ASTM E1775-16

Standard Guide for Evaluating Performance of On-Site Extraction and Field-Portable Electrochemical or Spectrophotometric Analysis for Lead

SIGNIFICANCE AND USE
4.1 This guide is intended for use in evaluating the performance of field-portable electroanalytical or spectrophotometric devices for lead determination, or both.  
4.2 Desired performance criteria for field-based extraction procedures are provided.  
4.3 Performance parameters of concern may be determined using protocols that are referenced in this guide.  
4.4 Example reference materials to be used in assessing the performance of field-portable lead analyzers are listed.  
4.5 Exhaustive details regarding quality assurance issues are outside the scope of this guide. Applicable quality assurance aspects are dealt with extensively in references that are cited in this guide.
SCOPE
1.1 This guide provides guidelines for determining the performance of field-portable quantitative lead analysis instruments.  
1.2 This guide applies to field-portable electroanalytical and spectrophotometric (including reflectance and colorimetric) analyzers.  
1.3 Sample matrices of concern herein include paint, dust, soil, and airborne particles.  
1.4 This guide addresses the desired performance characteristics of field-based sample extraction procedures for lead, as well as on-site extraction followed by field-portable analysis.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

• Status: Historical
• Publication Date: 29-Feb-2016
• ICS: 71.040.50 - Physicochemical methods of analysis
• Technical Committee: D22 - Air Quality
• Drafting Committee: D22.12 - Sampling and Analysis of Lead for Exposure and Risk Assessment

Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: E1775 − 16
Standard Guide for
Evaluating Performance of On-Site Extraction and Field-
Portable Electrochemical or Spectrophotometric Analysis
1
for Lead
This standard is issued under the fixed designation E1775; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope Coupled Plasma Atomic Emission Spectrometry (ICP-
AES)
1.1 This guide provides guidelines for determining the
D7144 Practice for Collection of Surface Dust by Micro-
performance of field-portable quantitative lead analysis instru-
vacuum Sampling for Subsequent Metals Determination
ments.
D7439 Test Method for Determination of Elements in Air-
1.2 This guide applies to field-portable electroanalytical and
borne Particulate Matter by Inductively Coupled Plasma-
spectrophotometric (including reflectance and colorimetric)
–Mass Spectrometry
analyzers.
E1605 Terminology Relating to Lead in Buildings
1.3 Sample matrices of concern herein include paint, dust, E1613 Test Method for Determination of Lead by Induc-
tively Coupled Plasma Atomic Emission Spectrometry
soil, and airborne particles.
(ICP-AES), Flame Atomic Absorption Spectrometry
1.4 This guide addresses the desired performance character-
(FAAS), or Graphite Furnace Atomic Absorption Spec-
istics of field-based sample extraction procedures for lead, as
trometry (GFAAS) Techniques
well as on-site extraction followed by field-portable analysis.
E1644 Practice for Hot Plate Digestion of Dust Wipe
1.5 This standard does not purport to address all of the
Samples for the Determination of Lead
safety concerns, if any, associated with its use. It is the
E1645 Practice for Preparation of Dried Paint Samples by
responsibility of the user of this standard to establish appro-
Hotplate or Microwave Digestion for Subsequent Lead
priate safety and health practices and determine the applica-
Analysis
bility of regulatory limitations prior to use.
E1726 Practice for Preparation of Soil Samples by Hotplate
Digestion for Subsequent Lead Analysis
2. Referenced Documents
E1727 Practice for Field Collection of Soil Samples for
2
2.1 ASTM Standards:
Subsequent Lead Determination
D5438 Practice for Collection of Floor Dust for Chemical
E1729 Practice for Field Collection of Dried Paint Samples
Analysis
for Subsequent Lead Determination
D6785 TestMethodforDeterminationofLeadinWorkplace
E1792 Specification for Wipe Sampling Materials for Lead
Air Using Flame or Graphite Furnace Atomic Absorption
in Surface Dust
Spectrometry
E1864 Practice for Evaluating Quality Systems of Organi-
D6966 Practice for Collection of Settled Dust Samples
zations Conducting Facility and Hazard Assessments for
Using Wipe Sampling Methods for Subsequent Determi-
Lead in Paint, Dust, Airborne Particulate, and Soil in and
nation of Metals
around Buildings and Related Structures (Withdrawn
3
D7035 Test Method for Determination of Metals and Met-
2011)
4
alloids in Airborne Particulate Matter by Inductively
2.2 U.S. EPA Documents:
EPA 600/R-93/200 Standard Operating Procedure for the
Field Analysis of Lead in Paint, Bulk Dust, and Soil by
1
This guide is under the jurisdiction of ASTM Committee D22 on Air Quality
Ultrasonic,AcidDigestionandColorimetricMeasurement
and is the direct responsibility of Subcommittee D22.12 on Sampling andAnalysis,
of Lead, for Exposure and Risk Assessment. (1993)
Current edition approved March 1, 2016. Published April 2016. Originally
approved in 1996. Last previous edition approved in 2016 as E1775 – 07 (2016).
3
DOI: 10.1520/E1775-16. The last approved version of this historical standard is referenced on
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or www.astm.org.
4
contact ASTM Customer Service at [e-mail]. For Annual Book of ASTM AvailablefromUnitedStatesEnvironmentalProtectionAgency(EPA),William
Standards volume information, refer to the standard’s Document Summary page on Jefferson Clinton Bldg., 1200 Pennsylvania Ave., NW, Washington, DC 20460,
the ASTM website. http://www.epa.gov.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
E1775 − 16
EPA 747-R-92-001 Laboratory Accreditation Guidelines: 4.5 Exhaustivedetailsregardingqualityassuranceissuesare
Measurement of Lead in Paint, Dust, and Soil (1992) outside the scope of this guide. Applicable quality assurance
5
aspects are dealt with extensively in references that are cited in
2.3 ISO Document:
this guide.
ISO Guide 30 Reference materials -- Selected terms and
definitions
5. Performan
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: E1775 − 07 (Reapproved 2016) E1775 − 16
Standard Guide for
Evaluating Performance of On-Site Extraction and Field-
Portable Electrochemical or Spectrophotometric Analysis
1
for Lead
This standard is issued under the fixed designation E1775; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This guide provides guidelines for determining the performance of field-portable quantitative lead analysis instruments.
1.2 This guide applies to field-portable electroanalytical and spectrophotometric (including reflectance and colorimetric)
analyzers.
1.3 Sample matrices of concern herein include paint, dust, soil, and airborne particles.
1.4 This guide addresses the desired performance characteristics of field-based sample extraction procedures for lead, as well
as on-site extraction followed by field-portable analysis.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
D5438 Practice for Collection of Floor Dust for Chemical Analysis
D6785 Test Method for Determination of Lead in Workplace Air Using Flame or Graphite Furnace Atomic Absorption
Spectrometry
D6966 Practice for Collection of Settled Dust Samples Using Wipe Sampling Methods for Subsequent Determination of Metals
D7035 Test Method for Determination of Metals and Metalloids in Airborne Particulate Matter by Inductively Coupled Plasma
Atomic Emission Spectrometry (ICP-AES)
D7144 Practice for Collection of Surface Dust by Micro-vacuum Sampling for Subsequent Metals Determination
D7439 Test Method for Determination of Elements in Airborne Particulate Matter by Inductively Coupled Plasma–Mass
Spectrometry
E1605 Terminology Relating to Lead in Buildings
E1613 Test Method for Determination of Lead by Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES),
Flame Atomic Absorption Spectrometry (FAAS), or Graphite Furnace Atomic Absorption Spectrometry (GFAAS) Techniques
E1644 Practice for Hot Plate Digestion of Dust Wipe Samples for the Determination of Lead
E1645 Practice for Preparation of Dried Paint Samples by Hotplate or Microwave Digestion for Subsequent Lead Analysis
E1726 Practice for Preparation of Soil Samples by Hotplate Digestion for Subsequent Lead Analysis
E1727 Practice for Field Collection of Soil Samples for Subsequent Lead Determination
E1729 Practice for Field Collection of Dried Paint Samples for Subsequent Lead Determination
E1792 Specification for Wipe Sampling Materials for Lead in Surface Dust
E1864 Practice for Evaluating Quality Systems of Organizations Conducting Facility and Hazard Assessments for Lead in Paint,
3
Dust, Airborne Particulate, and Soil in and around Buildings and Related Structures (Withdrawn 2011)
1
This guide is under the jurisdiction of ASTM Committee E06 on Performance of Buildings and is the direct responsibility of Subcommittee E06.23 on Lead Hazards
Associated with Buildings.
Current edition approved Jan. 1, 2016March 1, 2016. Published January 2016April 2016. Originally approved in 1996. Last previous edition approved in 20072016 as
E1775 – 07.E1775 – 07 (2016). DOI: 10.1520/E1775-07R16.10.1520/E1775-16.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at [e-mail]. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
3
The last approved version of this historical standard is referenced on www.astm.org.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
E1775 − 16
4
2.2 U.S. EPA Documents:
EPA 600/R-93/200 Standard Operating Procedure for the Field Analysis of Lead in Paint, Bulk Dust, and Soil by Ultrasonic,
Acid Digestion and Colorimetric Measurement (1993)
EPA 747-R-92-001 Laboratory Accreditation Guidelines: Measurement of Lead in Paint, Dust, and Soil (1992)
5
2.3 ISO Document:
ISO Guide 30 Reference materials -- Selected terms and definitions
3. Terminology
3.1 For definitio
...