ASTM D3911-08
(Test Method)Standard Test Method for Evaluating Coatings Used in Light-Water Nuclear Power Plants at Simulated Design Basis Accident (DBA) Conditions
Standard Test Method for Evaluating Coatings Used in Light-Water Nuclear Power Plants at Simulated Design Basis Accident (DBA) Conditions
SIGNIFICANCE AND USE
This test method is designed to provide a uniform test to determine the suitability of Coating Service Level 1 coatings used inside primary containment of light-water nuclear facilities under simulated DBA conditions. This test method is intended only to demonstrate that under DBA conditions, the coatings will remain intact and not form debris which could unacceptably compromise the operability of engineered safety systems. Deviations in actual surface preparation and in application and curing of the coating materials from qualification test parameters require an engineering evaluation to determine if additional testing is required.
Since different plants have different tolerance levels for coating conditions, the definition of appropriate acceptance criteria is to be developed by the license holder based on individual plant engineered safety systems operability considerations.
Use of this standard is predicated on the testing facility having a quality assurance program acceptable to the licensee.
SCOPE
1.1 This test method establishes procedures for evaluating protective coating systems test specimens under simulated DBA conditions. Included are a description of conditions and apparatus for temperature-pressure testing, and requirements for preparing, irradiating, testing, examining, evaluating, and documenting the samples.
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical conversions to SI units that are provided for information only and are not considered standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
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Designation: D3911 − 08
StandardTest Method for
Evaluating Coatings Used in Light-Water Nuclear Power
Plants at Simulated Design Basis Accident (DBA)
1
Conditions
This standard is issued under the fixed designation D3911; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
INTRODUCTION
During a DBAin nuclear power plants, conditions in the reactor containment will be characterized
by elevated temperature and pressure, as well as the presence of a radiation environment. Water
sprays, with or without chemical additives, may be used in the primary containment to suppress the
consequences of the event, to scavenge radioactive products, and to return the containment to
near-ambient pressure and temperature conditions.
1. Scope D4538 Terminology Relating to Protective Coating and
Lining Work for Power Generation Facilities
1.1 This test method establishes procedures for evaluating
D5139 Specification for Sample Preparation for Qualifica-
protective coating systems test specimens under simulated
tion Testing of Coatings to be Used in Nuclear Power
DBA conditions. Included are a description of conditions and
Plants
apparatus for temperature-pressure testing, and requirements
for preparing, irradiating, testing, examining, evaluating, and
3. Terminology
documenting the samples.
3.1 Definitions—Definitions for use with this standard are
1.2 The values stated in inch-pound units are to be regarded
shown in Terminology D4538 or other applicable standards.
as standard. The values given in parentheses are mathematical
4. Significance and Use
conversions to SI units that are provided for information only
and are not considered standard.
4.1 This test method is designed to provide a uniform test to
1.3 This standard does not purport to address all of the determine the suitability of Coating Service Level 1 coatings
safety concerns, if any, associated with its use. It is the used inside primary containment of light-water nuclear facili-
responsibility of the user of this standard to establish appro- ties under simulated DBA conditions. This test method is
priate safety and health practices and determine the applica- intended only to demonstrate that under DBA conditions, the
bility of regulatory limitations prior to use. coatings will remain intact and not form debris which could
unacceptably compromise the operability of engineered safety
2. Referenced Documents
systems. Deviations in actual surface preparation and in
2
application and curing of the coating materials from qualifica-
2.1 ASTM Standards:
tion test parameters require an engineering evaluation to
D714 Test Method for Evaluating Degree of Blistering of
determine if additional testing is required.
Paints
D4082 Test Method for Effects of Gamma Radiation on
4.2 Since different plants have different tolerance levels for
Coatings for Use in Nuclear Power Plants
coating conditions, the definition of appropriate acceptance
criteria is to be developed by the license holder based on
individual plant engineered safety systems operability consid-
1
This test method is under the jurisdiction of ASTM Committee D33 on
ProtectiveCoatingandLiningWorkforPowerGenerationFacilitiesandisthedirect erations.
responsibility of Subcommittee D33.02 on Service and Material Parameters.
4.3 Use of this standard is predicated on the testing facility
Current edition approved Nov. 1, 2008. Published January 2009. Originally
approved in 1980. Last previous edition approved in 2003 as D3911 – 03. DOI: having a quality assurance program acceptable to the licensee.
10.1520/D3911-08.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or 5. Apparatus
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
5.1 Environmental Test Chamber, constructed of materials
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. that are corrosion-resistant to the test solutions.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
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D3911 − 08
5.2 The equipment shall be capable of reproducing and 7.1.1 Test coatings using the applicable time-temperature-
continuouslyrecordingthetemperatureandpressureprofilesof pressure curves identified by the plant design basis. Examples
the DBA conditions.
of time-temperature-pressure test curves that have been used to
simulate primary containment atmospheres during a DBA are
5.3 Asufficient number of thermocouples shall be located in
shown in Fig. 1 and Fig. 2. These curves may no
...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation:D3911–03 Designation:D3911–08
Standard Test Method for
Evaluating Coatings Used in Light-Water Nuclear Power
Plants at Simulated Design Basis Accident (DBA)
1
Conditions
This standard is issued under the fixed designation D 3911; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
INTRODUCTION
During a DBAin nuclear power plants, conditions in the reactor containment will be characterized
by elevated temperature and pressure, as well as the presence of a radiation environment. Water
sprays, with or without chemical additives, may be used in the primary containment to suppress the
consequences of the event, to scavenge radioactive products, and to return the containment to
near-ambient pressure and temperature conditions.
1. Scope
1.1 This test method establishes procedures for evaluating protective coating systems test specimens under simulated DBA
conditions.Includedareadescriptionofconditionsandapparatusfortemperature-pressuretesting,andrequirementsforpreparing,
irradiating, testing, examining, evaluating, and documenting the samples.
1.2The values stated in inch-pound and degrees F units are to be regarded as the standard. The SI values given in parentheses
are for information only.
1.2 The values stated in inch-pound units are to be regarded as standard. The values given in parentheses are mathematical
conversions to SI units that are provided for information only and are not considered standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
D 714 Test Method for Evaluating Degree of Blistering of Paints
D1193Specification for Reagent Water Test Method for Evaluating Degree of Blistering of Paints
D 4082 Test Method for Effects of Gamma Radiation on Coatings Used for Use in Light-Water Nuclear Power Plants
D 4538 Terminology Relating to Protective Coating and Lining Work for Power Generation Facilities
4
D 5139 Specification for Sample Preparation for Qualification Testing of Coatings to be Used in Nuclear Power Plants
4
D5144Guide for Use of Protective Coating Standards in Nuclear Power Plants Specification for Sample Preparation for
Qualification Testing of Coatings to be Used in Nuclear Power Plants
3. Terminology
3.1 Definitions—Definitions for use with this standard are shown in Terminology D 4538 or other applicable standards.
3.2Definitions of Terms Specific to This Standard:
3.2.1blistering—the formation of bubbles in a coating (paint) film.
3.2.2chemical spray—asolutionofchemicals,suchasthosecontainedinTable1,whichcouldbeusedduringaDBAtosuppress
the incident, to scavenge fission products, and to return the facility to near-ambient pressure and temperature conditions.
1
ThistestmethodisunderthejurisdictionofASTMCommitteeD33onProtectiveCoatingandLiningWorkforPowerGenerationFacilitiesandisthedirectresponsibility
of Subcommittee D33.02 on Service and Material Parameters.
Current edition approved Jan. 10, 2003. Published March 2003. Originally approved in 1980. Last previous edition approved in 1995 as D3911–95.
Current edition approved Nov. 1, 2008. Published January 2009. Originally approved in 1980. Last previous edition approved in 2003 as D 3911 – 03.
2
For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
, Vol 06.01.volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1
---------------------- Page: 1 ----------------------
D3911–08
TABLE 1 Typical Spray Solutions
Composition Chemical Compound Concentration (in Deionized Water)
A Sodium borate 2000 to 4000 ppm boron
Sodium hydroxide adjust solution to pH 9.0 to 10.0
B Boric acid 2000 to 4000 ppm boron
Hydrazine 50 ppm unreacted excess
Sodium phosphate, dibasic adjust solution pH to 6.8 to 10.0
C Deionized water
3.2.3coating system—a protective film consisting of one or more coats applied in a predetermined order by prescribed methods
...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation:D3911–95 Designation:D3911–08
Standard Test Method for
Evaluating Coatings Used in Light-Water Nuclear Power
Plants at Simulated Design Basis Accident (DBA)
1
Conditions
This standard is issued under the fixed designation D 3911; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
INTRODUCTION
During a design basis accident (DBA) DBA in nuclear power plants, conditions in the reactor
containment will be characterized by elevated temperature and pressure, as well as the presence of a
radiation environment. Water sprays, with or without chemical additives, may be used in the primary
containment to suppress the consequences of the incident,event, to scavenge radioactive products, and
to return the containment to near-ambient pressure and temperature conditions.
1. Scope
1.1 This test method establishes procedures for evaluating protective coating systems test specimens under simulated DBA
conditions. Included are a description of conditions and apparatus for temperature-pressure testing, conditions for radiation testing,
and proceduresrequirements for preparing, irradiating, testing, examining, evaluating, and evaluatingdocumenting the samples.
1.2 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are mathematical
conversions to SI units that are provided for information only and are not considered standard.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
D 714 Test Method for Evaluating Degree of Blistering of Paints
D 4082 Test Method for Effects of Gamma Radiation on Coatings Used for Use in Light-Water Nuclear Power Plants
D 4538 Terminology Relating to Protective Coating and Lining Work for Power Generation Facilities
D 5139 Specification for Sample Preparation for Qualification Testing of Coatings to be Used in Nuclear Power Plants
3. Terminology
3.1 Definitions:
3.1.1blistering—the formation of bubbles in a coating (paint) film.
3.1.2boiling water reactor (BWR)—areactorinwhichthewatermoderator-coolantisboileddirectlywithinthereactorcore.The
pressure in the reactor vessel is only slightly greater than the steam turbine pressure.
3.1.3chemical spray—a solution of chemicals, such as those contained in Table 1, which could be used during a loss of coolant
accident (LOCA) to suppress the incident, to scavenge fission products, and to return the facility to near-ambient conditions.
3.1.4coating (paint) system—a polymeric protective film consisting of one or more coats applied in a predetermined order by
prescribed methods to a defined substrate.
3.1.5cracking—a break or a split in the coating (paint) system extending through the film or to the substrate.
3.1.6curing—the transformation of a coating or other material into a solid phase or film.
3.1.7DBA—a generic term for any one of a family of accident conditions which can result from postulated events. These
1
This test method is under the jurisdiction of ASTM Committee D-33D33 on Protective Coating and Lining Work for Power Generation Facilities and is the direct
responsibility of Subcommittee D33.02 on Service and Material Parameters.
Current edition approved Oct. 10, 1995.Nov. 1, 2008. Published December 1995.January 2009. Originally published as D3911–80.approved in 1980. Last previous edition
D3911–89.approved in 2003 as D 3911 – 03.
2
For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
, Vol 06.01.volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1
---------------------- Page: 1 ----------------------
D3911–08
TABLE 1 Typical Spray Solutions
Composition Chemical Compound Concentration (in Deionized Water)
A Sodium borate 2000 to 4000 ppm boron
Sodium hydroxide adjust solution to pH 9.0 to 10.0
B Boric acid 2000 to 4000 ppm boron
Hydrazine 50 ppm unreacted excess
Sodium phosphate, dib
...












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