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ASTM C1470-06(2013)

(Guide)

Standard Guide for Testing the Thermal Properties of Advanced Ceramics

Standard Guide for Testing the Thermal Properties of Advanced Ceramics

SIGNIFICANCE AND USE
5.1 The high-temperature capabilities of advanced ceramics are a key performance benefit for many demanding engineering applications. In many of those applications, advanced ceramics will have to perform across a broad temperature range. The thermal expansion, thermal diffusivity/conductivity, specific heat, and emittance/emissivity are crucial engineering factors in integrating ceramic components into aerospace, automotive, and industrial systems  
5.2 This guide is intended to serve as a reference and information source for testing the thermal properties of advanced ceramics, based on an understanding of the relationships between the composition and microstructure of these materials and their thermal properties.  
5.3 The use of this guide assists the testing community in correctly applying the ASTM thermal test methods to advanced ceramics to ensure that the thermal test results are properly measured, interpreted, and understood. This guide also assists the user in selecting the appropriate thermal test method to evaluate the particular thermal properties of the advanced ceramic of interest.  
5.4 The thermal properties of advanced ceramics are critical data in the development of ceramic components for aerospace, automotive, and industrial applications. In addition, the effect of environmental exposure on thermal properties of the advanced ceramics must also be assessed.
SCOPE
1.1 This guide covers the thermal property testing of advanced ceramics, to include monolithic ceramics, particulate/ whisker-reinforced ceramics, and continuous fiber-reinforced ceramic composites. It is intended to provide guidance and information to users on the special considerations involved in determining the thermal properties of these ceramic materials.  
1.2 Five thermal properties (specific heat capacity, thermal conductivity, thermal diffusivity, thermal expansion, and emittance/emissivity) are presented in terms of their definitions and general test methods. The relationship between thermal properties and the composition, microstructure, and processing of advanced ceramics (monolithic and composite) is briefly outlined, providing guidance on which material and specimen characteristics have to be considered in evaluating the thermal properties of advanced ceramics. Additional sections describe sampling considerations, test specimen preparation, and reporting requirements.  
1.3 Current ASTM test methods for thermal properties are tabulated in terms of test method concept, testing range, specimen requirements, standards/reference materials, capabilities, limitations, precision, and special instructions for monolithic and composite ceramics.  
1.4 This guide is based on the use of current ASTM standards for thermal properties where appropriate and on the development of new test standards where necessary. It is not the intent of this guide to rigidly specify particular thermal test methods for advanced ceramics. Guidance is provided on how to utilize the most commonly available ASTM thermal test methods, considering their capabilities and limitations.  
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard. See IEEE/ASTM SI 10.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
31-Jan-2013
ICS
81.060.30 - Advanced ceramics
Technical Committee
C28 - Advanced Ceramics
Drafting Committee
C28.03 - Physical Properties and Non-Destructive Evaluation
Current Stage
Ref Project

Relations

Replaces
ASTM C1470-06 - Standard Guide for Testing the Thermal Properties of Advanced Ceramics
Effective Date
01-Feb-2013
Replaced By
ASTM C1470-20 - Standard Guide for Testing the Thermal Properties of Advanced Ceramics
Effective Date
01-Jan-2020
Referred By
ASTM C1783-15 - Standard Guide for Development of Specifications for Fiber Reinforced Carbon-Carbon Composite Structures for Nuclear Applications
Effective Date
01-Feb-2013
Referred By
ASTM C1793-15 - Standard Guide for Development of Specifications for Fiber Reinforced Silicon Carbide-Silicon Carbide Composite Structures for Nuclear Applications
Effective Date
01-Feb-2013

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ASTM C1470-06(2013) - Standard Guide for Testing the Thermal Properties of Advanced CeramicsASTM C1470-06(2013) - Standard Guide for Testing the Thermal Properties of Advanced Ceramics
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ASTM C1470-06(2013) - Standard Guide for Testing the Thermal Properties of Advanced Ceramics
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: C1470 − 06 (Reapproved 2013)
Standard Guide for
1
Testing the Thermal Properties of Advanced Ceramics
This standard is issued under the fixed designation C1470; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope priate safety and health practices and determine the applica-
bility of regulatory limitations prior to use.
1.1 This guide covers the thermal property testing of ad-
vanced ceramics, to include monolithic ceramics, particulate/
2. Referenced Documents
whisker-reinforced ceramics, and continuous fiber-reinforced
2
2.1 ASTM Standards:
ceramic composites. It is intended to provide guidance and
information to users on the special considerations involved in 2.1.1 Specific Heat:
C351Test Method for Mean Specific Heat of Thermal
determining the thermal properties of these ceramic materials.
3
Insulation (Withdrawn 2008)
1.2 Five thermal properties (specific heat capacity, thermal
D2766Test Method for Specific Heat of Liquids and Solids
conductivity, thermal diffusivity, thermal expansion, and
E1269Test Method for Determining Specific Heat Capacity
emittance/emissivity)arepresentedintermsoftheirdefinitions
by Differential Scanning Calorimetry
and general test methods. The relationship between thermal
2.1.2 Thermal Conductivity:
propertiesandthecomposition,microstructure,andprocessing
C177Test Method for Steady-State Heat Flux Measure-
of advanced ceramics (monolithic and composite) is briefly
ments and Thermal Transmission Properties by Means of
outlined, providing guidance on which material and specimen
the Guarded-Hot-Plate Apparatus
characteristics have to be considered in evaluating the thermal
C182Test Method for Thermal Conductivity of Insulating
properties of advanced ceramics. Additional sections describe
Firebrick
samplingconsiderations,testspecimenpreparation,andreport-
C201Test Method forThermal Conductivity of Refractories
ing requirements.
C202Test Method for Thermal Conductivity of Refractory
1.3 Current ASTM test methods for thermal properties are
Brick
tabulated in terms of test method concept, testing range,
C408Test Method for Thermal Conductivity of Whiteware
specimen requirements, standards/reference materials,
Ceramics
capabilities, limitations, precision, and special instructions for
C518Test Method for Steady-State Thermal Transmission
monolithic and composite ceramics.
Properties by Means of the Heat Flow Meter Apparatus
C767Test Method for Thermal Conductivity of Carbon
1.4 This guide is based on the use of current ASTM
Refractories
standards for thermal properties where appropriate and on the
C1044Practice for Using a Guarded-Hot-PlateApparatus or
development of new test standards where necessary. It is not
Thin-Heater Apparatus in the Single-Sided Mode
theintentofthisguidetorigidlyspecifyparticularthermaltest
C1045Practice for Calculating Thermal Transmission Prop-
methods for advanced ceramics. Guidance is provided on how
erties Under Steady-State Conditions
to utilize the most commonly available ASTM thermal test
C1113Test Method for Thermal Conductivity of Refracto-
methods, considering their capabilities and limitations.
ries by Hot Wire (Platinum Resistance Thermometer
1.5 The values stated in SI units are to be regarded as
Technique)
standard. No other units of measurement are included in this
C1114Test Method for Steady-State Thermal Transmission
standard. See IEEE/ASTM SI10.
Properties by Means of the Thin-Heater Apparatus
1.6 This standard does not purport to address all of the
C1130Practice for Calibrating Thin Heat Flux Transducers
safety concerns, if any, associated with its use. It is the
E1225Test Method for Thermal Conductivity of Solids
responsibility of the user of this standard to establish appro-
1 2
This guide is under the jurisdiction of ASTM Committee C28 on Advanced For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Ceramics and is the direct responsibility of Subcommittee C28.03 on Physical contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Properties and Non-Destructive Evaluation. Standards volume information, refer to the standard’s Document Summary page on
Current edition approved Feb. 1, 2013. Published March 2013. Originally the ASTM website.
3
approved in 2000. Last previous edition approved in 2006 as C1470–06. DOI: The last approved version of this historical standard is referenced on
10.1520/C1470-06R13. www.astm.org.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

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ASTM C1674-23(Test Method)
Standard Test Method for Flexural Strength of Advanced Ceramics with Engineered Porosity (Honeycomb Cellular Channels) at Ambient Temperatures

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5.1 This test method is used to determine the mechanical properties in flexure of engineered ceramic components with multiple longitudinal hollow channels, commonly described as “honeycomb” channel architectures. The components generally have 30 % or more porosity and the cross-sectional dimensions of the honeycomb channels are on the order of 1 mm or greater.  
5.2 The experimental data and calculated strength values from this test method are used for material and structural development, product characterization, design data, quality control, and engineering/production specifications.
Note 1: Flexure testing is the preferred method for determining the nominal “tensile fracture” strength of these components, as compared to a compression (crushing) test. A nominal tensile strength is required, because these materials commonly fail in tension under thermal gradient stresses. A true tensile test is difficult to perform on these honeycomb specimens because of gripping and alignment challenges.  
5.3 The mechanical properties determined by this test method are both material and architecture dependent, because the mechanical response and strength of the porous test specimens are determined by a combination of inherent material properties and microstructure and the architecture of the channel porosity [porosity fraction/relative density, channel geometry (shape, dimensions, cell wall thickness, etc.), anisotropy and uniformity, etc.] in the specimen. Comparison of test data must consider both differences in material/composition properties as well as differences in channel porosity architecture between individual specimens and differences between and within specimen lots.  
5.4 Test Method A is a user-defined specimen geometry with a choice of four-point or three-point flexure testing geometries. It is not possible to define a single fixed specimen geometry for flexure testing of honeycombs, because of the wide range of honeycomb architectures and cell sizes and consid...
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1.1 This test method covers the determination of the flexural strength (modulus of rupture in bending) at ambient conditions of advanced ceramic structures with 2-dimensional honeycomb channel architectures.  
1.2 The test method is focused on engineered ceramic components with longitudinal hollow channels, commonly called “honeycomb” channels (see Fig. 1). The components generally have 30 % or more porosity and the cross-sectional dimensions of the honeycomb channels are on the order of 1 mm or greater. Ceramics with these honeycomb structures are used in a wide range of applications (catalytic conversion supports (1),2 high temperature filters (2, 3), combustion burner plates (4), energy absorption and damping (5), etc.). The honeycomb ceramics can be made in a range of ceramic compositions—alumina, cordierite, zirconia, spinel, mullite, silicon carbide, silicon nitride, graphite, and carbon. The components are produced in a variety of geometries (blocks, plates, cylinders, rods, rings).
FIG. 1 General Schematics of Typical Honeycomb Ceramic Structures  
1.3 The test method describes two test specimen geometries for determining the flexural strength (modulus of rupture) for a porous honeycomb ceramic test specimen (see Fig. 2):
FIG. 2 Flexure Loading Configurations  
L = Outer Span Length (for Test Method A, L = User defined; for Test Method B, L = 90 mm)
Note 1: 4-Point-1/4 Loading for Test Methods A1 and B.
Note 2: 3-Point Loading for Test Method A2.  
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1.3.2 Test Method B—A 4-point-1/4 point bending test with a defined rectangular specimen geometry (13 mm × 25 mm × > 116 mm) and a 90 mm outer support span geometry suitable for cordierite and silicon carbide honeycombs with small cell sizes.  
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ASTM C1341-13(2023)(Test Method)
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SIGNIFICANCE AND USE
5.1 This test method is used for material development, quality control, and material flexural specifications. Although flexural test methods are commonly used to determine design strengths of monolithic advanced ceramics, the use of flexure test data for determining tensile or compressive properties of CFCC materials is strongly discouraged. The nonuniform stress distributions in the flexure test specimen, the dissimilar mechanical behavior in tension and compression for CFCCs, low shear strengths of CFCCs, and anisotropy in fiber architecture all lead to ambiguity in using flexure results for CFCC material design data (1-4).3 Rather, uniaxial-forced tensile and compressive tests are recommended for developing CFCC material design data based on a uniformly stressed test condition.  
5.2 In this test method, the flexure stress is computed from elastic beam theory with the simplifying assumptions that the material is homogeneous and linearly elastic. This is valid for composites where the principal fiber direction is coincident/transverse with the axis of the beam. These assumptions are necessary to calculate a flexural strength value, but limit the application to comparative type testing such as used for material development, quality control, and flexure specifications. Such comparative testing requires consistent and standardized test conditions, that is, test specimen geometry/thickness, strain rates, and atmospheric/test conditions.  
5.3 Unlike monolithic advanced ceramics which fracture catastrophically from a single dominant flaw, CFCCs generally experience “graceful” fracture from a cumulative damage process. Therefore, the volume of material subjected to a uniform flexural stress may not be as significant a factor in determining the flexural strength of CFCCs. However, the need to test a statistically significant number of flexure test specimens is not eliminated. Because of the probabilistic nature of the strength of the brittle matrices and of the ceramic...
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1.1 This test method covers the determination of flexural properties of continuous fiber-reinforced ceramic composites in the form of rectangular bars formed directly or cut from sheets, plates, or molded shapes. Three test geometries are described as follows:  
1.1.1 Test Geometry I—A three-point loading system utilizing center point force application on a simply supported beam.  
1.1.2 Test Geometry IIA—A four-point loading system utilizing two force application points equally spaced from their adjacent support points, with a distance between force application points of one-half of the support span.  
1.1.3 Test Geometry IIB—A four-point loading system utilizing two force application points equally spaced from their adjacent support points, with a distance between force application points of one-third of the support span.  
1.2 This test method applies primarily to all advanced ceramic matrix composites with continuous fiber reinforcement: unidirectional (1D), bidirectional (2D), tridirectional (3D), and other continuous fiber architectures. In addition, this test method may also be used with glass (amorphous) matrix composites with continuous fiber reinforcement. However, flexural strength cannot be determined for those materials that do not break or fail by tension or compression in the outer fibers. This test method does not directly address discontinuous fiber-reinforced, whisker-reinforced, or particulate-reinforced ceramics. Those types of ceramic matrix composites are better tested in flexure using Test Methods C1161 and C1211.  
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ASTM C1869-18(2023)(Test Method)
Standard Test Method for Open-Hole Tensile Strength of Fiber-Reinforced Advanced Ceramic Composites

SIGNIFICANCE AND USE
5.1 Open-hole tests of composites are used for material and design development for the engineering application of composite materials (5-11). The presence of an open hole in a composite component reduces the cross-sectional area available to carry an applied force, creates stress concentrations, and creates new edges where delamination may occur. Standardized open-hole tests for composite materials can provide useful information about how a composite material may perform in an open-hole application and how to design the composite for notches and holes.  
5.2 The test method defines two baseline test specimen geometries and a test procedure for producing comparable, reproducible OHT test data. The test method is designed to produce OHT strength data for structural design allowables, material specifications, material development and comparison, material characterization, and quality assurance. The mechanical properties that may be calculated from this test method include:  
5.2.1 The open-hole (notched) tensile strength (SOHTx) for test specimen with a hole diameter x (mm).  
5.2.2 The net section tensile strength (SNSx) for a test specimen with a hole diameter x (mm).  
5.2.3 The proportional limit stress (σ0) for an OHT specimen with a given hole diameter.  
5.2.4 The stress response of the OHT test specimen, as shown by the stress-time or stress-displacement plot.  
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FIG. 1 OHT Test Specimens A and B  
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FIG. 1 Four-Point-1/4-Point Flexure Loading Configuration  
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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Standard Test Method for Knoop Indentation Hardness of Advanced Ceramics

SIGNIFICANCE AND USE
5.1 For advanced ceramics, Knoop indenters are used to create indentations. The surface projection of the long diagonal is measured with optical microscopes.  
5.2 The Knoop indentation hardness is one of many properties that is used to characterize advanced ceramics. Attempts have been made to relate Knoop indentation hardness to other hardness scales, but no generally accepted methods are available. Such conversions are limited in scope and should be used with caution, except for special cases where a reliable basis for the conversion has been obtained by comparison tests.  
5.3 For advanced ceramics, the Knoop indentation is often preferred to the Vickers indentation since the Knoop long diagonal length is 2.8 times longer than the Vickers diagonal for the same force, and cracking is much less of a problem (1).5 On the other hand, the long slender tip of the Knoop indentation is more difficult to precisely discern, especially in materials with low contrast. The indentation forces chosen in this test method are designed to produce indentations as large as may be possible with conventional microhardness equipment, yet not so large as to cause cracking.  
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5.5 Knoop hardness is calculated from the ratio of the applied force divided by the projected indentation area on the specimen surface. It is assumed that the elastic springback of the narrow diagonal is negligible. (Vickers indenters are also used to measure hardness, but Vickers hardness is calculated from the ratio of applied force to the area of contact of the four faces of the undeformed indenter.)  
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1.1 This test method covers the determination of the Knoop indentation hardness of advanced ceramics. In this test, a pointed, rhombic-based, pyramidal diamond indenter of prescribed shape is pressed into the surface of a ceramic with a predetermined force to produce a relatively small, permanent indentation. The surface projection of the long diagonal of the permanent indentation is measured using a light microscope. The length of the long diagonal and the applied force are used to calculate the Knoop hardness which represents the material’s resistance to penetration by the Knoop indenter.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 Units—When Knoop and Vickers hardness tests were developed, the force levels were specified in units of grams-force (gf) and kilograms-force (kgf). This standard specifies the units of force and length in the International System of Units (SI); that is, force in newtons (N) and length in mm or μm. However, because of the historical precedent and continued common usage, force values in gf and kgf units are occasionally provided for information. This test method specifies that Knoop hardness be reported either in units of GPa or as a dimensionless Knoop hardness number.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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ASTM C1495-16(2023)(Test Method)
Standard Test Method for Effect of Surface Grinding on Flexure Strength of Advanced Ceramics

SIGNIFICANCE AND USE
5.1 Surface grinding can cause a significant decrease4 in the flexure strength of advanced ceramic materials. The magnitude of the loss in strength is determined by the grinding conditions and the response of the material. This test method can be used to obtain a detailed characterization of the relationship between grinding conditions and flexure strength for an advanced ceramic material. The effect on flexure strength of varying a single grinding parameter or several grinding parameters can be measured. The method may also be used to compare and rank different materials according to their response to one or more different grinding conditions. Results obtained by this method can be used to develop an optimum grinding process with respect to maximizing material removal rate for a specified flexure strength requirement. The test method can assist in the development of improved grinding-damage-tolerant ceramic materials. It may also be used for quality control purposes to monitor and assure the consistency of a grinding process in the fabrication of parts from advanced ceramic materials. The test method is applicable to grinding methods that generate a planar surface and is not directly applicable to grinding methods that produce non-planar surfaces such as cylindrical and centerless grinding.
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1.1 This test method covers the determination of the effect of surface grinding on the flexure strength of advanced ceramics. Surface grinding of an advanced ceramic material can introduce microcracks and other changes in the near surface layer, generally referred to as damage (see Fig. 1 and Ref. (1)).2 Such damage can result in a change—most often a decrease—in flexure strength of the material. The degree of change in flexure strength is determined by both the grinding process and the response characteristics of the specific ceramic material. This method compares the flexure strength of an advanced ceramic material after application of a user-specified surface grinding process with the baseline flexure strength of the same material. The baseline flexure strength is obtained after application of a surface grinding process specified in this standard. The baseline flexure strength is expected to approximate closely the inherent strength of the material. The flexure strength is measured by means of ASTM flexure test methods.
FIG. 1 Microcracks Associated with Grinding (Ref. (1))2  
1.2 Flexure test methods used to determine the effect of surface grinding are C1161 Test Method for Flexure Strength of Advanced Ceramics at Ambient Temperatures and C1211 Test Method for Flexure Strength of Advanced Ceramics at Elevated Temperatures.  
1.3 Materials covered in this standard are those advanced ceramics that meet criteria specified in flexure testing standards C1161 and C1211.  
1.4 The flexure test methods supporting this standard (C1161 and C1211) require test specimens that have a rectangular cross section, flat surfaces, and that are fabricated with specific dimensions and tolerances. Only grinding processes that are capable of generating the specified flat surfaces, that is, planar grinding modes, are suitable for evaluation by this method. Among the applicable machine types are horizontal and vertical spindle reciprocating surface grinders, horizontal and vertical spindle rotary surface grinders, double disk grinders, and tool-and-cutter grinders. Incremental cross-feed, plunge, and creep-feed grinding methods may be used.  
1.5 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.7 This international standard was develop...

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ASTM C1211-18(2023)(Test Method)
Standard Test Method for Flexural Strength of Advanced Ceramics at Elevated Temperatures

SIGNIFICANCE AND USE
4.1 This test method may be used for material development, quality control, characterization, and design data generation purposes. This test method is intended to be used with ceramics whose flexural strength is ∼50 MPa (∼7 ksi) or greater.  
4.2 The flexure stress is computed based on simple beam theory, with assumptions that the material is isotropic and homogeneous, the moduli of elasticity in tension and compression are identical, and the material is linearly elastic. The average grain size should be no greater than 1/50 of the beam thickness. The homogeneity and isotropy assumptions in the test method rule out the use of it for continuous fiber-reinforced composites for which Test Method C1341 is more appropriate.  
4.3 The flexural strength of a group of test specimens is influenced by several parameters associated with the test procedure. Such factors include the testing rate, test environment, specimen size, specimen preparation, and test fixtures. Specimen and fixture sizes were chosen to provide a balance between the practical configurations and resulting errors as discussed in Test Method C1161, and Refs (1-3).4 Specific fixture and specimen configurations were designated in order to permit the ready comparison of data without the need for Weibull size scaling.  
4.4 The flexural strength of a ceramic material is dependent on both its inherent resistance to fracture and the size and severity of flaws. Variations in these cause a natural scatter in test results for a sample of test specimens. Fractographic analysis of fracture surfaces, although beyond the scope of this test method, is highly recommended for all purposes, especially if the data will be used for design as discussed in Ref (4) and Practices C1322 and C1239.  
4.5 This method determines the flexural strength at elevated temperature and ambient environmental conditions at a nominal, moderately fast testing rate. The flexural strength under these conditions may or may not necessarily be the...
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1.1 This test method covers determination of the flexural strength of advanced ceramics at elevated temperatures.2 Four-point-1/4-point and three-point loadings with prescribed spans are the standard as shown in Fig. 1. Rectangular specimens of prescribed cross-section are used with specified features in prescribed specimen-fixture combinations. Test specimens may be 3 by 4 by 45 to 50 mm in size that are tested on 40-mm outer span four-point or three-point fixtures. Alternatively, test specimens and fixture spans half or twice these sizes may be used. The test method permits testing of machined or as-fired test specimens. Several options for machining preparation are included: application matched machining, customary procedures, or a specified standard procedure. This test method describes the apparatus, specimen requirements, test procedure, calculations, and reporting requirements. The test method is applicable to monolithic or particulate- or whisker-reinforced ceramics. It may also be used for glasses. It is not applicable to continuous fiber-reinforced ceramic composites.  
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM C1323-22(Test Method)
Standard Test Method for Ultimate Strength of Advanced Ceramics with Diametrally Compressed C-Ring Specimens at Ambient Temperature

SIGNIFICANCE AND USE
4.1 This test method may be used for material development, material comparison, quality assurance, and characterization. Extreme care should be exercised when generating design data.  
4.2 For a C-ring under diametral compression, the maximum tensile stress occurs at the outer surface. Hence, the C-ring specimen loaded in compression will predominately evaluate the strength distribution and flaw population(s) on the external surface of a tubular component in the hoop direction. Accordingly, the condition of the inner surface may be of lesser consequence in specimen preparation and testing.
Note 1: A C-ring in tension or an O-ring in compression may be used to evaluate the internal surface.  
4.2.1 The flexure stress is computed based on simple curved beam theory (1-5).3 It is assumed that the material is isotropic and homogeneous, the moduli of elasticity are identical in compression or tension, and the material is linearly elastic. These homogeneity and isotropy assumptions preclude the use of this standard for continuous fiber reinforced composites. Average grain size(s) should be no greater than one fiftieth (1/50 ) of the C-ring thickness. The curved beam stress solution from engineering mechanics is in good agreement (within 2 %) with an elasticity solution as discussed in (6) for the test specimen geometries recommended for this standard. The curved beam stress equations are simple and straightforward, and therefore it is relatively easy to integrate the equations for calculations for effective area or effective volume for Weibull analyses as discussed in Appendix X1.  
4.2.2 The simple curved beam and theory of elasticity stress solutions both are two-dimensional plane stress solutions. They do not account for stresses in the axial (parallel to b) direction, or variations in the circumferential (hoop, σθ) stresses through the width (b) of the test piece. The variations in the circumferential stresses increase with increases in width (b) and ring thicknes...
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1.1 This test method covers the determination of ultimate strength under monotonic loading of advanced ceramics in tubular form at ambient temperatures. The ultimate strength as used in this test method refers to the strength obtained under monotonic compressive loading of C-ring specimens such as shown in Fig. 1, where monotonic refers to a continuous nonstop test rate with no reversals from test initiation to final fracture. This method permits a range of sizes and shapes since test specimens may be prepared from a variety of tubular structures. The method may be used with microminiature test specimens.
FIG. 1 C-Ring Test Geometry with Defining Geometry and Reference Angle (θ) for the Point of Fracture Initiation on the Circumference  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.2.1 Values expressed in this test method are in accordance with the International System of Units (SI) and IEEE/ASTM SI 10.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM C1292-22(Test Method)
Standard Test Method for Shear Strength of Continuous Fiber-Reinforced Advanced Ceramics at Ambient Temperatures

SIGNIFICANCE AND USE
5.1 Continuous fiber-reinforced ceramic composites can be candidate materials for structural applications requiring high degrees of wear and corrosion resistance, and damage tolerance at high temperatures.  
5.2 Shear tests provide information on the strength and deformation of materials under shear stresses.  
5.3 This test method may be used for material development, material comparison, quality assurance, characterization, and design data generation.  
5.4 For quality control purposes, results derived from standardized shear test specimens may be considered indicative of the response of the material from which they were taken for given primary processing conditions and post-processing heat treatments.
SCOPE
1.1 This test method covers the determination of shear strength of continuous fiber-reinforced ceramic composites (CFCCs) at ambient temperature. The test methods addressed are (1) the compression of a double-notched test specimen to determine interlaminar shear strength, and (2) the Iosipescu test method to determine the shear strength in any one of the material planes of laminated composites. Test specimen fabrication methods, testing modes (load or displacement control), testing rates (load rate or displacement rate), data collection, and reporting procedures are addressed.  
1.2 This test method is used for testing advanced ceramic or glass matrix composites with continuous fiber reinforcement having unidirectional (1D) or bidirectional (2D) fiber architecture. This test method does not address composites with 3D fiber architecture or discontinuous fiber-reinforced, whisker-reinforced, or particulate-reinforced ceramics.  
1.3 The values stated in SI units are to be regarded as the standard and are in accordance with IEEE/ASTM SI 10.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific hazard statements are given in 8.1 and 8.2.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM C1469-22(Test Method)
Standard Test Method for Shear Strength of Joints of Advanced Ceramics at Ambient Temperature

SIGNIFICANCE AND USE
5.1 Advanced ceramics can be candidate materials for structural applications requiring high degrees of wear and corrosion resistance, often at elevated temperatures.  
5.2 Joints are produced to enhance the performance and applicability of materials. While the joints between similar materials are generally made for manufacturing complex parts and repairing components, those involving dissimilar materials usually are produced to exploit the unique properties of each constituent in the new component. Depending on the joining process, the joint region may be the weakest part of the component. Since under mixed-mode and shear loading the load transfer across the joint requires reasonable shear strength, it is important that the quality and integrity of joint under in-plane shear forces be quantified. Shear strength data are also needed to monitor the development of new and improved joining techniques.  
5.3 Shear tests provide information on the strength and deformation of materials under shear stresses.  
5.4 This test method may be used for material development, material comparison, quality assurance, characterization, and design data generation.  
5.5 For quality control purposes, results derived from standardized shear test specimens may be considered indicative of the response of the material from which they were taken for given primary processing conditions and post-processing heat treatments.
SCOPE
1.1 This test method covers the determination of shear strength of joints in advanced ceramics at ambient temperature using asymmetrical four-point flexure. Test specimen geometries, test specimen fabrication methods, testing modes (that is, force or displacement control), testing rates (that is, force or displacement rate), data collection, and reporting procedures are addressed.  
1.2 This test method is used to measure shear strength of ceramic joints in test specimens extracted from larger joined pieces by machining. Test specimens fabricated in this way are not expected to warp due to the relaxation of residual stresses but are expected to be much straighter and more uniform dimensionally than butt-jointed test specimens prepared by joining two halves, which is not recommended. In addition, this test method is intended for joints, which have either low or intermediate strengths with respect to the substrate material to be joined. Joints with high strengths should not be tested by this test method because of the high probability of invalid tests resulting from fractures initiating at the reaction points rather than in the joint. Determination of the shear strength of joints using this test method is appropriate particularly for advanced ceramic matrix composite materials but also may be useful for monolithic advanced ceramic materials.  
1.3 Values expressed in this test method are in accordance with the International System of Units (SI) and IEEE/ASTM SI 10.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are noted in 8.1.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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