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ASTM D1337-04

(Test Method)

Standard Practice for Storage Life of Adhesives by Viscosity and Bond Strength

Standard Practice for Storage Life of Adhesives by Viscosity and Bond Strength

SIGNIFICANCE AND USE
This practice is applicable to all adhesives having a relatively short storage life.
This practice is intended to determine whether the storage life conforms to the minimum specified storage life required of an adhesive by viscosity tests (Procedure A) or by bond strength tests (Procedure B), or by both. It does so by providing results before and after a set of standard conditions that simulate storage life. The determination of what the requirements for percentage of the original property retained or the minimum value for a property is found in the relevant material specification, or as agreed between manufacturer and user. PROCEDURE A—VISCOSITY TEST   Top
SCOPE
1.1 This practice covers a means by which the storage life of an adhesive can be measured using viscosity and adhesive performance testing.
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
31-Mar-2004
ICS
83.180 - Adhesives
Technical Committee
D14 - Adhesives
Drafting Committee
D14.10 - Working Properties
Current Stage
Ref Project

Relations

Replaces
ASTM D1337-96 - Standard Test Method for Storage Life of Adhesives by Consistency and Bond Strength
Effective Date
01-Apr-2004
Replaced By
ASTM D1337-10 - Standard Practice for Storage Life of Adhesives by Viscosity and Bond Strength
Effective Date
01-Nov-2010
Referred By
ASTM D7799-12a(2021) - Standard Specification for Tufted and Woven Broadloom Carpet Adhesives Without Homogenous PVC or Non-PVC Backings
Effective Date
01-Apr-2004
Referred By
ASTM D8397-23 - Standard Specification for Acrylic and Reactive Adhesives for Installation of Vinyl and Rubber Floor Coverings
Effective Date
01-Apr-2004
Referred By
ASTM D8089-17 - Standard Practice for Accelerated Heat Aging for Floor Covering Adhesives
Effective Date
01-Apr-2004
Referred By
ASTM D6465-99(2016) - Standard Guide for Selecting Aerospace and General Purpose Adhesives and Sealants
Effective Date
01-Apr-2004

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ASTM D1337-04 - Standard Practice for Storage Life of Adhesives by Viscosity and Bond StrengthASTM D1337-04 - Standard Practice for Storage Life of Adhesives by Viscosity and Bond Strength
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ASTM D1337-04 - Standard Practice for Storage Life of Adhesives by Viscosity and Bond Strength
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D1337–04
Standard Practice for
1
Storage Life of Adhesives by Viscosity and Bond Strength
This standard is issued under the fixed designation D1337; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 4. Significance and Use
1.1 Thispracticecoversameansbywhichthestoragelifeof 4.1 This practice is applicable to all adhesives having a
an adhesive can be measured using viscosity and adhesive relatively short storage life.
performance testing. 4.2 This practice is intended to determine whether the
1.2 The values stated in SI units are to be regarded as the storage life conforms to the minimum specified storage life
standard. The values given in parentheses are for information required of an adhesive by viscosity tests (Procedure A) or by
only. bond strength tests (Procedure B), or by both. It does so by
1.3 This standard does not purport to address all of the providing results before and after a set of standard conditions
safety concerns, if any, associated with its use. It is the that simulate storage life. The determination of what the
responsibility of the user of this standard to establish appro- requirements for percentage of the original property retained or
priate safety and health practices and determine the applica- the minimum value for a property is found in the relevant
bility of regulatory limitations prior to use. material specification, or as agreed between manufacturer and
user.
2. Referenced Documents
2
PROCEDURE A—VISCOSITY TEST
2.1 ASTM Standards:
D618 Practice for Conditioning Plastics for Testing
5. Apparatus
D897 Test Method for Tensile Properties of Adhesive
5.1 Viscometer—Use the apparatus as described in Test
Bonds
Methods D1084, Method B.
D906 Test Method for Strength Properties of Adhesives in
5.2 Controlled-Temperature Chamber, capable of maintain-
Plywood Type Construction in Shear by Tension Loading
ing temperature to 63°C (65°F), to provide temperature
D907 Terminology of Adhesives
storage conditions.
D1002 Test Method for Apparent Shear Strength of Single-
Lap-Joint Adhesively Bonded Metal Specimens by Ten-
6. Storage of Adhesive
sion Loading (Metal-to-Metal)
6.1 Store the adhesive and all its components, if there are
D1084 Test Methods for Viscosity of Adhesives
any, in their original and unopened containers when the
3. Terminology container is approximately litre (or quart) size. When the
adhesive is supplied in larger containers, the desired number of
3.1 Definitions—Many terms in this practice are defined in
samples is withdrawn from the large container. In this latter
Terminology D907.
case, the size, type of closure, and nature (such as glass, steel,
or tin-coated steel) of the small storage container is agreed
upon by the purchaser and the manufacturer.
1
This practice is under the jurisdiction of ASTM Committee D14 on Adhesives
6.2 For storage temperature, use any one of the standard
and is the direct responsibility of Subcommittee D14.10 on Working Properties.
temperatures specified in Practice D618. The time of storage is
Current edition approved April 1, 2004. Published April 2004. Originally
any time agreed upon by the purchaser and the manufacturer. If
approved in 1954. Last previous edition approved in 1996 as D1337 – 96. DOI:
10.1520/D1337-04.
the effect of storage time is desired, it is suggested that at least
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
three quantities of the adhesive be stored under the prescribed
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
conditions, and tested at various intervals of time. Use a
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. separate, unopened container at each such test.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D1337–04
7. Conditioning 13. Preparation of Test Specimens
7.1 Condition all containers after storage at 23 6 3°C (73.4 13.1 Prepare test panels or sheets for determining the bond
6 5°F) before opening. If the adhesive consists of two or more strength of the adhesive in accordance with any of the ASTM
components, blend the components in accordance with the testmethodssuitableforthepurpose.Forexample,thelap-type
instructions from the manufacturer, and again adjust the shear specimens or the spool-type tension specimens such as
temperature to 23 6 3°C, if required. those described in the following methods are acceptable for
use: Test Method D897, Test Method
...

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This specification provides the means to measure and evaluate the performance of adhesives for structural or semistructural bonding of wood-to-wood in manufactured homes. Wood as used in this specification includes lumber, plywood, particleboard, gypsum board, and all materials having woodbased surfaces at the bondline. The adhesives can be classified according to resistance to deformation: Group A or structural, and Group B or semistructural. Also, the adhesives may be designated into three types, according to their recommended use based on their resistance to water and water vapor: Type 1 for interior and exterior use, Type 2 for weather-protected interior use, and Type 3 for interior use only. Different tests shall be performed in order to determine the following properties of adhesives: shear strength, gap-filling ability, total deformation resistance, moisture and temperature limitation during fabrication, high-temperature resistance, low-temperature resistance, moisture resistance, aging, oxidation resistance, and mold resistance.
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1.1.1 The performance of the adhesives is measured in the following tests:    
Number  
Test  
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4.1 Creep data that are obtained over a relatively short period of time in this test method can provide a measure of an adhesive bond's ability to withstand static loading in shear over a relatively long period of time. Creep measurements are made over a range of expected service conditions, including level of stress, temperature, relative humidity, and duration of load. Creep rate, creep strain, and creep modulus are calculated at the various service conditions.  
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4.4 With proper caution, time-to-failure data derived from relatively short loading periods can be extrapolated to estimate the useful service life of an adhesive at working levels of static stress. This property may also be used with creep data to accomplish purposes listed in 4.2.  
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SCOPE
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4.1 These test methods are designed to be used to determine the susceptibility of the adhesive film to biodegradation and whether the adhesive will carry into the bond line sufficient anti-fungal properties to prevent growth of fungi frequently present on the gluing equipment, on adherends, or in the adhesive as applied.  
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Note 2: The method given here using the MSA is based on Practice G21, adapted to be used with adhesives. Requirements for the use of the MSA are described in 10.2, and a mixed species of fungi is prescribed in 8.2 for the inoculum.  
4.3 The results obtained when using the procedures given in this method apply only to the species used for the testing. The test species listed in Section 8 are frequently used by laboratories to test for antifungal properties, but they are not the only ones which could be used. Selection of the fungal species to test against requires informed judgment by the testing laboratory or by the party requesting the tests. These methods are especially useful when species that have been isolated from contaminated adhesives are used as the test species (see Section 8) to aid in the selection of more effective fungicides.  
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4.1 Tension tests provide reasonably accurate information with regard to the tensile strength of adhesives. Tensile strength data may be suitable for specification acceptance, service evaluation, manufacturing control, research, and development. Tension tests are not considered significant for applications differing from the test in rate, direction, and type of loading.
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5.1 This test method evaluates the performance of the adhesive in laminated wood as measured by resistance to creep under static load.  
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1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
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1.1 This test method is used to make comparative assessments of the securing or locking effect of adhesives used in threaded assemblies.  
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5.1 This test method is designed for obtaining a qualitative estimate of the compatibility of plastics and adhesives. Due to the many process variables associated with the fabrication of plastic parts, it is not possible to use this test as a substitute for compatibility tests on actual parts.  
5.2 The detection of cracks or crazes may be determined with or without optical aid. Make comparisons only among tests employing crack detection methods of equivalent sensitivity.
SCOPE
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1.2 Specimen configurations and test fixture designs are given.  
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1.4 The values stated in SI units are to be regarded as the standard. The inch-pound units given in parentheses are for information only.  
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Standard Terminology of Adhesives

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1.1 This terminology standard is a compilation of definitions used in the science and technology of the adhesives industry. Terms that are generally understood or adequately defined in other readily available sources are not included.  
1.2 Any changes in this standard since 1988 are documented as follows:  
1.2.1 Appendix X1 gives a history of revisions made since 1988. Table X1.1 lists the terms that are affected as: (1) Terms Added, (2) Terms Revised, and (3) Terms Deleted.
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