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ASTM D1296-01(2007)

(Test Method)

Standard Test Method for Odor of Volatile Solvents and Diluents

Standard Test Method for Odor of Volatile Solvents and Diluents

SIGNIFICANCE AND USE
The comparative odor characteristics can be used, combined with other tests, for product identification and assessing compliance with a specification.
The residual odor characteristics can be used to judge the presence of relatively nonvolatile materials that may be associated with manufacture or contamination during distribution. Since volatile solvents and diluents are used in a wide variety of chemical processes and residual materials may affect the efficiency of such processes, this test method provides a comparative test for manufacturing control and assessing compliance with a specification.
SCOPE
1.1 This test method covers a comparative procedure for observing the characteristic and residual odors of volatile organic solvents and diluents to determine their odor acceptability in a solvent system.
1.2 It is not intended that this test method be employed to determine subtle odor differences between materials or to determine odor intensity.
1.3 It is recommended that this test method not be employed to determine the residual odor of a liquid if its time for evaporation to dryness at room temperature exceeds 30 min or as agreed upon.
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. For specific hazard statements, see Section 4.
1.5 For specific hazard information, see the supplier's Material Safety Data Sheet (MSDS).

General Information

Status
Historical
Publication Date
31-May-2007
ICS
87.060.30 - Solvents
Technical Committee
D01 - Paint and Related Coatings, Materials, and Applications
Drafting Committee
D01.35 - Solvents, Plasticizers, and Chemical Intermediates
Current Stage
Ref Project

Relations

Replaces
ASTM D1296-01 - Standard Test Method for Odor of Volatile Solvents and Diluents
Effective Date
01-Jun-2007
Referred By
ASTM D3131-07(2021) - Standard Specification for Isopropyl Acetate (99 % Grade)
Effective Date
01-Jun-2007
Referred By
ASTM D3622-11(2019) - Standard Specification for 1-Propanol (<emph type="bdit">n</emph>-Propyl Alcohol)
Effective Date
01-Jun-2007
Referred By
ASTM D6763-16(2022) - Standard Guide for Testing Exterior Wood Stains and Clear Water Repellents
Effective Date
01-Jun-2007
Referred By
ASTM D1836-07(2021) - Standard Specification for Commercial Hexanes
Effective Date
01-Jun-2007
Referred By
ASTM D2634-07(2021) - Standard Specification for Methyl Amyl Acetate (95 % Grade)
Effective Date
01-Jun-2007
Referred By
ASTM D1153-22 - Standard Specification for Methyl Isobutyl Ketone
Effective Date
01-Jun-2007
Referred By
ASTM D608-05(2019) - Standard Specification for Dibutyl Phthalate
Effective Date
01-Jun-2007
Referred By
ASTM D3730-17(2022) - Standard Guide for Testing High-Performance Interior Architectural Wall Coatings
Effective Date
01-Jun-2007
Referred By
ASTM D3735-22 - Standard Specification for VM&amp;P Naphthas
Effective Date
01-Jun-2007
Referred By
ASTM D268-22 - Standard Guide for Sampling and Testing Volatile Solvents and Chemical Intermediates for Use in Paint and Related Coatings and Material
Effective Date
01-Jun-2007
Referred By
ASTM D5146-10(2019) - Standard Guide to Testing Solvent-Borne Architectural Coatings
Effective Date
01-Jun-2007
Referred By
ASTM D235-22 - Standard Specification for Mineral Spirits (Petroleum Spirits) (Hydrocarbon Dry Cleaning Solvent)
Effective Date
01-Jun-2007
Referred By
ASTM D329-07(2021) - Standard Specification for Acetone
Effective Date
01-Jun-2007
Referred By
ASTM E3237-19 - Standard Specification for Undenatured Ethanol from Biomass for Use in Industrial Applications
Effective Date
01-Jun-2007

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ASTM D1296-01(2007) - Standard Test Method for Odor of Volatile Solvents and DiluentsASTM D1296-01(2007) - Standard Test Method for Odor of Volatile Solvents and Diluents
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ASTM D1296-01(2007) - Standard Test Method for Odor of Volatile Solvents and Diluents
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D1296 − 01 (Reapproved 2007)
StandardTest Method for
Odor of Volatile Solvents and Diluents
This standard is issued under the fixed designation D1296; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
This standard has been approved for use by agencies of the Department of Defense.
1. Scope* associated with manufacture or contamination during distribu-
tion. Since volatile solvents and diluents are used in a wide
1.1 This test method covers a comparative procedure for
variety of chemical processes and residual materials may affect
observing the characteristic and residual odors of volatile
the efficiency of such processes, this test method provides a
organic solvents and diluents to determine their odor accept-
comparative test for manufacturing control and assessing
ability in a solvent system.
compliance with a specification.
1.2 It is not intended that this test method be employed to
determine subtle odor differences between materials or to
4. Hazards
determine odor intensity.
4.1 Many solvents and diluents are hazardous or toxic. Take
1.3 It is recommended that this test method not be employed
special precautions while determining the odor of all products.
to determine the residual odor of a liquid if its time for
Make the tests only as frequently as is necessary for control
evaporation to dryness at room temperature exceeds 30 min or
and base the evaluations on short sniffs, inhaling as little vapor
as agreed upon.
as possible.
1.4 The values stated in SI units are to be regarded as
4.2 Provide adequate ventilation to maintain solvent or
standard. No other units of measurement are included in this
diluent concentration below the personnel exposure limit value
standard.
established for the general work area as given in the MSDS.
1.5 This standard does not purport to address all of the
4.3 Other hazards may also be present. These may be, but
safety concerns, if any, associated with its use. It is the
are not limited to, flammable, combustible, corrosive, or
responsibility of the user of this standard to establish appro-
explosive hazards.
priate safety and health practices and determine the applica-
bility of regulatory limitations prior to use. For specific hazard
5. Procedures
statements, see Section 4.
5.1 Characteristic Odor—Dip 25 by 75-mm strips of rapid
1.6 For specific hazard information, see the supplier’s
qualititive paper, free of foreign odor, to a depth of 50 mm into
Material Safety Data Sheet (MSDS).
the specimen and the reference standard, each contained in a
2. Reference Standards
beaker or other suitable container. Make an immediate com-
parison between the odor of the two materials on the filter
2.1 Samples of the particular products being tested, having
papers.
odor characteristics satisfactory to purchaser and manufacturer,
are required.
5.2 Residual Odor—Dip 25 by 75-mm strips of a rapid
qualitative paper, free of foreign odor, to a depth of 50 mm into
3. Significance and Use
the specimen under test and the reference sample, each
3.1 The comparative odor characteristics can be used, com-
contained in a beaker or other suitable container. Permit the
bined with other tests, for product identification and assessing
papers to dry in air at room temperature and examine them at
compliance with a specification.
suitable intervals for differences in odor (see 1.3). The evapo-
ration step may be omitted if only the“ characteristic” odor of
3.2 The residual odor characteristics can be used to judge
the material is to be determined.
the presence of relatively nonvolatile materials that may be
6. Report
This test method is under the jurisdiction of ASTM Committee D01 on Paint
and Related Coatings, Materials, andApplications and is the direct responsibility of
6.1 Characteristic Odor—Report the odor as “charac
...

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Standard Test Method for Acetone, Methyl Acetate, and Parachlorobenzotrifluoride Content of Paints, and Coatings by Solid Phase Microextraction-Gas Chromatography

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5.1 In order to calculate the volatile organic content (VOC) of paints containing EPA exempt solvents, it is necessary to know the acetone, methyl acetate, or parachlorobenzotrifluoride content. This gas chromatographic test method provides a simple and direct way for measuring these solvents. Each analyte is measured with respect to a unique internal standard. For acetone, the internal standard used is acetone-d6, for methyl acetate it is methyl acetate-d3, and for PCBTF it is metachlorobenzotrifluoride (MCBTF). These unique analyte/internal standard pairs behave very nearly as single solvents with respect to evaporation rate and adsorption rate onto a coated silica fiber (SPME) but are separable on a gas chromatograph (GC) capillary column. The only critical analytical technique required for successfully performing this test method is the ability of an analyst to weigh a paint sample and internal standard, corresponding to the analyte of interest, into a septum capped vial. After weighing, solvent evaporation has no effect on the final value of the determination. Since whole paint is not injected into the gas chromatograph, the analytical system is never compromised.
SCOPE
1.1 This test method is for the determination of acetone, methyl acetate, or parachlorobenzotrifluoride (PCBTF), or combination of any of the three, in paints and coatings, by solid phase microextraction (SPME) headspace sampling, and subsequent injection into a gas chromatograph. It has been evaluated for cellulose nitrate, acrylic, and urethane solvent-borne systems. The established working range of this test method is: acetone, 28 to 90 %; methyl acetate, 12 to 22 %; parachlorobenzotrifluoride, 10 to 17 %. There is no reason to believe that it will not work outside these ranges. A minor modification of this test method would make it suitable for the analysis of the same analytes in water-borne coatings (see Note 1).
Note 1: Water-borne paints are internally standardized and diluted with water followed by addition of solid sodium chloride.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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