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ASTM C1363-97

(Test Method)

Standard Test Method for the Thermal Performance of Building Assemblies by Means of a Hot Box Apparatus

Standard Test Method for the Thermal Performance of Building Assemblies by Means of a Hot Box Apparatus

SCOPE
1.1 This test method covers the laboratory measurement of heat transfer through a specimen under controlled air temperature, air velocity, and thermal radiation conditions established in a metering chamber on one side and in a climatic chamber on the other side.

General Information

Status
Historical
Publication Date
09-Aug-1997
ICS
91.120.10 - Thermal insulation of buildings
Technical Committee
C16 - Thermal Insulation
Drafting Committee
C16.30 - Thermal Measurement
Current Stage
Ref Project

Relations

Replaced By
ASTM C1363-05 - Standard Test Method for Thermal Performance of Building Materials and Envelope Assemblies by Means of a Hot Box Apparatus
Effective Date
01-May-2005
Referred By
ASTM E2634-18(2022) - Standard Specification for Flat Wall Insulating Concrete Form (ICF) Systems
Effective Date
10-Aug-1997
Referred By
ASTM D7793-21 - Standard Specification for Insulated Vinyl Siding
Effective Date
10-Aug-1997
Referred By
ASTM C1029-20 - Standard Specification for Spray-Applied Rigid Cellular Polyurethane Thermal Insulation
Effective Date
10-Aug-1997
Referred By
ASTM C578-22 - Standard Specification for Rigid, Cellular Polystyrene Thermal Insulation
Effective Date
10-Aug-1997
Referred By
ASTM C1825-19 - Standard Guide for Developing Specifications for Masonry Units
Effective Date
10-Aug-1997
Referred By
ASTM C1410-17(2023) - Standard Specification for Cellular Melamine Thermal and Sound-Absorbing Insulation
Effective Date
10-Aug-1997
Referred By
ASTM C687-18 - Standard Practice for Determination of Thermal Resistance of Loose-Fill Building Insulation
Effective Date
10-Aug-1997
Referred By
ASTM C1484-10(2018) - Standard Specification for Vacuum Insulation Panels
Effective Date
10-Aug-1997
Referred By
ASTM C726-17 - Standard Specification for Mineral Wool Roof Insulation Board
Effective Date
10-Aug-1997
Referred By
ASTM D7425/D7425M-13(2019) - Standard Specification for Spray Polyurethane Foam Used for Roofing Applications
Effective Date
10-Aug-1997
Referred By
ASTM C1149-23 - Standard Specification for Self-Supported Spray Applied Cellulosic Thermal Insulation
Effective Date
10-Aug-1997
Referred By
ASTM C1558-19 - Standard Guide for Development of Standard Data Records for Computerization of Thermal Transmission Test Data for Thermal Insulation
Effective Date
10-Aug-1997
Referred By
ASTM C1224-22 - Standard Specification for Reflective Insulation for Building Applications
Effective Date
10-Aug-1997
Referred By
ASTM C1289-23 - Standard Specification for Faced Rigid Cellular Polyisocyanurate Thermal Insulation Board
Effective Date
10-Aug-1997

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ASTM C1363-97 - Standard Test Method for the Thermal Performance of Building Assemblies by Means of a Hot Box ApparatusASTM C1363-97 - Standard Test Method for the Thermal Performance of Building Assemblies by Means of a Hot Box Apparatus
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ASTM C1363-97 - Standard Test Method for the Thermal Performance of Building Assemblies by Means of a Hot Box Apparatus
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: C 1363 – 97
Standard Test Method for
the Thermal Performance of Building Assemblies by Means
1
of a Hot Box Apparatus
This standard is issued under the fixed designation C 1363; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope metering area. Special calibration specimens and procedures
are required for these tests. The general testing procedures for
1.1 This test method covers the laboratory measurement of
these cases are described in Annex A4.
heat transfer through a specimen under controlled air tempera-
1.6 Specific procedures for the thermal testing of window
ture, air velocity, and thermal radiation conditions established
and door systems are described in Test Method C 1199 and
in a metering chamber on one side and in a climatic chamber
Practice E 1423. The hot box also may be used to investigate
on the other side.
the effect of non-homogeneous building assemblies such as
1.2 This test method generally is used for large homoge-
structural members, piping, electrical outlets, or construction
neous or nonhomogeneous specimens. This test method may
defects such as insulation voids.
be applied to any building structure or composite assemblies of
1.7 This test method governs steady-state tests and does not
building elements for which it is possible to build a represen-
establish procedures or criteria for conducting dynamic tests or
tative specimen of a size that is appropriate for the apparatus.
for analysis of dynamic test data. However, several hot box
NOTE 1—This test method was prepared for the purpose of replacing
apparatuses have been operated under dynamic (non-steady-
Test Methods C 236 and C 976. The test method was developed by
state) conditions (1). Dynamic control strategies have included
combining the technical information contained in the two existing hot box
both periodic or non-periodic temperature cycles, for example,
methods with some additional information added to improve the test
to follow a diurnal cycle.
accuracy and reproducibility. Test apparatus, designed and operated under
Test Methods C 236 and C 976, should, in most cases, meet the require- 1.8 This test method does not permit intentional mass
ments of this test method with only slight modifications to calibration and
transfer of air or moisture through the specimen during
operational procedures.
measurements of energy transfer. Air infiltration or moisture
migration can significantly alter net heat transfer. Complicated
1.3 Thistestmethodisintendedforuseatconditionstypical
interactions and dependence upon many variables, coupled
of normal building applications. The usual consideration is to
withonlyalimitedexperienceintestingundersuchconditions,
duplicate naturally occurring outside conditions that in temper-
have made it inadvisable to include this type of testing in this
ate zones may range from approximately –48 to 85°C and
test method. ASTM Subcommittee C16.30 has several task
normal inside residential temperatures of approximately 21°C.
groups that are researching this testing need, and will be
Building materials used to construct the specimens are gener-
preparing a separate standard. Further considerations for such
ally pre-conditioned to typical laboratory conditions of 23°C
testing are given in Appendix X1.
and 50 % relative humidity prior to assembly. Practice C 870
1.9 This test method sets forth the general design require-
may be used as a guide for sample conditioning. Further
ments necessary to construct and operate a satisfactory hot box
conditioning prior to testing may be performed to provide
apparatus, and covers a wide variety of apparatus construc-
moisture conditioned samples, if necessary.
tions, test conditions, and operating conditions. Detailed de-
1.4 This test method permits operation under natural or
signs conforming to this test method are not given, but must be
forced convective conditions at the specimen surface. The
developed within the constraints of the general requirements.
direction of air flow motion may be either perpendicular or
Examples of analysis tools, concepts, and procedures used in
parallel to the surface.
thedesign,construction,calibration,andoperationofahotbox
1.5 The hot box apparatus also can be used for measure-
apparatus are provided in Refs (1-26).
ments of individual building elements that are smaller than the
1.10 This test method does not specify all details necessary
for the operation of the apparatus. Decisions on sampling,
1
This test method is under the jurisdiction of ASTM Committee C-16 on
specimen selection, preconditioning, specimen mounti
...

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ASTM C1373/C1373M-23(Practice)
Standard Practice for Determination of Thermal Resistance of Attic Insulation Systems Under Simulated Winter Conditions

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FIG. 1 Schematic of Thermal Resistance for a Permeable Attic Insulation Under Simulated Winter Conditions (Heat Flow Up)
Note 1: A constant hot-side temperature (T, hot) is used for both tests and the temperature difference increases as the cold side temperature (T, cold) is decreased. See 5.1.6 for requirements on size of air space.  
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1.1 This practice presents a laboratory procedure to determine the thermal resistance of attic insulation systems under simulated steady-state winter conditions. The practice applies only to attic insulation systems that face an open attic air space.  
1.2 The thermal resistance of the insulation is inferred from calculations based on measurements on a ceiling system consisting of components consistent with the system being studied. For example, such a system might consist of a gypsum board or plywood ceiling, wood ceiling joists, and attic insulation with its top exposed to an open air space. The temperature applied to the gypsum board or plywood shall be in the range of 18 to 24°C [64 to 75°F]. The air temperature above the insulation shall correspond to winter conditions and ranges from –46°C to 10°C [–51 to 50°F]. The gypsum board or plywood ceiling shall be sealed to prevent direct airflow between the warm and cold sides of the system.  
1.3 This practice applies to a wide variety of loose-fill or blanket thermal insulation products including fibrous glass, rock/slag wool, or cellulosic fiber materials; granular types including vermiculite and perlite; pelletized products; and any other insulation material that is installed pneumatically or poured in place. The practice considers the effects on heat transfer of structures, specifically the ceiling joists, substrate, for example, gypsum board, air films, and possible facings, films, or other materials that are used in conjunction with the insulation.  
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ASTM C1859-23(Practice)
Standard Practice for Determination of Thermal Resistance of Pneumatically Installed Loose-Fill Building Insulation (Behind Netting) for Enclosed Applications of the Building Thermal Envelope

SIGNIFICANCE AND USE
4.1 The thermal resistance, R, of an insulation is used to describe its thermal performance.  
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4.3 In normal use, the thickness of these products range from less than 100 mm (4 in.) to greater than 150 mm (6 in.). Installed densities depend upon the product type, the installed thickness, the installation equipment used, the installation techniques, and the geometry of the insulated space.  
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4.6 If the density for test purposes is not available from the coverage chart, a test density shall be established by use of applicable specifications and codes or, if none apply, agreement between the requesting body and the testing organization.  
4.7 Generally, thin sections of these materials are not uniform. Thus, the test thickness must be greater than or equal to the product’s representative thickness if the results are to be consistent and typical of use.
Note 1: The representative thickness is specific for each product and is determined by running a series of tests in which the density is held constant but the thickness is increased. The representative thickness is defined here as that thickness above which there is no more than a 2 % change in the resistivity of the product. The representative thickness is a function of product blown density. In gene...
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1.1 This practice presents a laboratory guide to determine the thermal resistance of pneumatically installed loose-fill building insulations for enclosed applications of the building thermal envelope behind netting at mean temperatures between –10 and 35°C (14 to 95°F).  
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ABSTRACT
This specification establishes the composition and physical properties of rigid polyimide cellular foams intended for use as thermal and sound-isolating insulation in commercial and industrial environments. The polyimide insulations covered are classified into three types (Types I, II, and III) according to closed cell content, and into four grades (Grades 1, 2, 3, and 4) according to density. Type II insulation is further divided into two classes (Classes 1 and 2) according to upper temperature limits. Materials shall be manufactured from the appropriate monomers and necessary ingredients. Specimens shall be sampled, tested, and conform accordingly to the following physical property requirements: apparent thermal conductivity; water and gas permeability; density; percent closed cell; upper temperature limit; high temperature stability; compressive strength; compressive force deflection; water vapor transmission; steam aging characteristics (tensile strength, dimensional and weight changes), corrosiveness; chemical resistance; vertical burn characteristics (flame application and time, burn length, and dripping); specific optical smoke density for both flaming and non-flaming exposures; toxic smoke generation; surface burning characteristics (flame spread and smoke developed indices); combustion by-products (carbon monoxide, hydrogen fluoride, hydrogen chloride, nitrogen oxides, sulfur dioxide, and hydrogen cyanide); oxygen index, and 14 scale room burn.
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1.1.1 The annex shall apply to this specification for marine applications.  
1.1.2 This standard is designed as a material specification and not a design document.  
1.1.3 The values stated in Table 1 and Table 2 are not to be used as design values. It is the buyer’s responsibility to specify design requirements and obtain supporting documentation from the material supplier.  
* = Not available consult manufacturer for additional information.
NA = Not Applicable
NB = A manufacturer can only claim conformance to this standard to the values reported in this table. The * notes are confidential data to the manufacturers and as such are not considered part of any qualifying requirements for the standard and only tell the user to inquire about that data.  
* = Not available consult manufacturer for additional information.
NA = Not Applicable
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1.1 This practice covers standard mean temperatures for reporting thermal properties of thermal insulations, products, and materials, and of related systems and components, both insulated and uninsulated.  
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Note 1: Standard referenced materials are needed to span the temperature range of the tests.  
1.3 This practice recommends standard conditions for use in testing and evaluating thermal properties as a function of temperature by standard test methods.  
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ASTM C1374-18(2023)(Test Method)
Standard Test Method for Determination of Installed Thickness of Pneumatically Applied Loose-Fill Building Insulation

SIGNIFICANCE AND USE
5.1 This test method was designed to give the manufacturer of loose-fill insulation products a way of determining what the initial installed thickness should be in a horizontal open attic for pneumatic applications.  
5.2 The installed thickness value developed by this test method is intended to provide guidance to the installer in order to achieve a minimum mass/unit area for a given R-value.  
5.3 For the purpose of product design, testing should be done at a variety of R-values. At least three R-values should be used: the lowest R-value on the product label, the highest R-value on the product label, and an R-value near the midpoint of the R-value range.
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5.4 Specimens are blown in a manner consistent with the intended installation procedure. Blowing machine settings should be representative of those typically used for field application with that machine.  
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1.1 This test method covers determination of the installed thickness of pneumatically applied loose-fill building insulations prior to settling by simulating an open attic with horizontal blown applications.  
1.2 This test method is a laboratory procedure for use by manufacturers of loose-fill insulation for product design, label development, and quality control testing. The apparatus used produces installed thickness results at a given mass/unit area.  
1.3 This test method is not the same as the design density procedures described in Test Methods C520 or Specifications C739 or C764.  
1.4 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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Standard Specification for Self-Supported Spray Applied Cellulosic Thermal Insulation

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This specification covers self-supported spray applied cellulosic thermal insulation for use as thermal insulation or acoustical absorbent material, or both. The chemically-treated cellulosic materials that are also covered in this specification are used for pneumatic applications operating within a specific temperature range. The materials are classified into two types based on the type of adhesive used and exposure of the application. Specimens for testing should be prepared and tested using the prescribed methods and should conform to the specified values of density, thermal resistance, surface bonding characteristics, adhesive strength, cohesive strength, smoldering combustion, fungi resistance, corrosion, moisture vapor absorption, odor, flame resistance permanency, substrate deflection, and air erosion.
SCOPE
1.1 The specification covers the physical properties of self-supported spray applied cellulosic fibers intended for use as thermal insulation or an acoustical absorbent material, or both.  
1.2 This specification covers chemically treated cellulosic materials intended for pneumatic applications where temperatures do not exceed 82.2°C and where temperatures will routinely remain below 65.6°C.  
1.2.1 Type I—Material applied with liquid adhesive and suitable for either exposed or enclosed applications.  
1.2.2 Type II—Materials containing a dry adhesive that is activated by water during installation and intended only for enclosed or covered applications.  
1.3 This is a material specification only and is not intended to deal with methods of application that are supplied by the manufacturer.  
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM C1919-22(Practice)
Standard Practice for Measurement of the Steady-State Thermal Transmission Properties of Small Specimens Using the Heat Flow Meter Apparatus

SIGNIFICANCE AND USE
5.1 Thermal conductivity measurements on small insulation specimens are important during new product development processes or when larger specimens cannot be collected during forensic investigation (that is, failure analysis) (1, 2).  
5.2 Numerous research projects have recently been initiated to develop insulation materials that have very high thermal resistivities (greater than 83 (m K)/W). Projects ranging from coatings to improve the thermal performance of single pane/layer glazing systems to the development of novel insulation products for building envelopes are being undertaken (1-4). All these projects have struggled in the development of new material technologies due to the difficulty associated with the measurement of thermal conductivity of small sections (approximately 0.025 m by 0.025 m) of high thermal resistance materials. As new materials are being developed, the size of each test specimen impacts the cost of development. Most of the existing test equipment and the methods do not align with the researcher’s need; the equipment requires a large specimen size is time consuming, and expensive to produce.  
5.3 This practice provides a standardized procedure to enable the thermal characterization of small specimens of insulation materials. Accurate, and reliable thermal metrology to assess thermal properties of new insulation materials, such as novel very low thermal conductivity (  
5.4 The ratio of the area of the specimen and the heat flux transducer has a significant impact on the uncertainty of the results obtained from this practice. As the specimen area decreases this ratio decreases, a smaller percentage of the total heat flow is associated with the unknown specimen. Information from the literature (4) shows that some heat-flow-meter apparatus, generally not available commercially and used by the research laboratories only, can be modified to change out the heat flux transducer so that transducers of varying sizes can be deployed. The observat...
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1.1 This practice covers the measurement of steady state thermal transmission properties of the small flat slab thermal insulation specimen using a heat-flow-meter apparatus.  
1.2 This practice provides a supplemental procedure for use in conjunction with Test Method C518 for testing a small specimen. This practice is limited to only small specimens and, in all other particulars, the requirements of Test Method C518 apply.  
1.3 This practice characterizes small specimens having lateral dimensions less than the lateral dimensions of the heat flux transducer used to measure the heat flow. The procedure in Test Method C518 shall be used for specimens having lateral dimensions equal to or larger than the lateral dimensions of the heat flux transducer.
Note 1: The lower limit for specimen size is typically determined by the user for their particular material. As an example, Ref. (1)2 established a lower limit for specimen dimensions of 0.1 m by 0.1 m for several different thermal insulation materials for a 0.3 m by 0.3 m heat-flow-meter apparatus having a heat flux transducer 0.15 m by 0.15 m.  
1.4 This practice is intended only for research purposes, in particular, when larger specimens are unavailable. This practice shall not be used in conjunction with Test Method C518 for certification testing of products; compliance with ASTM Specifications; or compliance with regulatory or building code requirements.  
1.5 The values stated in SI units are to be regarded as the standard. No other units of measurement are included in this practice.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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ASTM C1199-22(Test Method)
Standard Test Method for Measuring the Steady-State Thermal Transmittance of Fenestration Systems Using Hot Box Methods

SIGNIFICANCE AND USE
4.1 This test method details the calibration and testing procedures and necessary additional temperature instrumentation required in applying Test Method C1363 to measure the thermal transmittance of fenestration systems mounted vertically in the thermal chamber.  
4.2 The thermal transmittance of a test specimen is affected by its size and three-dimensional geometry. Care must be exercised when extrapolating to product sizes smaller or larger than the test specimen. Therefore, it is recommended that fenestration systems be tested at the recommended sizes specified in Practice E1423 or NFRC 100.  
4.3 Since both temperature and surface heat transfer coefficient conditions affect results, use of recommended conditions will assist in reducing confusion caused by comparing results of tests performed under dissimilar conditions. Standardized test conditions for determining the thermal transmittance of fenestration systems are specified in Practice E1423 and Section 6.2. The performance of a test specimen measured at standardized test conditions is potentially different than the performance of the same fenestration product when installed in the wall of a building located outdoors. Standardized test conditions often represent extreme summer or winter design conditions, which are potentially different than the average conditions typically experienced by a fenestration product installed in an exterior wall. For the purpose of comparison, it is essential to calibrate with surface heat transfer coefficients on the Calibration Transfer Standard (CTS) which are as close as possible to the conventionally accepted values for building design; however, this procedure can be used at other conditions for research purposes or product development.  
4.4 Similarly, it would be desirable to have a surround panel that closely duplicates the actual wall where the fenestration system would be installed. Since there are such a wide variety of fenestration system openings in North American...
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1.1 This test method covers requirements and guidelines and specifies calibration procedures required for the measurement of the steady-state thermal transmittance of fenestration systems installed vertically in the test chamber. This test method specifies the necessary measurements to be made using measurement systems conforming to Test Method C1363 for determination of fenestration system thermal transmittance.  
Note 1: This test method allows the testing of projecting fenestration products (that is, garden windows, skylights, and roof windows) installed vertically in a surround panel. Current research on skylights, roof windows, and projecting products hopefully will provide additional information that can be added to the next version of this test method so that skylight and roof windows can be tested horizontally or at some angle typical of a sloping roof.  
1.2 This test method refers to the thermal transmittance, U of a fenestration system installed vertically in the absence of solar radiation and air leakage effects.
Note 2: The methods described in this document may also be adapted for use in determining the thermal transmittance of sections of building wall, and roof and floor assemblies containing thermal anomalies, which are smaller than the hot box metering area.  
1.3 This test method describes how to determine the thermal transmittance, US of a fenestration product (also called test specimen) at well-defined environmental conditions. The thermal transmittance is also a reported test result from Test Method C1363. If only the thermal transmittance is reported using this test method, the test report must also include a detailed description of the environmental conditions in the thermal chamber during the test as outlined in 10.1.14.  
1.4 For rating purposes, this test method also describes how to calculate a standardized thermal transmittance,  UST, which can be used to compare test results from labor...

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ASTM
ASTM C1155-95(2021)(Practice)
Standard Practice for Determining Thermal Resistance of Building Envelope Components from the In-Situ Data

SIGNIFICANCE AND USE
5.1 Significance of Thermal Resistance Measurements—Knowledge of the thermal resistance of new buildings is important to determine whether the quality of construction satisfies criteria set by the designer, by the owner, or by a regulatory agency. Differences in quality of materials or workmanship may cause building components not to achieve design performance.  
5.1.1 For Existing Buildings—Knowledge of thermal resistance is important to the owners of older buildings to determine whether the buildings should receive insulation or other energy-conserving improvements. Inadequate knowledge of the thermal properties of materials or heat flow paths within the construction or degradation of materials may cause inaccurate assumptions in calculations that use published data.  
5.2 Advantage of In-Situ Data—This practice provides information about thermal performance that is based on measured data. This may determine the quality of new construction for acceptance by the owner or occupant or it may provide justification for an energy conservation investment that could not be made based on calculations using published design data.  
5.3 Heat Flow Paths—This practice assumes that net heat flow is perpendicular to the surface of the building envelope component within a given subsection. Knowledge of surface temperature in the area subject to measurement is required for placing sensors appropriately. Appropriate use of infrared thermography is often used to obtain such information. Thermography reveals nonuniform surface temperatures caused by structural members, convection currents, air leakage, and moisture in insulation. Practices C1060 and C1153 detail the appropriate use of infrared thermography. Note that thermography as a basis for extrapolating the results obtained at a measurement site to other similar parts of the same building is beyond the scope of this practice.  
5.4 User Knowledge Required—This practice requires that the user have knowledge that the data empl...
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1.1 This practice covers how to obtain and use data from in-situ measurement of temperatures and heat fluxes on building envelopes to compute thermal resistance. Thermal resistance is defined in Terminology C168 in terms of steady-state conditions only. This practice provides an estimate of that value for the range of temperatures encountered during the measurement of temperatures and heat flux.  
1.2 This practice presents two specific techniques, the summation technique and the sum of least squares technique, and permits the use of other techniques that have been properly validated. This practice provides a means for estimating the mean temperature of the building component for estimating the dependence of measured R-value on temperature for the summation technique. The sum of least squares technique produces a calculation of thermal resistance which is a function of mean temperature.  
1.3 Each thermal resistance calculation applies to a subsection of the building envelope component that was instrumented. Each calculation applies to temperature conditions similar to those of the measurement. The calculation of thermal resistance from in-situ data represents in-service conditions. However, field measurements of temperature and heat flux may not achieve the accuracy obtainable in laboratory apparatuses.  
1.4 This practice permits calculation of thermal resistance on portions of a building envelope that have been properly instrumented with temperature and heat flux sensing instruments. The size of sensors and construction of the building component determine how many sensors shall be used and where they should be placed. Because of the variety of possible construction types, sensor placement and subsequent data analysis require the demonstrated good judgement of the user.  
1.5 Each calculation pertains only to a defined subsection of the building envelope. Combining results from different subsections to characterize...

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ASTM
ASTM C518-21(Test Method)
Standard Test Method for Steady-State Thermal Transmission Properties by Means of the Heat Flow Meter Apparatus

SIGNIFICANCE AND USE
4.1 This test method provides a rapid means of determining the steady-state thermal transmission properties of thermal insulations and other materials with a high level of accuracy when the apparatus has been calibrated appropriately.  
4.2 Proper calibration of the heat flow meter apparatus requires that it be calibrated using specimen(s) having thermal transmission properties determined previously by Test Methods C177, or C1114.
Note 1: Calibration of the apparatus typically requires specimens that are similar to the types of materials, thermal conductances, thicknesses, mean temperatures, and temperature gradients as expected for the test specimens.  
4.3 The thermal transmission properties of specimens of a given material or product may vary due to variability of the composition of the material; be affected by moisture or other conditions; change with time; change with mean temperature and temperature difference; and depend upon the prior thermal history. It must be recognized, therefore, that the selection of typical values of thermal transmission properties representative of a material in a particular application should be based on a consideration of these factors and will not apply necessarily without modification to all service conditions.  
4.3.1 As an example, this test method provides that the thermal properties shall be obtained on specimens that do not contain any free moisture although in service such conditions may not be realized. Even more basic is the dependence of the thermal properties on variables, such as mean temperature and temperature difference. These dependencies should be measured or the test made at conditions typical of use.  
4.4 Special care shall be taken in the measurement procedure for specimens exhibiting appreciable inhomogeneities, anisotropies, rigidity, or especially high or low resistance to heat flow (see Practice C1045). The use of a heat flow meter apparatus when there are thermal bridges present in the specimen may ...
SCOPE
1.1 This test method covers the measurement of steady state thermal transmission through flat slab specimens using a heat flow meter apparatus.  
1.2 The heat flow meter apparatus is used widely because it is relatively simple in concept, rapid, and applicable to a wide range of test specimens. The precision and bias of the heat flow meter apparatus can be excellent provided calibration is carried out within the range of heat flows expected. This means calibration shall be carried out with similar types of materials, of similar thermal conductances, at similar thicknesses, mean temperatures, and temperature gradients, as expected for the test specimens.  
1.3 This a comparative, or secondary, method of measurement since specimens of known thermal transmission properties shall be used to calibrate the apparatus. Properties of the calibration specimens must be traceable to an absolute measurement method. The calibration specimens should be obtained from a recognized national standards laboratory.  
1.4 The heat flow meter apparatus establishes steady state one-dimensional heat flux through a test specimen between two parallel plates at constant but different temperatures. By appropriate calibration of the heat flux transducer(s) with calibration standards and by measurement of the plate temperatures and plate separation. Fourier’s law of heat conduction is used to calculate thermal conductivity, and thermal resistivity or thermal resistance and thermal conductance.  
1.5 This test method shall be used in conjunction with Practice C1045. Many advances have been made in thermal technology, both in measurement techniques and in improved understanding of the principles of heat flow through materials. These advances have prompted revisions in the conceptual approaches to the measurement of the thermal transmission properties (1-4).2 All users of this test method should be aware of these concepts.  
1.6 This test method is ...

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