Standard Test Method for Viscosity and Gel Time of Chemical Grouts by Rotational Viscometer (Laboratory Method) (Withdrawn 2023)

SIGNIFICANCE AND USE
5.1 This test is intended for materials that will penetrate soil voids and rock fissures. Viscosity alone is not necessarily an exact index of grout penetrability.
SCOPE
1.1 This test method covers the determination of viscosity of catalyzed chemical grouts with a rotational viscometer (laboratory method), over the range from 1.0 mPa·s to 1000 mPa·s (1.0 to 1000 cP).  
1.2 All observed and calculated values shall conform to the guidelines for significant digits and rounding established in Practice D6026.  
1.2.1 The procedures used to specify how data are collected/recorded or calculated, in this standard are regarded as the industry standard. In addition, they are representative of the significant digits that generally should be retained. The procedures used do not consider material variation, purpose of obtaining the data, special purpose studies, or any consideratons for the user’s objectives; and it is common practice to increase or reduce significant digits of reported data to be commensurate with these considerations. It is beyond the scope of this standard to consider significant digits used in analysis methods for engineering design.  
1.3 The values stated in SI units are the standard. Other units provided in parentheses are for the convenience of the user.  
1.4 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
WITHDRAWN RATIONALE
This test method covers the determination of viscosity of catalyzed chemical grouts with a rotational viscometer (laboratory method), over the range from 1.0 mPa·s to 1000 mPa·s (1.0 to 1000 cP).
Formerly under the jurisdiction of Committee D18 on Soil and Rock, this test method was withdrawn in January 2023 in accordance with section 10.6.3 of the Regulations Governing ASTM Technical Committees, which requires that standards shall be updated by the end of the eighth year since the last approval date.

General Information

Status
Withdrawn
Publication Date
14-Jun-2014
Withdrawal Date
08-Jan-2023
Technical Committee
Drafting Committee
Current Stage
Ref Project

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ASTM D4016-14 - Standard Test Method for Viscosity and Gel Time of Chemical Grouts by Rotational Viscometer (Laboratory Method) (Withdrawn 2023)
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D4016 − 14
Standard Test Method for
Viscosity and Gel Time of Chemical Grouts by Rotational
1
Viscometer (Laboratory Method)
This standard is issued under the fixed designation D4016; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope* 2. Referenced Documents
2
2.1 ASTM Standards:
1.1 This test method covers the determination of viscosity
D653 Terminology Relating to Soil, Rock, and Contained
of catalyzed chemical grouts with a rotational viscometer
Fluids
(laboratory method), over the range from 1.0 mPa·s to 1000
D6026 Practice for Using Significant Digits in Geotechnical
mPa·s (1.0 to 1000 cP).
Data
1.2 All observed and calculated values shall conform to the
E1 Specification for ASTM Liquid-in-Glass Thermometers
guidelines for significant digits and rounding established in
E1142 Terminology Relating to Thermophysical Properties
Practice D6026.
3. Terminology
1.2.1 Theproceduresusedtospecifyhowdataarecollected/
3.1 For common definitions of terms used in this standard,
recorded or calculated, in this standard are regarded as the
refer to Terminologies D653 and E1142.
industry standard. In addition, they are representative of the
significant digits that generally should be retained. The proce-
4. Summary of Test Method
dures used do not consider material variation, purpose of
4.1 A rotating spindle is immersed in a container of cata-
obtaining the data, special purpose studies, or any considera-
lyzed chemical grout. The test specimen viscosity is obtained
tons for the user’s objectives; and it is common practice to
from the drag on the spindle exerted by the test specimen, and
increase or reduce significant digits of reported data to be
the rotational speed of the spindle.
commensuratewiththeseconsiderations.Itisbeyondthescope
of this standard to consider significant digits used in analysis
5. Significance and Use
methods for engineering design.
5.1 This test is intended for materials that will penetrate soil
1.3 The values stated in SI units are the standard. Other voids and rock fissures. Viscosity alone is not necessarily an
exact index of grout penetrability.
units provided in parentheses are for the convenience of the
user.
6. Apparatus
1.4 This standard does not purport to address all of the
6.1 Rotational Viscometer—The essential instrumentation
safety problems, if any, associated with its use. It is the
required providing the minimum rotational viscometer analyti-
responsibility of the user of this standard to establish appro-
cal capabilities for this method include:
priate safety and health practices and determine the applica-
6.1.1 A drive motor to apply a unidirectional rotational
bility of regulatory limitations prior to use.
displacement to the specimen at a rate from 0.3 revolutions per
1.5 This international standard was developed in accor-
minute (rev/min) to 60 rev/min constant to within 1 %.
dance with internationally recognized principles on standard-
6.1.2 Aforcesensor to measure the torque developed by the
ization established in the Decision on Principles for the specimen.
Development of International Standards, Guides and Recom- 6.1.3 A coupling shaft or other means to transmit the
rotational displacement from the motor to the specimen.
mendations issued by the World Trade Organization Technical
Barriers to Trade (TBT) Committee. 6.1.4 A geometry, spindle, tool or rotational element to fix
the specimen between the drive shaft and a stationary position
with a range of 1 mPa•s to 1000 mPa•s.
1
This test method is under the jurisdiction ofASTM Committee D18 on Soil and
2
Rock and is the direct responsibility of Subcommittee D18.16 on Grouting. For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Current edition approved June 15, 2014. Published July 2014. Originally contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
approved in 1981. Last previous edition approved in 2008 as D4016 – 08. DOI: Standards volume information, refer to the standard’s Document Summary page on
10.1520/D4016-14. the ASTM website.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

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D4016 − 14
NOTE 1—Each spindle typically covers a range of about 2 decades of
8.6 Record the viscosity (or torque and rotational speed)
viscosity.The spindle is selected so that the measured viscosity is between
every 60 seconds.
20 and 80 % of the range of the spindle.
NOTE 6—For material
...

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