ASTM D6114/D6114M-09
(Specification)Standard Specification for Asphalt-Rubber Binder (Withdrawn 2018)
Standard Specification for Asphalt-Rubber Binder (Withdrawn 2018)
ABSTRACT
This specification covers asphalt-rubber binder, consisting of a blend of paving grade asphalt cements, ground recycled tire (that is, vulcanized) rubber and other additives, as needed, for use as binder in pavement construction. The rubber shall be blended and interacted in the hot asphalt cement sufficiently to cause swelling of the rubber particles prior to use. Tests shall be performed to conform with the physical requirements of the asphalt-rubber binder, in accordance with the following test methods: apparent viscosity; modified test method; penetration; softening point; resilience; flash point; thin-film oven test residue; and penetration retention.
SCOPE
1.1 This specification covers asphalt-rubber binder, consisting of a blend of paving grade asphalt cements, ground recycled tire (that is, vulcanized) rubber and other additives, as needed, for use as binder in pavement construction. The rubber shall be blended and interacted in the hot asphalt cement sufficiently to cause swelling of the rubber particles prior to use.
Note 1—It has been found that at least 15 % rubber by weight of the total blend is usually necessary to provide acceptable properties of asphalt-rubber.
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.
1.3 The following precautionary caveat pertains to the test method portions only, Sections 4 and 5 of this Specification: This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Specific precautionary statements are given in 4.3.2.
WITHDRAWN RATIONALE
This specification covered asphalt-rubber binder, consisting of a blend of paving grade asphalt cements, ground recycled tire (that is, vulcanized) rubber and other additives, as needed, for use as binder in pavement construction.
Formerly under the jurisdiction of Committee D04 on Road and Paving Materials, this specification was withdrawn in January 2018 in accordance with section 10.6.3 of the Regulations Governing ASTM Technical Committees, which requires that standards shall be updated by the end of the eighth year since the last approval date.
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Designation: D6114/D6114M −09
Standard Specification for
1
Asphalt-Rubber Binder
This standard is issued under the fixed designation D6114/D6114M; the number immediately following the designation indicates the
year of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last
reapproval. A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D140 Practice for Sampling Bituminous Materials
D946 Specification for Penetration-Graded Asphalt Cement
1.1 This specification covers asphalt-rubber binder, consist-
for Use in Pavement Construction
ing of a blend of paving grade asphalt cements, ground
D1754 Test Method for Effects of Heat andAir onAsphaltic
recycled tire (that is, vulcanized) rubber and other additives, as
Materials (Thin-Film Oven Test)
needed, for use as binder in pavement construction.The rubber
D1864 TestMethodforMoistureinMineralAggregateUsed
shall be blended and interacted in the hot asphalt cement
on Built-Up Roofs
sufficiently to cause swelling of the rubber particles prior to
D2196 Test Methods for Rheological Properties of Non-
use.
Newtonian Materials by Rotational (Brookfield type)
NOTE 1—It has been found that at least 15 % rubber by weight of the
Viscometer
total blend is usually necessary to provide acceptable properties of
D2872 Test Method for Effect of Heat andAir on a Moving
asphalt-rubber.
Film of Asphalt (Rolling Thin-Film Oven Test)
1.2 The values stated in either SI units or inch-pound units
D3381 Specification for Viscosity-Graded Asphalt Cement
are to be regarded separately as standard. The values stated in
for Use in Pavement Construction
each system may not be exact equivalents; therefore, each
D5329 Test Methods for Sealants and Fillers, Hot-Applied,
system shall be used independently of the other. Combining
for Joints and Cracks in Asphaltic and Portland Cement
values from the two systems may result in non-conformance
Concrete Pavements
with the standard.
D5644 Test Methods for Rubber Compounding Materials—
1.3 The following precautionary caveat pertains to the test
Determination of Particle Size Distribution of Recycled
method portions only, Sections 4 and 5 of this Specification: Vulcanizate Particulate Rubber
This standard does not purport to address all of the safety
D6373 Specification for Performance Graded Asphalt
concerns, if any, associated with its use. It is the responsibility Binder
of the user of this standard to establish appropriate safety and
health practices and determine the applicability of regulatory
3. Materials
limitations prior to use. Specific precautionary statements are
3.1 Asphalt Cement—The asphalt cement shall meet the
given in 4.3.2.
requirements of Specifications D946, D3381 or D6373. Ac-
ceptable grades shall be able to produce the properties of Table
2. Referenced Documents
1 of this specification when interacted with ground recycled
2
2.1 ASTM Standards:
tire rubber.
D5 Test Method for Penetration of Bituminous Materials
3.2 Ground Recycled Tire Rubber:
D36 Test Method for Softening Point of Bitumen (Ring-and-
Ball Apparatus) 3.2.1 The ground recycled tire rubber shall contain less than
0.75 % moisture by weight and shall be free flowing. The
D92 Test Method for Flash and Fire Points by Cleveland
Open Cup Tester specific gravity of the rubber shall be 1.15 6 0.05. The ground
recycled tire rubber shall contain no visible nonferrous metal
particles and no more than 0.01 % ferrous metal particles by
1
weight.
This specification is under the jurisdiction of ASTM Committee D04 on Road
and Paving Materials and is the direct responsibility of Subcommittee D04.40 on
3.2.2 For use in hot mix binders, the fiber content shall not
Asphalt Specifications.
exceed 0.5 % by weight of ground recycled tire rubber.
CurrenteditionapprovedJune1,2009.PublishedJuly2009.Originallyapproved
Howeverforuseinbindersforsprayapplications,fibercontent
in 1997. Last previous edition approved in 2002 as D6114 – 97 (2002). DOI:
10.1520/D6114_D6114M-09.
shall not exceed 0.1 % by weight. Up to 4 % by weight of
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
mineral powder (such as talc) is permitted to prevent sticking
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
andcakingoftherubberparticles.Otherforeigncontaminating
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. materials (see Note 2) shall be less than 0.25 % by weight.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
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D6114/D6114M − 09
TABLE 1 Physical Requirements for Asphalt-Rubber Binder
A
Binder Designation Type I Type II Type III
Ap
...
This document is not anASTM standard and is intended only to provide the user of anASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation:D6114–97 (Reapproved 2002) Designation: D 6114/D 6114M – 09
Standard Specification for
1
Asphalt-Rubber Binder
This standard is issued under the fixed designation D 6114/D 6114M; the number immediately following the designation indicates the
year of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last
reapproval. A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This specification covers asphalt-rubber binder, consisting of a blend of paving grade asphalt cements, ground recycled tire
(that is, vulcanized) rubber and other additives, as needed, for use as binder in pavement construction.The rubber shall be blended
and interacted in the hot asphalt cement sufficiently to cause swelling of the rubber particles prior to use.
NOTE 1—Ithasbeenfoundthatatleast15 %rubberbyweightofthetotalblendisusuallynecessarytoprovideacceptablepropertiesofasphalt-rubber.
1.2The values stated in SI units are to be regarded as the standard.The inch-pound units given in parentheses are for information
only.
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each
system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the
two systems may result in non-conformance with the standard.
1.3 The following precautionary caveat pertains to the test method portions only, Sections 4 and 5 of this Specification: This
standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user
of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior
to use. Specific precautionary statements are given in 4.3.2.
2. Referenced Documents
2
2.1 ASTM Standards:
D5 Test Method for Penetration of Bituminous Materials
D36 Test Method for Softening Point of Bitumen (Ring-and-Ball Apparatus)
D93TestMethodsforFlashPointbyPensky-MartensClosedCupTester 92 TestMethodforFlashandFirePointsbyCleveland
Open Cup Tester
D 140 Practice for Sampling Bituminous Materials
D 946 Specification for Penetration-Graded Asphalt Cement for Use in Pavement Construction
D 1754 Test Method for Effects of Heat and Air on Asphaltic Materials (Thin-Film Oven Test)
D 1864 Test Method for Moisture in Mineral Aggregate Used on Built-Up Roofs
D 2196 Test Methods for Rheological Properties of Non-Newtonian Materials by Rotational (Brookfield type) Viscometer
D2872
D 2872 Test Method for Effect of Heat and Air on a Moving Film of Asphalt (Rolling Thin-Film Oven Test)
D 3381 Specification for Viscosity-Graded Asphalt Cement for Use in Pavement Construction
D 5329 Test Methods for Sealants and Fillers, Hot-Applied, for Joints and Cracks in Asphaltic and Portland Cement Concrete
Pavements
D5644
D 5644 Test Methods for Rubber Compounding MaterialsDetermination of Particle Size Distribution of Recycled Vulcanizate
Particulate Rubber Determination of Particle Size Distribution of Recycled Vulcanizate Particulate Rubber
D 6373 Specification for Performance Graded Asphalt Binder
3. Materials
3.1 Asphalt Cement— The asphalt cement shall meet the requirements of Specification D946 or Table 1 or 3 of Specification
D3381— The asphalt cement shall meet the requirements of Specifications D 946, D 3381 or D 6373.Acceptable grades shall be
1
This specification is under the jurisdiction ofASTM Committee D04 on Road and Paving Materials and is the direct responsibility of Subcommittee D04.40 onAsphalt
Specifications.
Current edition approved May 10, 1997. Published October 1998. Originally published as D 6114 – 97. Last previous edition D 6114 – 97.
Current edition approved June 1, 2009. Published July 2009. Originally approved in 1997. Last previous edition approved in 2002 as D 6114 – 97 (2002).
2
For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at service@astm.org. For Annual Book ofASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1
---------------------- Page: 1 ----------------------
D 6114/D 6114M – 09
able to produce the properties of Table 1 of this specification when interacted with ground recycled tire rubber.
3.2 Ground Recycled Tire Rubber :
3.2.
...
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