel by Spark Atomic Emission Spectrometry

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5.1 The chemical composition of high manganese steel alloys must be determined accurately to ensure the desired metallurgical properties. This procedure is suitable for manufacturing control and inspection testing.
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1.1 This test method covers the analysis of high manganese steel by spark atomic emission spectrometry for the following elements in the ranges shown:    
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Composition Range, %  
Aluminum (Al)  
0.02 to 0.15  
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0.25 to 2.00  
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1.2 This test method may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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Standard Test Method for Analysis of Austenitic Stainless Steel by Spark Atomic Emission Spectrometry

SIGNIFICANCE AND USE
5.1 The chemical composition of stainless steels must be determined accurately to ensure the desired metallurgical properties. This test method is suitable for manufacturing control and inspection testing.
SCOPE
1.1 This test method2 covers the analysis of austenitic stainless steel by spark atomic emission spectrometry for the following elements in the ranges shown    
Element  
Composition Range, %  
Chromium  
17.0 to 23.0  
Nickel  
7.5 to 13.0  
Molybdenum  
0.01 to 3.0    
Manganese  
0.01 to 2.0    
Silicon  
0.01 to 0.90  
Copper  
0.01 to 0.30  
Carbon  
0.005 to 0.25  
Phosphorus  
0.003 to 0.15  
Sulfur  
0.003 to 0.065  
1.2 This test method is designed for the analysis of chill-cast disks or inspection testing of stainless steel samples that have a flat surface of at least 13 mm (0.5 in.) in diameter. The samples must be sufficiently massive to prevent overheating during the discharge and of a similar metallurgical condition and composition as the reference materials.  
1.3 One or more of the reference materials must closely approximate the composition of the specimen. The technique of analyzing reference materials with unknowns and performing the indicated mathematical corrections (typically referred to as type standardization) may also be used to correct for interference effects and to compensate for errors resulting from instrument drift. A variety of such systems are commonly used. Any of these that will achieve analytical accuracy equivalent to that reported for this test method are acceptable.  
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