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ASTM D8066/D8066M-17

(Practice)

Standard Practice Unnotched Compression Testing of Polymer Matrix Composite Laminates

Standard Practice Unnotched Compression Testing of Polymer Matrix Composite Laminates

SIGNIFICANCE AND USE
5.1 This practice provides supplemental instructions for the use of Test Method D6484/D6484M to determine unnotched compressive strength data for material specifications, research and development, material design allowables, and quality assurance. Factors that influence compressive strengths and shall therefore be reported include the following: material, methods of material fabrication, accuracy of lay-up, laminate stacking sequence and overall thickness, specimen preparation, specimen conditioning, environment of testing, specimen alignment and gripping, speed of testing, time at temperature, void content, and volume percent reinforcement. Composite properties in the test direction that may be obtained from this test method include:  
5.1.1 Unnotched compressive (UNC) strength, Fxunc,  
5.1.2 Ultimate compressive strain,  
5.1.3 Compressive (linear or chord) modulus of elasticity, Ec, and  
5.1.4 Poisson's ratio in compression.  
5.2 This practice provides a compression test method for laminates containing fibers in multiple fiber directions, particularly those combining axial (0 degree) fibers and off-axis (± θ degree) fibers. Other compression strength test methods include SACMA SRM-1 (also known as the modified D695), D3410/D3410M, D5467/D5467M, D6641/D6641M, and D7249/D7249M. The SRM-1 test uses 12.6 mm [0.50 in.] wide specimens, which is only appropriate for unidirectional tape, cross-ply [0/90]ns tape, or small unit-cell-size fabrics (e.g. 3K-70-P). Larger cell-size fabrics (e.g., spread-tow 12K fabrics) should be tested with wider specimens. The standard D3410/D3410M and D6641/D6641M test fixtures do permit the use of wider specimens, e.g., 25.4 mm [1.0 in.] wide, and thus can be used to test laminates containing both axial and off-axis fibers; however their gage lengths are relatively short. Test Method D5467/D5467M is intended to obtain the compressive strength of unidirectional laminates, but is expensive due to the sandwich beam configuration. Test...
SCOPE
1.1 This practice provides instructions for using the Test Method D6484 open hole compression test fixture to determine unnotched compressive strength of multi-directional laminates. The composite material forms are limited to continuous-fiber reinforced polymer matrix composites in which the laminate is both symmetric and balanced with respect to the test direction. The range of acceptable test laminates and thicknesses are described in 8.2.1.  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.  
1.2.1 Within the text the inch-pound units are shown in brackets.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Historical
Publication Date
31-Jul-2017
ICS
83.140.20 - Laminated sheets
Technical Committee
D30 - Composite Materials
Drafting Committee
D30.05 - Structural Test Methods
Current Stage
Ref Project

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ASTM D8066/D8066M-17 - Standard Practice Unnotched Compression Testing of Polymer Matrix Composite LaminatesASTM D8066/D8066M-17 - Standard Practice Unnotched Compression Testing of Polymer Matrix Composite Laminates
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ASTM D8066/D8066M-17 - Standard Practice Unnotched Compression Testing of Polymer Matrix Composite Laminates
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D8066/D8066M − 17
Standard Practice
Unnotched Compression Testing of Polymer Matrix
1
Composite Laminates
This standard is issued under the fixed designation D8066/D8066M; the number immediately following the designation indicates the
year of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last
reapproval. A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D3410/D3410M Test Method for Compressive Properties of
Polymer Matrix Composite Materials with Unsupported
1.1 This practice provides instructions for using the Test
Gage Section by Shear Loading
Method D6484 open hole compression test fixture to determine
D3171 Test Methods for Constituent Content of Composite
unnotched compressive strength of multi-directional laminates.
Materials
The composite material forms are limited to continuous-fiber
D3878 Terminology for Composite Materials
reinforced polymer matrix composites in which the laminate is
D5229/D5229M Test Method for Moisture Absorption Prop-
both symmetric and balanced with respect to the test direction.
erties and Equilibrium Conditioning of Polymer Matrix
The range of acceptable test laminates and thicknesses are
Composite Materials
described in 8.2.1.
D5467/D5467M Test Method for Compressive Properties of
1.2 The values stated in either SI units or inch-pound units
Unidirectional Polymer Matrix Composite Materials Us-
are to be regarded separately as standard. The values stated in
ing a Sandwich Beam
each system may not be exact equivalents; therefore, each
D6484/D6484M Test Method for Open-Hole Compressive
system shall be used independently of the other. Combining
Strength of Polymer Matrix Composite Laminates
values from the two systems may result in non-conformance
D6507 Practice for Fiber Reinforcement Orientation Codes
with the standard.
for Composite Materials
1.2.1 Within the text the inch-pound units are shown in
D6641/D6641M Test Method for Compressive Properties of
brackets.
Polymer Matrix Composite Materials Using a Combined
1.3 This standard does not purport to address all of the Loading Compression (CLC) Test Fixture
safety concerns, if any, associated with its use. It is the
D7249/D7249M Test Method for Facing Properties of Sand-
responsibility of the user of this standard to establish appro-
wich Constructions by Long Beam Flexure
priate safety, health and environmental practices and deter- E6 Terminology Relating to Methods of Mechanical Testing
mine the applicability of regulatory limitations prior to use.
E132 Test Method for Poisson’s Ratio at Room Temperature
1.4 This international standard was developed in accor- E177 Practice for Use of the Terms Precision and Bias in
dance with internationally recognized principles on standard-
ASTM Test Methods
ization established in the Decision on Principles for the E456 Terminology Relating to Quality and Statistics
Development of International Standards, Guides and Recom-
3. Terminology
mendations issued by the World Trade Organization Technical
Barriers to Trade (TBT) Committee.
3.1 Definitions—Terminology D3878 defines terms relating
to high-modulus fibers and their composites, as well as terms
2. Referenced Documents
relating to structural sandwich constructions. Terminology
D883 defines terms relating to plastics. Terminology E6 defines
2.1 ASTM Standards:
terms relating to mechanical testing. Terminology E456 and
D695 Test Method for Compressive Properties of Rigid
Practice E177 define terms relating to statistics. In the event of
Plastics
a conflict between terms, Terminology D3878 shall have
D792 Test Methods for Density and Specific Gravity (Rela-
precedence over the other standards.
tive Density) of Plastics by Displacement
D883 Terminology Relating to Plastics
3.2 Definitions of Terms Specific to This Standard—
NOTE 1—If the term represents a physical quantity, its analytical
1
dimensions are stated immediately following the term (or letter symbol) in
This test method is under the jurisdiction of ASTM Committee D30 on
fundamental dimension form, using the following ASTM International
Composite Materials and is the direct responsibility of Subcommittee D30.05 on
standard symbology for fundamental dimensions, shown within square
Structural Test Methods.
brackets: [M] for mass, [L] for length, [T] for time, [θ] for thermodynamic
Current edition approved Aug. 1, 2017. Published September 2017. DOI:
10.1520/D8066_D8066M-17. temperature, and [nd] for non-dimensional quantities. Use of these
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D8066/D8066M − 17
symbols is restricted to analytical dimensions when use
...

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Standard Practice Unnotched Compression Testing of Polymer Matrix Composite Laminates

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5.1 This practice provides supplemental instructions for the use of Test Method D6484/D6484M to determine unnotched compressive strength data for material specifications, research and development, material design allowables, and quality assurance. Factors that influence compressive strengths and shall therefore be reported include the following: material, methods of material fabrication, accuracy of lay-up, laminate stacking sequence and overall thickness, specimen preparation, specimen conditioning, environment of testing, specimen alignment and gripping, speed of testing, time at temperature, void content, and volume percent reinforcement. Composite properties in the test direction that may be obtained from this test method include:  
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5.2 This practice provides a compression test method for laminates containing fibers in multiple fiber directions, particularly those combining axial (0 degree) fibers and off-axis (± θ degree) fibers. Other compression strength test methods include SACMA SRM-1 (also known as the modified D695), D3410/D3410M, D5467/D5467M, D6641/D6641M, and D7249/D7249M. The SRM-1 test uses 12.6 mm [0.50 in.] wide specimens, which is only appropriate for unidirectional tape, cross-ply [0/90]ns tape, or small unit-cell-size fabrics (e.g. 3K-70-P). Larger cell-size fabrics (for example, spread-tow 12K fabrics) should be tested with wider specimens. The standard D3410/D3410M and D6641/D6641M test fixtures do permit the use of wider specimens, for example, 25.4 mm [1.0 in.] wide, and thus can be used to test laminates containing both axial and off-axis fibers; however their gage lengths are relatively short. Test Method D5467/D5467M is intended to obtain the compressive strength of unidirectional laminates, but is expensive due to the sandwich beam confi...
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1.1 This test practice defines the procedure for determination of the tensile strength of a tapered or stepped joint of polymer matrix composite materials. It is applicable to secondary bonded or co-bonded laminates with either unidirectional plies or woven fabric reinforcements. The materials to be bonded may be different material systems. In the bondline, a separate adhesive material may or may not be used (example: adhesives may be used with a prepreg system or may not be used with a wet lay-up repair system). The range of acceptable test laminates and thicknesses is described in 8.2.1.  
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Standard Test Method for Short-Beam Strength of Polymer Matrix Composite Materials and Their Laminates

SIGNIFICANCE AND USE
5.1 In most cases, because of the complexity of internal stresses and the variety of failure modes that can occur in this specimen, it is not generally possible to relate the short-beam strength to any one material property. However, failures are normally dominated by resin and interlaminar properties, and the test results have been found to be repeatable for a given specimen geometry, material system, and stacking sequence  (4).  
5.2 Short-beam strength determined by this test method can be used for quality control and process specification purposes. It can also be used for comparative testing of composite materials, provided that failures occur consistently in the same mode (5) .  
5.3 This test method is not limited to specimens within the range specified in Section 8, but is limited to the use of a loading span length-to-specimen thickness ratio of 4.0 and a minimum specimen thickness of 2.0 mm [0.08 in.].
SCOPE
1.1 This test method determines the short-beam strength of high-modulus fiber-reinforced composite materials. The specimen is a short beam machined from a curved or a flat laminate up to 6.00 mm [0.25 in.] thick. The beam is loaded in three-point bending.  
1.2 Application of this test method is limited to continuous- or discontinuous-fiber-reinforced polymer matrix composites, for which the elastic properties are balanced and symmetric with respect to the longitudinal axis of the beam.  
1.3 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.3.1 Within the text, the inch-pound units are shown in brackets.  
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Standard Test Method for Transverse Compressive Properties of Hoop Wound Polymer Matrix Composite Cylinders

SIGNIFICANCE AND USE
5.1 This test method is designed to produce transverse compressive property data for material specifications, research and development, quality assurance, and structural design and analysis. Factors that influence the transverse compressive response and should therefore be reported are: material, method of material preparation, specimen preparation, specimen conditioning, environment of testing, specimen alignment and gripping, speed of testing, void content, and fiber volume fraction. Properties in the test direction that may be obtained from this test method are:  
5.1.1 Transverse compressive strength, σ22uc,  
5.1.2 Transverse compressive strain at failure, ε22uc,  
5.1.3 Transverse compressive modulus of elasticity, E22, and  
5.1.4 Poisson's ratio, γ21.
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1.1 This test method determines the transverse compressive properties of wound polymer matrix composites reinforced by high-modulus continuous fibers. It describes testing of hoop wound (90°) cylinders in axial compression for determination of transverse compressive properties.  
1.2 The technical content of this test method has been stable since 1993 without significant objection from its stakeholders. As there is limited technical support for the maintenance of this test method, changes since that date have been limited to items required to retain consistency with other ASTM D30 Committee standards, including editorial changes and incorporation of updated guidance on specimen preconditioning and environmental testing. The test method, therefore, should not be considered to include any significant changes in approach and practice since 1993. Future maintenance of the test method will only be in response to specific requests and performed only as technical support allows.  
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ASTM D5450/D5450M-22(Test Method)
Standard Test Method for Transverse Tensile Properties of Hoop Wound Polymer Matrix Composite Cylinders

SIGNIFICANCE AND USE
5.1 This test method is used to produce transverse tensile property data for material specifications, research and development, quality assurance, and structural design and analysis. Factors which influence the transverse tensile response and should, therefore, be reported are: material, methods of material preparation, specimen preparation, specimen conditioning, environment of testing, specimen alignment and gripping, speed of testing, void content, and fiber volume fraction. Properties, in the test direction, which may be obtained from this test method include:  
5.1.1 Transverse Tensile Strength,    
5.1.2 Transverse Tensile Strain at Failure,    
5.1.3 Transverse Tensile Modulus of Elasticity,  E22, and  
5.1.4 Poisson's Ratio,  υ21.
SCOPE
1.1 This test method determines the transverse tensile properties of wound polymer matrix composites reinforced by high-modulus continuous fibers. It describes testing of hoop wound (90°) cylinders in axial tension for determination of transverse tensile properties.  
1.2 The technical content of this test method has been stable since 1993 without significant objection from its stakeholders. As there is limited technical support for the maintenance of this test method, changes since that date have been limited to items required to retain consistency with other ASTM D30 Committee standards, including editorial changes and incorporation of updated guidance on specimen preconditioning and environmental testing. The test method, therefore, should not be considered to include any significant changes in approach and practice since 1993. Future maintenance of the test method will only be in response to specific requests and performed only as technical support allows.  
1.3 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.3.1 Within the text, the inch-pound units are shown in brackets.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM E1922/E1922M-22(Test Method)
Standard Test Method for Translaminar Fracture Toughness of Laminated and Pultruded Polymer Matrix Composite Materials

SIGNIFICANCE AND USE
5.1 The parameter KTL  determined by this test method is a measure of the resistance of a polymer matrix composite laminate to notch-tip damage and effective translaminar crack growth under opening mode loading. The result is valid only for conditions in which the damage zone at the notch tip is small compared with the notch length and the in-plane specimen dimensions. Alternately, for materials exhibiting distributed damage in a larger volume, observed force-displacement and discrete damage events are still valid structural responses for certain specific engineering applications.  
5.2 This test method can serve the following purposes. In research and development, (a) KTL data can quantitatively establish the effects of fiber and matrix variables and stacking sequence of the laminate on the translaminar fracture resistance of composite laminates; and (b) quantified distributed damage measurements can be used to validate progressive composite damage models. In structural design, KTL data can, within the constraints of the specimen geometry and loading, be used to assess composite laminate resistance to damage growth from edge flaws and notches.  
5.3 The translaminar fracture toughness,  KTL, as well as distributed damage observations, determined by this test method may be a function of the testing speed and temperature. This test method is intended for room temperature and quasi-static conditions, but it can apply to other test conditions provided that the requirements of 13.2 and 13.3 are met. Application of KTL in the design of service components should be made with awareness that the test parameters specified by this test may differ from service conditions, possibly resulting in a different material response than that seen in service. Distributed damage observations are also limited to the material and geometry tested, but may be more generally applied to a variety of structural analysis validation applications.  
5.4 Not all types of laminated polymer matrix...
SCOPE
1.1 This test method covers the determination of translaminar fracture toughness, KTL, for laminated, molded, or pultruded polymer matrix composite materials of various fiber orientations using test results from monotonically loaded notched specimens. If the material response is such that the KTL calculation is not valid, alternate reporting methods are provided.  
1.2 This test method is applicable to room temperature laboratory air environments.  
1.3 Composite materials that can be tested by this test method are not limited by thickness or by type of polymer matrix or fiber, provided that the specimen sizes and the test results meet the requirements of this test method. This test method was developed primarily from test results of various carbon fiber – epoxy matrix laminates and from additional results of glass fiber – epoxy matrix, glass fiber-polyester matrix pultrusions and carbon fiber – bismaleimide matrix laminates (1-4, 5, 6).2  
1.4 A range of eccentrically loaded, single-edge-notch tension, ESE(T), specimen sizes with proportional planar dimensions is provided, but planar size may be variable and adjusted, with associated changes in the applied test load. Specimen thickness is a variable, independent of planar size.  
1.5 Specimen configurations other than those contained in this test method may be used. It is particularly important that the requirements discussed in 5.1 and 5.4 regarding contained notch-tip damage be met when using alternative specimen configurations in conjunction with the KTL calculation.  
1.6 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.6.1 Within the text, the inch-pound units are shown ...

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