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ASTM D608-05(2019)

(Specification)

Standard Specification for Dibutyl Phthalate

Standard Specification for Dibutyl Phthalate

ABSTRACT
This specification establishes the properties and requirements of 99 % grade dibutyl phthalate. The material shall be sampled and tested suitably, and shall conform to properties as to apparent specific gravity, color (Pt-Co scale), odor, water content, acidity (free acid as phthalic acid), and ester value.
SCOPE
1.1 This specification covers dibutyl phthalate (99 % grade).  
1.2 The following applies to all specified limits in this standard: for purposes of determining conformance with this standard, an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29.  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 For specific hazard information and guidance, see the supplier's Material Safety Data Sheet for materials listed in this specification.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
31-Mar-2019
ICS
87.060.30 - Solvents
Technical Committee
D01 - Paint and Related Coatings, Materials, and Applications
Drafting Committee
D01.35 - Solvents, Plasticizers, and Chemical Intermediates
Current Stage
Ref Project

Relations

Replaces
ASTM D608-05(2011) - Standard Specification for Dibutyl Phthalate
Effective Date
01-Apr-2019
Refers
ASTM D1613-06(2012) - Standard Test Method for Acidity in Volatile Solvents and Chemical Intermediates Used in Paint, Varnish, Lacquer, and Related Products
Effective Date
01-Jun-2012
Refers
ASTM D5386-10 - Standard Test Method for Color of Liquids Using Tristimulus Colorimetry
Effective Date
01-Jan-2010
Refers
ASTM E29-08 - Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
Effective Date
01-Oct-2008
Refers
ASTM D268-01(2007) - Standard Guide for Sampling and Testing Volatile Solvents and Chemical Intermediates for Use in Paint and Related Coatings and Material
Effective Date
01-Jun-2007
Refers
ASTM D1617-07 - Standard Test Method for Ester Value of Solvents and Thinners
Effective Date
01-Jun-2007
Refers
ASTM D1296-01(2007) - Standard Test Method for Odor of Volatile Solvents and Diluents
Effective Date
01-Jun-2007
Refers
ASTM D1364-02(2007) - Standard Test Method for Water in Volatile Solvents (Karl Fischer Reagent Titration Method)
Effective Date
01-Jun-2007
Refers
ASTM D1476-02(2007) - Standard Test Method for Heptane Miscibility of Lacquer Solvents
Effective Date
01-Jun-2007
Refers
ASTM E29-06b - Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
Effective Date
15-Nov-2006
Refers
ASTM E29-06a - Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
Effective Date
15-Sep-2006
Refers
ASTM E29-06 - Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
Effective Date
01-May-2006
Refers
ASTM D1613-06 - Standard Test Method for Acidity in Volatile Solvents and Chemical Intermediates Used in Paint, Varnish, Lacquer, and Related Products
Effective Date
01-Apr-2006
Refers
ASTM D5386-05 - Standard Test Method for Color of Liquids Using Tristimulus Colorimetry
Effective Date
15-Oct-2005
Refers
ASTM D1209-05 - Standard Test Method for Color of Clear Liquids (Platinum-Cobalt Scale)
Effective Date
15-May-2005

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ASTM D608-05(2019) - Standard Specification for Dibutyl PhthalateASTM D608-05(2019) - Standard Specification for Dibutyl Phthalate
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ASTM D608-05(2019) - Standard Specification for Dibutyl Phthalate
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D608 −05 (Reapproved 2019)
Standard Specification for
Dibutyl Phthalate
This standard is issued under the fixed designation D608; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D1476 Test Method for Heptane Miscibility of Lacquer
Solvents
1.1 Thisspecificationcoversdibutylphthalate(99 %grade).
D1613 Test Method for Acidity in Volatile Solvents and
1.2 The following applies to all specified limits in this
Chemical Intermediates Used in Paint, Varnish, Lacquer,
standard: for purposes of determining conformance with this
and Related Products
standard, an observed value or a calculated value shall be
D1617 TestMethodforEsterValueofSolventsandThinners
rounded off “to the nearest unit” in the last right-hand digit
D4052 Test Method for Density, Relative Density, and API
used in expressing the specification limit, in accordance with
Gravity of Liquids by Digital Density Meter
the rounding-off method of Practice E29.
D5386 Test Method for Color of Liquids Using Tristimulus
Colorimetry
1.3 The values stated in SI units are to be regarded as
standard. No other units of measurement are included in this E29 Practice for Using Significant Digits in Test Data to
Determine Conformance with Specifications
standard.
E300 Practice for Sampling Industrial Chemicals
1.4 For specific hazard information and guidance, see the
2.2 U.S. Federal Specification:
supplier’sMaterialSafetyDataSheetformaterialslistedinthis
PPP-C-2020 Chemicals, Liquid, Dry, and Paste: Packaging
specification.
of
1.5 This international standard was developed in accor-
dance with internationally recognized principles on standard-
3. Properties
ization established in the Decision on Principles for the
3.1 Dibutyl phthalate (99 % grade) shall conform to the
Development of International Standards, Guides and Recom-
following requirements:
mendations issued by the World Trade Organization Technical
Apparent specific gravity:
Barriers to Trade (TBT) Committee.
20/20 °C 1.046 to 1.050
or
2. Referenced Documents
25/25 °C 1.043 to 1.047
A
Color, Pt-Co scale, max 20
2.1 ASTM Standards: B
Odor nonresidual
C
D268 Guide for Sampling and Testing Volatile Solvents and Water, max, weight % 0.2
D
Acidity (free acid as phthalic 0.01
Chemical Intermediates for Use in Paint and Related
acid), max, weight %
Coatings and Material
Ester value, max, weight % not less than 99.0
D1209 Test Method for Color of Clear Liquids (Platinum- ______________
Cobalt Scale)
A
Instrumental Pt-Co color determined by Test Method D5386 has been shown to
D1296 Test Method for Odor of Volatile Solvents and
have no statistically significant difference from Pt-Co color determined by Test
Diluents
Method D1209. However, it is not known whether dibutyl phthalate was part of the
sample set included in the interlaboratory study.
D1364 Test Method for Water in Volatile Solvents (Karl
B
Optional as agreed upon between supplier and consumer.
Fischer Reagent Titration Method)
C
This quantitative limit ensures that the mat
...

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5.1 In order to calculate the volatile organic content (VOC) of paints containing EPA exempt solvents, it is necessary to know the acetone, methyl acetate, or parachlorobenzotrifluoride content. This gas chromatographic test method provides a simple and direct way for measuring these solvents. Each analyte is measured with respect to a unique internal standard. For acetone, the internal standard used is acetone-d6, for methyl acetate it is methyl acetate-d3, and for PCBTF it is metachlorobenzotrifluoride (MCBTF). These unique analyte/internal standard pairs behave very nearly as single solvents with respect to evaporation rate and adsorption rate onto a coated silica fiber (SPME) but are separable on a gas chromatograph (GC) capillary column. The only critical analytical technique required for successfully performing this test method is the ability of an analyst to weigh a paint sample and internal standard, corresponding to the analyte of interest, into a septum capped vial. After weighing, solvent evaporation has no effect on the final value of the determination. Since whole paint is not injected into the gas chromatograph, the analytical system is never compromised.
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1.1 This test method is for the determination of acetone, methyl acetate, or parachlorobenzotrifluoride (PCBTF), or combination of any of the three, in paints and coatings, by solid phase microextraction (SPME) headspace sampling, and subsequent injection into a gas chromatograph. It has been evaluated for cellulose nitrate, acrylic, and urethane solvent-borne systems. The established working range of this test method is: acetone, 28 to 90 %; methyl acetate, 12 to 22 %; parachlorobenzotrifluoride, 10 to 17 %. There is no reason to believe that it will not work outside these ranges. A minor modification of this test method would make it suitable for the analysis of the same analytes in water-borne coatings (see Note 1).
Note 1: Water-borne paints are internally standardized and diluted with water followed by addition of solid sodium chloride.  
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