ASTM D1337-96
(Test Method)Standard Test Method for Storage Life of Adhesives by Consistency and Bond Strength
Standard Test Method for Storage Life of Adhesives by Consistency and Bond Strength
SCOPE
1.1 This test method covers a means by which the storage life of an adhesive can be measured using rheological and adhesive performance testing.
1.2 The values stated in SI units are to be regarded as the standard. the values in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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Designation: D 1337 – 96
Standard Test Method for
Storage Life of Adhesives by Consistency and Bond
Strength
This standard is issued under the fixed designation D 1337; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope 4.2 This test method is intended to determine whether the
storage life conforms to the minimum specified storage life
1.1 This test method covers a means by which the storage
required of an adhesive by consistency tests (Procedure A) or
life of an adhesive can be measured using rheological and
by bond strength tests (Procedure B), or by both.
adhesive performance testing.
1.2 The values stated in SI units are to be regarded as the
PROCEDURE A—CONSISTENCY TEST
standard. The values in parentheses are for information only.
1.3 This standard does not purport to address all of the
5. Apparatus
safety concerns, if any, associated with its use. It is the
5.1 Viscometer—Any means of measuring the viscosity or
responsibility of the user of this standard to establish appro-
consistency of the adhesive is selected, provided that the
priate safety and health practices and determine the applica-
results are expressed in fundamental units.
bility of regulatory limitations prior to use.
5.2 Controlled-Temperature Chamber, capable of maintain-
ing temperature to 61.1°C (62°F), to provide temperature
2. Referenced Documents
storage conditions.
2.1 ASTM Standards:
D 618 Practice for Conditioning Plastics for Testing
6. Storage of Adhesive
D 897 Test Method for Tensile Properties of Adhesive
6.1 Store the adhesive and all its components, if there are
Bonds
any, in their original and unopened containers when the
D 906 Test Method for Strength Properties of Adhesives in
container is approximately quart (or litre) size. When the
Plywood Type Construction in Shear by Tension Loading
adhesive is supplied in larger containers, the desired number of
D 907 Terminology of Adhesives
samples is withdrawn from the large container. In this latter
D 1002 Test Method for Apparent Shear Strength of Single-
case, the size, type of closure, and nature (such as glass, steel,
Lap-Joint Adhesively Bonded Metal Specimens by Ten-
or tin-coated steel) of the small storage container is agreed
sion Loading (Metal-to-Metal)
upon by the purchaser and the manufacturer.
6.2 For storage temperature, use any one of the standard
3. Terminology
temperatures specified in Practice D 618. The time of storage is
3.1 Definitions—Many terms in this test method are defined
any time agreed upon by the purchaser and the manufacturer. If
in Terminology D 907.
the effect of storage time is desired, it is suggested that at least
three quantities of the adhesive be stored under the prescribed
4. Significance and Use
conditions, and tested at various intervals of time. Use a
4.1 This test method is applicable to all adhesives having a
separate, unopened container at each such test.
relatively short storage life.
7. Conditioning
1 7.1 Condition all containers after storage at 23 6 1°C (73.4
This test method is under the jurisdiction of ASTM Committee D-14 on
6 2°F) before opening. If the adhesive consists of two or more
Adhesives and is the direct responsibility of Subcommittee D14.10 on Working
Properties.
components, blend the components in accordance with the
Current edition effective Sept. 10, 1996. Published November 1996. Originally
instructions from the manufacturer, and again adjust the
published as D 1337 – 54. Last previous edition D 1337 – 91.
temperature to 23 6 1°C, if required.
Annual Book of ASTM Standards, Vol 08.01.
Annual Book of ASTM Standards, Vol 15.06.
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D 1337
8. Procedure 13. Preparation of Test Specimens
13.1 Prepare test panels or sheets for determining the bond
8.1 Measure the consistency on both the original adhesive
strength of the adhesive in accordance with any of the ASTM
as received, and on the adhesive after being subjected to
test methods suitable for the purpose. For example, the lap-type
storage. Test the adhesive in either its original container or after
shear specimens or the spool-type tension specimens such as
transferring into a more suitable container.
those described in
...
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