ASTM D850-18

Standard Test Method for Distillation of Industrial Aromatic Hydrocarbons and Related Materials

SIGNIFICANCE AND USE
5.1 This test method is suitable for setting specifications, for use as an internal quality control tool, and for use in development or research work on industrial aromatic hydrocarbons and related materials.  
5.2 This test method gives a broad indication of general purity and can also indicate presence of excessive moisture. It will not differentiate between products of similar boiling range.
SCOPE
1.1 This test method covers the distillation of industrial aromatic hydrocarbons and related materials of relatively narrow boiling ranges from 30 to 250°C.  
1.2 The following applies to all specified limits in this test method: for the purposes of determining conformance to this test method, an observed or calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29.  
1.3 Warning—Mercury has been designated by EPA and many state agencies as a hazardous material that can cause central nervous system, kidney and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for details and EPA’s website (http://www.epa.gov/mercury/faq.htm) for additional information. Users should be aware that selling mercury or mercury-containing products, or both, in your state may be prohibited by state law.  
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see 6.5.2, 6.6.1 and Section 7.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

• Status: Historical
• Publication Date: 31-May-2018
• ICS: 75.140 - Waxes, bituminous materials and other petroleum products
• Technical Committee: D16 - Aromatic, Industrial, Specialty and Related Chemicals
• Drafting Committee: D16.04 - Instrumental Analysis

Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D850 − 18
Standard Test Method for
Distillation of Industrial Aromatic Hydrocarbons and Related
1
Materials
This standard is issued under the fixed designation D850; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope* Development of International Standards, Guides and Recom-
mendations issued by the World Trade Organization Technical
1.1 This test method covers the distillation of industrial
Barriers to Trade (TBT) Committee.
aromatic hydrocarbons and related materials of relatively
narrow boiling ranges from 30 to 250°C.
2. Referenced Documents
2
1.2 The following applies to all specified limits in this test
2.1 ASTM Standards:
method: for the purposes of determining conformance to this
D1078 Test Method for Distillation Range of Volatile Or-
test method, an observed or calculated value shall be rounded
ganic Liquids
off “to the nearest unit” in the last right-hand digit used in
D3437 Practice for Sampling and Handling Liquid Cyclic
expressing the specification limit, in accordance with the
Products
rounding-off method of Practice E29.
D4790 Terminology ofAromatic Hydrocarbons and Related
Chemicals
1.3 Warning—Mercury has been designated by EPA and
D6809 Guide for Quality Control and Quality Assurance
many state agencies as a hazardous material that can cause
Procedures for Aromatic Hydrocarbons and Related Ma-
central nervous system, kidney and liver damage. Mercury, or
terials
its vapor, may be hazardous to health and corrosive to
E1 Specification for ASTM Liquid-in-Glass Thermometers
materials.Cautionshouldbetakenwhenhandlingmercuryand
E29 Practice for Using Significant Digits in Test Data to
mercury-containing products. See the applicable product
Determine Conformance with Specifications
Safety Data Sheet (SDS) for details and EPA’s website (http://
E133 Specification for Distillation Equipment
www.epa.gov/mercury/faq.htm) for additional information.
E220 Test Method for Calibration of Thermocouples By
Users should be aware that selling mercury or mercury-
Comparison Techniques
containingproducts,orboth,inyourstatemaybeprohibitedby
E691 Practice for Conducting an Interlaboratory Study to
state law.
Determine the Precision of a Test Method
1.4 The values stated in SI units are to be regarded as
2.2 Other Document:
standard. No other units of measurement are included in this
OSHA Regulations, 29 CFR paragraphs 1910.1000 and
standard.
3
1910.1200
1.5 This standard does not purport to address all of the
3. Terminology
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appro-
3.1 Definitions:
priate safety, health, and environmental practices and deter-
3.1.1 See Terminology D4790 for definitions of terms used
mine the applicability of regulatory limitations prior to use.
in this test method.
For specific hazard statements, see 6.5.2, 6.6.1 and Section 7.
4. Summary of Test Method
1.6 This international standard was developed in accor-
dance with internationally recognized principles on standard-
4.1 The distillation of a 100-mL sample of industrial aro-
ization established in the Decision on Principles for the
matic hydrocarbons and related materials is carried out via a
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
1
This test method is under the jurisdiction of ASTM Committee D16 on contact ASTM Customer Service at [e-mail]. For Annual Book of ASTM
Aromatic, Industrial, Specialty and Related Chemicals and is the direct responsi- Standards volume information, refer to the standard’s Document Summary page on
bility of Subcommittee D16.04 on Instrumental Analysis. the ASTM website.
3
Current edition approved June 1, 2018. Published June 2018. Originally AvailablefromU.S.GovernmentPrintingOfficeSuperintendentofDocuments,
approved in 1945. Last previous edition approved in 2016 as D850 – 16. DOI: 732 N. Capitol St., NW, Mail Stop: SDE, Washington, DC 20401, http://
10.1520/D0850-18. www.access.gpo.gov.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D850 − 18
TABLE 1 ASTM Thermometers for Distillation Test of Industrial
carefully controlled distillation wherein temperature readings
Aromatic Hydrocarbons
are noted for the first drop of distillate and when 5, 10, and
ASTM
each additional 10 up to 90, and 95 % of the s
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D850 − 16 D850 − 18
Standard Test Method for
Distillation of Industrial Aromatic Hydrocarbons and Related
1
Materials
This standard is issued under the fixed designation D850; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the U.S. Department of Defense.
1. Scope*
1.1 This test method covers the distillation of industrial aromatic hydrocarbons and related materials of relatively narrow boiling
ranges from 30 to 250°C.
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.2 The following applies to all specified limits in this test method: for the purposes of determining conformance to this test
method, an observed or calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing
the specification limit, in accordance with the rounding-off method of Practice E29.
1.3 Warning—Mercury has been designated by EPA and many state agencies as a hazardous material that can cause central
nervous system, kidney and liver damage. Mercury, or its vapor, may be hazardous to health and corrosive to materials. Caution
should be taken when handling mercury and mercury-containing products. See the applicable product Safety Data Sheet (SDS) for
details and EPA’s website (http://www.epa.gov/mercury/faq.htm) for additional information. Users should be aware that selling
mercury or mercury-containing products, or both, in your state may be prohibited by state law.
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety safety, health, and healthenvironmental practices and determine the
applicability of regulatory limitations prior to use. For specific hazard statements, see 6.5.2, 6.6.1 and Section 7.
1.6 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
D1078 Test Method for Distillation Range of Volatile Organic Liquids
D3437 Practice for Sampling and Handling Liquid Cyclic Products
D4790 Terminology of Aromatic Hydrocarbons and Related Chemicals
D6809 Guide for Quality Control and Quality Assurance Procedures for Aromatic Hydrocarbons and Related Materials
E1 Specification for ASTM Liquid-in-Glass Thermometers
E29 Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
E133 Specification for Distillation Equipment
E220 Test Method for Calibration of Thermocouples By Comparison Techniques
E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
1
This test method is under the jurisdiction of ASTM Committee D16 on Aromatic Hydrocarbons Aromatic, Industrial, Specialty and Related Chemicals and is the direct
responsibility of Subcommittee D16.04 on Instrumental Analysis.
Current edition approved June 1, 2016June 1, 2018. Published July 2016June 2018. Originally approved in 1945. Last previous edition approved in 20112016 as
D850 – 11.D850 – 16. DOI: 10.1520/D0850-16.10.1520/D0850-18.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at [e-mail]. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D850 − 18
2.2 Other Document:
3
OSHA Regulations, 29 CFR paragraphs 1910.1000 and 1910.1200
3. Terminology
3.1 Definitions:
3.1.1 See Terminology D4790 for definitions of terms used in this test method.
4. Summary of Test Method
4.1 The distillation of a 100-mL samp
...