ASTM E1077-01e1
(Test Method)Standard Test Methods for Estimating the Depth of Decarburization of Steel Specimens
Standard Test Methods for Estimating the Depth of Decarburization of Steel Specimens
SCOPE
1.1 These test methods cover procedures for estimating the depth of decarburization of steels irrespective of the composition, matrix microstructure, or section shape. The following basic procedures may be used:
1.1.1 Screening methods.
1.1.2 Microscopical methods.
1.1.3 Microindentation hardness methods.
1.1.4 Chemical analysis methods.
1.2 In case of a dispute, the rigorous quantitative or lineal analysis method (see 7.3.5 and 7.3.6) shall be the referee method. These methods can be employed with any cross-sectional shape. The chemical analytical methods generally reveal a greater depth of decarburization than the microscopical methods but are limited to certain simple shapes and by availability of equipment. These techniques are generally reserved for research studies. The microindentation hardness method is suitable for accurate measurements of hardened structures with relatively homogeneous microstructures.
1.3 The values stated in SI units are to be regarded as standard. The inch-pound equivalents are in parentheses and may be approximate.
1.4 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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e1
Designation:E1077–01
Standard Test Methods for
Estimating the Depth of Decarburization of Steel
1
Specimens
This standard is issued under the fixed designation E 1077; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
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e NOTE—Sections 2.1 and 3.1.1 were editorially revised in June 2001.
INTRODUCTION
These test methods may be used to estimate the average or greatest depth of decarburization in
hardened or non-hardened steel products. The test methods described range from simple screening
tests to more statistically rigorous test methods depending upon the needs of the investigation.
1. Scope 2. Referenced Documents
1.1 These test methods cover procedures for estimating the 2.1 ASTM Standards:
depth of decarburization of steels irrespective of the composi- A 941 Terminology Relating to Steel, Stainless Steel, Re-
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tion, matrix microstructure, or section shape. The following lated Alloys and Ferroalloys
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basic procedures may be used: E 3 Practice for Preparation of Metallographic Specimens
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1.1.1 Screening methods. E 7 Terminology Relating to Metallography
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1.1.2 Microscopical methods. E 340 Test Method for Macroetching Metals and Alloys
1.1.3 Microindentation hardness methods. E 350 Test Methods for ChemicalAnalysis of Carbon Steel,
1.1.4 Chemical analysis methods. Low-Alloy Steel, Silicon Electrical Steel, Ingot Iron, and
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1.2 In case of a dispute, the rigorous quantitative or lineal Wrought Iron
analysis method (see 7.3.5 and 7.3.6) shall be the referee E 384 Test Method for Microindentation Hardness of Ma-
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method. These methods can be employed with any cross- terials
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sectional shape. The chemical analytical methods generally E 407 Practice for Microetching Metals and Alloys
reveal a greater depth of decarburization than the microscopi- E 415 Test Method for Optical Emission Vacuum Spectro-
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cal methods but are limited to certain simple shapes and by metric Analysis of Carbon and Low-Alloy Steel
availability of equipment. These techniques are generally E 1951 Guide for Calibrating Reticals and Light Micro-
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reserved for research studies. The microindentation hardness scope Magnifications
method is suitable for accurate measurements of hardened
3. Terminology
structures with relatively homogeneous microstructures.
1.3 The values stated in SI units are to be regarded as 3.1 Definitions:
standard. The inch-pound equivalents are in parentheses and 3.1.1 Fordefinitionsoftermsusedinthesetestmethods,see
Terminology E 7 and Terminology A 941.
may be approximate.
1.4 This standard does not purport to address all of the 3.2 Definitions of Terms Specific to This Standard:
3.2.1 average depth of decarburization—the mean value of
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appro- five or more measurements of the total depth of decarburiza-
tion.
priate safety and health practices and determine the applica-
bility of regulatory limitations prior to use. 3.2.2 average free-ferrite depth—the mean value of five or
more measurements of the depth of complete decarburization.
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These test methods are under the jurisdiction of ASTM Committee E04 on
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Metallography and are the direct responsibility of Subcommittee E04.14 on Annual Book of ASTM Standards, Vol 01.02.
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Quantitative Metallography. Annual Book of ASTM Standards, Vol 03.01.
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Current edition approved March 10, 2001. Published May 2001. Originally Annual Book of ASTM Standards, Vol 03.05.
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published as E 1077 – 85. Last previous edition E 1077 – 91 (1997). Annual Book of ASTM Standards, Vol 03.06.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
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E1077–01
3.2.3 complete decarburization—loss of carbon content at 5.7 Microscopical tests are generally satisfactory for deter-
the surface of a steel specimen to a level below the solubility miningthesuitabilityofmaterialforintendeduse,specification
limit of carbon in ferrite so that only ferrite is present. acceptance, manufacturing control, development, or research.
3.2.4 free-ferrite depth—the perpendicular distance from
6. Sampling
the surface of the specimen to that location where the structure
is no longer fully ferritic, that is, other transformation products
6.1 Samples should be taken at locations that are represen-
are observed.
tative of the bulk specimen. The location and number of
samplestakendependsonthenatureofthema
...
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