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ASTM D3270-00

(Test Method)

Standard Test Methods for Analysis for Fluoride Content of the Atmosphere and Plant Tissues (Semiautomated Method)

Standard Test Methods for Analysis for Fluoride Content of the Atmosphere and Plant Tissues (Semiautomated Method)

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1.1 These test methods describe the semiautomated procedure for the analyses of various types of samples for the purpose of determining total fluoride. Since the test methods incorporate microdistillation of the sample, they may be applied to any fluoride-containing solution where standards of identical composition have been carried through the same sample preparation procedures and have proven to provide quantitative recovery when analyzed by the semiautomated system. Conversely, the methods shall not be applied for analyses until the applicability has been demonstrated.
1.2 In normal use, the procedure can detect 0.1 [mu]g/mL of F. The normal range of analysis is from 0.1 to 1.6 [mu]g/mL of F. Higher concentrations can be analyzed by careful dilution of samples with reagent water. If digested samples routinely exceed 1.6 [mu]g/mL of F, the analytical portion of the pump manifold can be modified to reduce sensitivity. However, the best procedure is to analyze a smaller aliquot of the sample. Most accurate results are obtained when the fluoride concentration falls in the middle or upper part of the calibration curve.
1.3 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. See 8.3 for additional precautions.

General Information

Status
Historical
Publication Date
09-Mar-2000
ICS
13.040.20 - Ambient atmospheres
Technical Committee
D22 - Air Quality
Drafting Committee
D22.03 - Ambient Atmospheres and Source Emissions
Current Stage
Ref Project

Relations

Replaced By
ASTM D3270-00(2006) - Standard Test Methods for Analysis for Fluoride Content of the Atmosphere and Plant Tissues (Semiautomated Method)
Effective Date
01-Apr-2006
Referred By
ASTM D3266-91(2018) - Standard Test Method for Automated Separation and Collection of Particulate and Acidic Gaseous Fluoride in the Atmosphere (Double Paper Tape Sampler Method)
Effective Date
10-Mar-2000
Referred By
ASTM D3268-91(2018) - Standard Test Method for Separation and Collection of Particulate and Gaseous Fluorides in the Atmosphere (Sodium Bicarbonate-Coated Glass Tube and Particulate Filter Method)
Effective Date
10-Mar-2000
Referred By
ASTM D3267-20 - Standard Test Method for Separation and Collection of Particulate and Water-Soluble Gaseous Fluorides in the Atmosphere (Filter and Impinger Method)
Effective Date
10-Mar-2000

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ASTM D3270-00 - Standard Test Methods for Analysis for Fluoride Content of the Atmosphere and Plant Tissues (Semiautomated Method)ASTM D3270-00 - Standard Test Methods for Analysis for Fluoride Content of the Atmosphere and Plant Tissues (Semiautomated Method)
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ASTM D3270-00 - Standard Test Methods for Analysis for Fluoride Content of the Atmosphere and Plant Tissues (Semiautomated Method)
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D3270–00
Standard Test Methods for
Analysis for Fluoride Content of the Atmosphere and Plant
1
Tissues (Semiautomated Method)
This standard is issued under the fixed designation D3270; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope D3266 Test Method forAutomated Separation and Collec-
tion of Particulate and Acidic Gaseous Fluoride in the
1.1 These test methods describe the semiautomated proce-
3
Atmosphere (Double Paper Tape Sampler Method)
dure for the analyses of various types of samples for the
D3267 Test Method for Separation and Collection of Par-
purpose of determining total fluoride. Since the test methods
ticulate and Water-Soluble Gaseous Fluorides in the At-
incorporate microdistillation of the sample, they may be
3
mosphere (Filter and Impinger Method)
applied to any fluoride-containing solution where standards of
D3268 Test Method for Separation and Collection of Par-
identical composition have been carried through the same
ticulateandGaseousFluoridesintheAtmosphere(Sodium
sample preparation procedures and have proven to provide
Bicarbonate-Coated Glass Tube and Particulate Filter
quantitative recovery when analyzed by the semiautomated
3
Method)
system. Conversely, the methods shall not be applied for
D3269 Test Methods for Analysis for Fluoride Content of
analyses until the applicability has been demonstrated.
3
the Atmosphere and Plant Tissues (Manual Procedures)
1.2 In normal use, the procedure can detect 0.1 µg/mLof F.
D3614 Guide for Laboratories Engaged in Sampling and
The normal range of analysis is from 0.1 to 1.6 µg/mL of F.
3
Analysis of Atmospheres and Emissions
Higher concentrations can be analyzed by careful dilution of
samples with reagent water. If digested samples routinely
3. Terminology
exceed 1.6 µg/mL of F, the analytical portion of the pump
3.1 Definitions—For definitions of terms used in these
manifold can be modified to reduce sensitivity. However, the
methods, see Terminology D1356.
best procedure is to analyze a smaller aliquot of the sample.
Most accurate results are obtained when the fluoride concen-
4. Summary of Test Methods
trationfallsinthemiddleorupperpartofthecalibrationcurve.
4.1 These semiautomated methods are based on the distil-
1.3 The values stated in SI units are to be regarded as the
lation of hydrogen fluoride (HF) from the sample and subse-
standard. The values given in parentheses are for information
quent reaction of the distillate with alizarin fluorine blue-
only.
lanthanum nitrate reagent, to form a blue complex which is
1.4 This standard does not purport to address all of the
4
measured colorimetrically at 624 nm (1) , or the subsequent
safety concerns, if any, associated with its use. It is the
measurement with a specific ion probe.
responsibility of the user of this standard to establish appro-
4.2 General, Plant Material:
priate safety and health practices and determine the applica-
4.2.1 The plant material including leaf samples, washed or
bility of regulatory limitations prior to use.See8.3,10.2.4,and
unwashed, is dried, and ground, then dissolved with perchloric
10.2.5 for additional precautions.
acid and diluted to 50 mL with water. In the case of leaf
samples, an appreciable amount of fluoride may be deposited
2. Referenced Documents
on the external leaf surfaces. This fluoride behaves differently
2.1 ASTM Standards:
2 physiologically from fluoride absorbed into the leaf and it is
D1193 Specification for Reagent Water
oftendesirabletowashitfromthesurfaceasapreliminarystep
D1356 Terminology Relating to Sampling andAnalysis of
3 in the analysis. Details of a leaf-washing process are described
Atmospheres
in 9.1.
4.3 General, Atmospheric Samples:
4.3.1 Test Methods D3269 contains acceptable procedures
1
These test methods are under the jurisdiction of ASTM Committee D22 on and also techniques for the proper preparation of atmospheric
Sampling and Analysis of Atmospheres and are the direct responsibility of
samples. Test Methods D3266, D3267, and D3268 are
Subcommittee D22.03 on Ambient Atmospheres and Source Emissions.
Current edition approved March 10, 2000. Published May 2000. Originally
e1
published as D 3270 - 91. Last previous edition D 3270 - 91 (1995) .
2 4
Annual Book of ASTM Standards, Vol 11.01. The boldface numbers in parenthesis refer to the references at the end of this
3
Annual Book of ASTM Standards, Vol 11.03. method.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D3270–00
sampling
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1.5 The values stated in SI units are to be regarded as the standard.  
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SIGNIFICANCE AND USE
5.1 This practice establishes standardized tests for the performance evaluation of sensor-based continuous instruments for ambient air quality measurements. Public and private air monitoring interests have manifested themselves as a driving force for the deployment of air quality sensors and instruments to quantify air pollutant concentrations in communities, around schools, around industrial facilities, and elsewhere. Users of air quality sensors require information on the performance and limitations of these devices so that informed decisions regarding their suitability for various purposes can be determined. This practice describes both laboratory and field tests that provide information on candidate instrument repeatability, sensitivity, linearity, cross-interferences, drift and comparability with more costly instruments typically used by entities such as government agencies. The air quality sensors are first evaluated in a laboratory chamber by comparing their response to a reference instrument and challenging the gas sensors with interferents. The sensors are then deployed outdoors for field testing at two sites with different climates against reference air quality instruments. This practice is intended to be referenced in standards and codes that establish minimum performance quality for sensor-based ambient outdoor air monitoring.  
5.2 This practice is intended for air quality sensors that measure one or more of the criteria pollutants in ambient air (ozone, carbon monoxide, nitrogen dioxide, sulfur dioxide, PM10 and PM2.5) that can be operated in outdoor environments and can log a concentration reading. It is not intended for devices or transducers that require additional enclosures for deployment outdoors or post-processing to convert their output signal into a pollutant concentration reading.  
5.3 It is anticipated that the main users of this practice will be manufacturers, developers, and distributors of outdoor air quality sensors, air quality agenc...
SCOPE
1.1 This practice establishes standardized tests for the performance evaluation of sensor-based continuous instruments for ambient outdoor air quality measurements. It describes both laboratory and field tests that provide information on candidate sensor repeatability, sensitivity, linearity, cross-interferences, drift, and comparability against reference instruments.  
1.2 This practice does not apply to sensors or instruments that remotely measure atmospheric pollutants using open path, lidar, or imaging technology.  
1.3 The evaluation procedures contained in this practice are for sensors that alone or in combination measure outdoor criteria pollutants in ambient air: particulate matter (PM2.5 and PM10), sulfur dioxide (SO2), ozone (O3), carbon monoxide (CO), or nitrogen dioxide (NO2) at concentrations that are relevant to public health.  
1.4 Testing is to be performed by a competent entity able to demonstrate that it operates in conformity with internationally accepted test laboratory quality standards such as ISO/IEC 17025.  
1.5 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D2914-15(2022)(Test Method)
Standard Test Methods for Sulfur Dioxide Content of the Atmosphere (West-Gaeke Method)

SIGNIFICANCE AND USE
5.1 Sulfur dioxide is a major air pollutant, commonly formed by the combustion of sulfur-bearing fuels. The Environmental Protection Agency (EPA) has set primary and secondary air quality standards (7) that are designed to protect the public health and welfare.  
5.2 The Occupational Safety and Health Administration (OSHA) has promulgated exposure limits for sulfur dioxide in workplace atmospheres (8).  
5.3 These methods have been found satisfactory for measuring sulfur dioxide in ambient and workplace atmospheres over the ranges pertinent in 5.1 and 5.2.  
5.4 Method A has been designed to correspond to the EPA-Designated Reference Method (7) for the determination of sulfur dioxide.
SCOPE
1.1 These test methods cover the bubbler collection and colorimetric determination of sulfur dioxide (SO2) in the ambient or workplace atmosphere.  
1.2 These test methods are applicable for determining SO2 over the range from approximately 25 μg/m3 (0.01 ppm(v)) to 1000 μg/m3 (0.4 ppm(v)), corresponding to a solution concentration of 0.03 μg SO2/mL to 1.3 μg SO2/mL. Beer's law is followed through the working analytical range from 0.02 μg SO2/mL to 1.4 μg SO2/mL.  
1.3 The lower limit of detection is 0.075 μg SO2/mL (1),2 representing an air concentration of 25 μg SO2/m3 (0.01 ppm(v)) in a 30-min sample, or 13 μg SO2/m3 (0.005 ppm(v)) in a 24-h sample.  
1.4 These test methods incorporate sampling for periods between 30 min and 24 h.  
1.5 These test methods describe the determination of the collected (impinged) samples. A Method A and a Method B are described.  
1.6 Method A is preferred over Method B, as it gives the higher sensitivity, but it has a higher blank. Manual Method B is pH-dependent, but is more suitable with spectrometers having a spectral band width greater than 20 nm.
Note 1: These test methods are applicable at concentrations below 25 μg/m3 by sampling larger volumes of air if the absorption efficiency of the particular system is first determined, as described in Annex A4.
Note 2: Concentrations higher than 1000 μg/m3 can be determined by using smaller gas volumes, larger collection volumes, or by suitable dilution of the collected sample with absorbing solution prior to analysis.  
1.7 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.8 Warning—Mercury has been designated by many regulatory agencies as a hazardous material that can cause serious medical issues. Mercury, or its vapor, has been demonstrated to be hazardous to health and corrosive to materials. Caution should be taken when handling mercury and mercury containing products. See the applicable product Safety Data Sheet (SDS) for additional information. Users should be aware that selling mercury and/or mercury containing products into your state or country may be prohibited by law.  
1.9 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific precautionary statements, see 8.3.1, Section 9, and A3.1.3.  
1.10 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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