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ASTM D2259-02

(Test Method)

Standard Test Method for Shrinkage of Yarns

Standard Test Method for Shrinkage of Yarns

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1.1 This test method is used to determine the shrinkage of yarns in skein form when treated in boiling water, dry heat, saturated steam, or solvents. This test method is applicable to yarns made from any fiber or combination of fibers where the tex of the yarn is known or can be determined. This test method is not recommended for elastomeric yarns and those yarns that stretch more than 5 % under the tension loadings prescribed, although it has been used for the latter.
Note 1—Procedures for determining yarn shrinkage and bulk properties of textured yarns are covered in Test Method D 4031.
1.2 This test method shows the values in both SI and inch-pound units. "SI" units is the technically correct name for the system of metric units known as the International System of Units. "Inch-pound" units is the technically correct name for the customary units used in the United States. The values stated in either SI units or in other units shall be regarded as standard. The values expressed in each system may not be exact equivalents; therefore each system must be used independently of the other without combining in any way.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
09-Sep-2002
ICS
59.080.20 - Yarns
Technical Committee
D13 - Textiles
Drafting Committee
D13.58 - Yarns and Fibers
Current Stage
Ref Project

Relations

Replaces
ASTM D2259-96 - Standard Test Method for Shrinkage of Yarns
Effective Date
10-Sep-2002
Replaced By
ASTM D2259-02(2006)e1 - Standard Test Method for Shrinkage of Yarns
Effective Date
01-Jun-2006
Referred By
ASTM D4849-21 - Standard Terminology Related to Yarns and Fibers
Effective Date
10-Sep-2002
Referred By
ASTM D3218-07(2018) - Standard Specification for Polyolefin Monofilaments
Effective Date
10-Sep-2002

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ASTM D2259-02 - Standard Test Method for Shrinkage of YarnsASTM D2259-02 - Standard Test Method for Shrinkage of Yarns
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ASTM D2259-02 - Standard Test Method for Shrinkage of Yarns
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D2259–02
Standard Test Method for
1
Shrinkage of Yarns
This standard is issued under the fixed designation D 2259; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
3
1. Scope D 4031 Test Method for Bulk Properties of TexturedYarns
D 4848 Terminology of Force, Deformation and Related
1.1 This test method is used to determine the shrinkage of
3
Properties of Textiles
yarns in skein form when treated in boiling water, dry heat,
3
D 4849 Terminology Relating to Fibers and Yarns
saturated steam, or solvents. This test method is applicable to
E 145 Specification for Gravity-Convection and Forced-
yarns made from any fiber or combination of fibers where the
4
Ventilation Ovens
texoftheyarnisknownorcanbedetermined.Thistestmethod
is not recommended for elastomeric yarns and those yarns that
3. Terminology
stretch more than 5 % under the tension loadings prescribed,
3.1 Definitions:
although it has been used for the latter.
3.1.1 For definitions of textile terms used in this test
NOTE 1—Procedures for determining yarn shrinkage and bulk proper-
method: skein and skein loop-length, refer to Terminology
ties of textured yarns are covered in Test Method D 4031.
D 4849.
1.2 This test method shows the values in both SI and
3.1.2 For definition of the term extension used in this test
inch-pound units. “SI” units is the technically correct name for
method, refer to Terminology D 4848.
thesystemofmetricunitsknownastheInternationalSystemof
3.1.3 Forothertextiletermsusedinthistestmethod,referto
Units. “Inch-pound” units is the technically correct name for
Terminology Standards, D 123, D 3888, D 3990,D 4848 and
thecustomaryunitsusedintheUnitedStates.Thevaluesstated
D 4849.
in either SI units or in other units shall be regarded as standard.
4. Summary of Test Method
The values expressed in each system may not be exact
equivalents; therefore each system must be used independently 4.1 The loop length of a conditioned skein of yarn is
of the other without combining in any way.
measured under a specific tension, which is sufficient to
1.3 This standard does not purport to address all of the straighten but not stretch the skein. The tension-free skein is
safety concerns, if any, associated with its use. It is the
then immersed in boiling water or exposed to dry heat or
responsibility of the user of this standard to establish appro-
saturated steam or in the solvent reconditioned, and remea-
priate safety and health practices and determine the applica- sured.Theshrinkage(orinsomecases,growth)iscalculatedas
bility of regulatory limitations prior to use.
the change in length expressed as a percentage of the length
before immersion or exposure.
2. Referenced Documents
5. Significance and Use
2.1 ASTM Standards:
2
D 123 Terminology Relating to Textiles 5.1 Test Method D 2259 for testing yarn for shrinkage in
D 1059 Test Method for Yarn Number Based on Short-
boiling water, saturated steam, dry heat, or solvents is consid-
2
Length Specimens ered satisfactory for acceptance testing of commercial ship-
2
D 1776 Practice for Conditioning and Testing Textiles
ments of yarn because the test method has been used exten-
D 1907 Test Method for Linear Density of Yarn (Yarn sively in the trade for that purpose.
2
Number) by the Skein Method
5.1.1 If there are differences of practical significance be-
2
D 2258 Practice for Sampling Yarn for Testing tween reported test results for two laboratories (or more),
3
D 3888 Terminology Related to Open-End Spinning
comparative tests should be performed to determine if there is
3
D 3990 Terminology Realting to Fabric Defects a statistical bias between them, using competent statistical
assistance. As a minimum, use the samples for such compara-
tive tests that are as homogeneous as possible, drawn from the
1
same lot of material as the samples that resulted in disparate
This test method is under the jurisdiction of Committee D13 on Textiles and is
the direct responsibility of Subcommittee D13.58 on Yarn Test Methods, General.
results during initial testing and randomly assigned in equal
Current edition approved Sept. 10, 2002. Published November 2002. Originally
published as D 2259 – 64 T. Last previous edition D 2259 – 97.
2
Annual Book of ASTM Standards, Vol 07.01.
3 4
Annual Book of ASTM Standards, Vol 07.02. Annual Book of ASTM Standards, Vol 14.02.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
D2259–02
numbers to each laboratory. The test results from the labora- 6.
...

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1.1 This test method describes the measurement of abrasion resistance properties for manufactured fiber yarns in dry and wet conditions.  
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5.1 This test method is considered satisfactory for acceptance testing of commercial shipments because current estimates of between-laboratory precision are acceptable and the method is used extensively in the trade for acceptance testing.  
5.1.1 If there are differences or practical significance between reported test results for two laboratories (or more), comparative tests should be performed to determine if there is a statistical bias between them, using competent statistical assistance. As a minimum, the test samples to be used are as homogeneous as possible, are drawn from the material from which the disparate test results are obtained, and are assigned randomly in equal numbers to each laboratory for testing. Other materials with established test values may be used for this purpose. The test results from the two laboratories should be compared using a statistical test for unpaired data, at a probability level chosen prior to the testing series. If a bias is found, either its cause must be found and corrected, or future test results must be adjusted in consideration of the known bias.  
5.2 Elapsed time between spinning and testing has a marked effect on the results of the draw tension test, especially during the first 24 h. Therefore, if tested within 24 h of spinning, specimens should be compared only if tested after the same elapsed time. No specimen should be tested within 4 h of spinning because the aging process is at its most rapid rate during this period, and the differences in rate due to fiber structure are most pronounced.  
5.3 The extension force of manufactured filament yarns is related to the alignment of the molecules in the yarn filaments, which influences the yarn processing behavior. Knowledge of this property of partially oriented yarn is useful to determine processing conditions.
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1.1 This test method covers the measurement of extension force developed while drawing a partially oriented filament yarn between pairs of draw rolls of different surface speeds.  
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ASTM D1059-17(2022)(Test Method)
Standard Test Method for Yarn Number Based on Short-Length Specimens

SIGNIFICANCE AND USE
5.1 This is a quick method used for the determination of the approximate yarn number of short-length specimens taken from packages or fabrics.  
5.2 Because any error present in the reported length of the specimen is multiplied many times when calculating the theoretical yarn number using Eq 2 or Eq 3, it is extremely important that the length be measured as precisely as practicable.  
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1.1 This test method covers the determination of the yarn number of all types of cotton, woolen, worsted, and man-made fiber yarns taken from packages; or from any textile fabrics in which the yarns are intact and can be removed in measurable lengths. The test method is not applicable to yarns taken from napped or cut pile fabrics. Because this test method is based on short-length specimens, the results should only be considered as approximations of yarn number.
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1.2 This test method is applicable to yarns which stretch less than 5 % when tension on yarn is increased from 0.25 to 0.75 cN/tex (0.25 to 0.75 gf/tex). By mutual agreement it may be adapted to yarns which stretch more than 5 % by use of tension lower than that specified in the method for elastomers or use of tension higher than that specified in the method to pull the crimp out of textured yarns.  
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
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5.1 This test method may be used for the acceptance testing of commercial shipments of yarns and cords. Caution is advised because yarn and cord may contract in length over a period of time due to room temperature retraction. Thermal shrinkage values are reduced proportionately by the amount of room temperature retraction.
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Standard Test Method for Crimp and Shrinkage Properties for Textured Yarns Using a Dynamic Textured Yarn Tester

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5.1 Test Method D6774, for determining maximum total contraction, crimp, and residual fiber shrinkage in textured filament yarns is suitable for acceptance testing of commercial shipments.  
5.1.1 If there are differences of practical significance between reported test results for two laboratories (or more), comparative tests should be performed to determine if there is a statistical bias between them, using competent statistical assistance. As a minimum, use the samples for such a comparative tests that are as homogeneous as possible, drawn from the same lot of material as the samples that resulted in disparate results during initial testing and randomly assigned in equal numbers to each laboratory. The test results from the laboratories involved should be compared using a statistical test for unpaired data, a probability level chosen prior to the testing series. If a bias is found, either its cause must be found and corrected, or future test results for that material must be adjusted in consideration of the known bias.  
5.2 The properties and their variability as measured by this method relate to bulk appearance, stretch and recovery of fabrics and dyeability of yarns.  
5.3 For some yarns, elapsed time between processing and testing has a marked effect on the results, of this test, especially during the first 72 h. The effect is caused by stress decay which is known to be minimal beyond the seventh day and after which time the yarn remains relatively stable. Therefore, specimens should only be compared if tested after the same elapsed time. Samples can be tested at-line, thus having little to no elapsed time between processing and testing.
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1.2 This test method is limited to crimped, multi-filament yarns ranging from 22.0 dtex to 890 dtex (15 denier to 800 denier) and for BCF yarns from 890 dtex to 4200 dtex (800 denier to 3800 denier).  
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Standard Test Method for Twist in Yarns by Direct-Counting

SIGNIFICANCE AND USE
5.1 Test Method D1423 for testing twist in yarns by direct-counting is considered satisfactory for acceptance testing of commercial shipments because current estimates of between-laboratory precision are acceptable and the method has been used extensively in the trade for acceptance testing.  
5.1.1 If there are differences of practical significance between reported test results for two laboratories (or more), comparative tests should be performed to determine if there is a statistical bias between them, using competent statistical assistance. As a minimum use the samples for such comparative tests as homogeneous as possible, drawn from the same lot of material that resulted in the disparate test results and randomly in equal numbers to each laboratory. The test results from the laboratories involved should be compared using a statistical test for unpaired data, at a probability level chosen prior to the testing series. If a bias is found, either its cause must be found and corrected, or future test results for that material must be adjusted in consideration of the known bias.  
5.2 The determination of twist in a straight section of a yarn is not the simple straightforward operation it appears to be, for the test results may be greatly influenced by variations in test procedures and techniques. In all manipulations, extreme care is necessary to prevent specimen rotation altering the twist level before testing begins.  
5.3 The twist in a yarn before it is packaged may be different from that of the yarn after it has been withdrawn from the package because of changes in tension and the effect of the method of withdrawal. If the yarn is withdrawn over-end, a slight increase or decrease in twist will take place, depending upon the direction of the twist in the yarn, the direction of winding on the package, and the length of the wrap on the package.  
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1.1 This test method covers the determination of the amount and direction of twist at the completion of any stage of twisting in single (spun or filament), plied, cabled, or novelty (exclusive of long-term repeat patterns) yarns. The procedures are designed primarily for yarns in packages, but, with special precautions, they are applicable to yarns taken from fabrics. The procedure for spun yarn in 9.2 is also applicable to rovings.  
1.2 For plied yarns, this test method covers the determination of the twist of the plied yarns and the twist of the single yarn before plying. For cabled yarns, the test method covers the determination of the cable or hawser twist; the twist of the plied yarn after plying, but prior to the last twisting operation; and the twist of the single yarn before plying. Procedures are also included for the determination of the twists of the single and plied yarn components as they lie in the final structure. Also, directions are included for the determination of twist in plied yarn made with direct cabling technology.  
1.3 This test method is not intended for yarns that extend more than 5.0 % when tension is increased from 2.5 to 7.5 mN/tex [0.25 to 0.75 gf/tex]. Following the procedures of this test method for such yarns would be independent of the bias and precision determined for this test method. The report from such testing should include the tension used for this testing.  
1.4 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.
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Note 2: This test method has been evaluated for use in de...

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ASTM D6612-00(2022)(Test Method)
Standard Test Method for Yarn Number and Yarn Number Variability Using Automated Tester

SIGNIFICANCE AND USE
5.1 Test Method D6612 for yarn number and yarn number variability is satisfactory for acceptance of commercial shipments and is used in the trade.  
5.1.1 If there are differences of practical significance between the reported test results for two or more laboratories, comparative tests should be performed by those laboratories to determine if there is a statistical bias between them, using competent statistical assistance. As a minimum, samples used for each comparative tests should be as homogeneous as possible, drawn from the same lot of material as the samples that results in disparate results during initial testing, and randomly assigned in equal numbers to each laboratory. Other fabrics with established tests values are used for this purpose. The test results from the laboratories involved should be compared appropriate statistical analysis and a probability level chosen by the two parties before testing begins, at a probability level chosen prior to the testing series. If a bias is found, either its cause must be found and corrected, or future test results adjusted in consideration of the known bias.  
5.1.2 The average results from the two laboratories should be compared using appropriate statistical analysis and a probability level chosen by the two parties before the testing is begun. If a bias is found, either its cause must be found and corrected or the purchaser and the supplier must agree to interpret future test results with consideration to the known bias.  
5.2 Test Method D6612 also is used for the quality control of filament yarns.  
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1.1 This test method covers the measurement of yarn number up to 4000 dtex (3600 denier) and related variability properties of filament and spun yarns using an automated tester with capability for measuring mass variability characteristics.  
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Note 1: For determination of yarn number by use of reel and balance, refer to Test Method D1907. For another method of measuring variability (unevenness) in yarn, refer to Test Method D1425.  
1.3 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore to ensure conformance with this standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D2258/D2258M-16(2022)(Practice)
Standard Practice for Sampling Yarn for Testing

SIGNIFICANCE AND USE
5.1 Assigning a value to any property of the material in a container or in a lot, consignment, or delivery involves a measurement process that includes both sampling and testing procedures. The correctness of the value assigned depends upon the variability due to testing and sampling plan. Even when the variability due to testing is minimized by carefully developed procedures, correct and consistent estimates of the true value of the property are possible only when the sampling procedure avoids systematic bias, minimizes variations due to sampling, and provides a laboratory sample of adequate size.  
5.2 Practice D2258 may not give the most efficient sampling plan that might be devised in special situations but does present a general procedure that gives satisfactory precision with an economical amount of sampling. Many plans that include stratified sampling can be found in textbooks and through the use of statistical software tools and calculators.  
5.2.1 If not specified by the purchaser, the manufacturer will define suitable production lots based on one or more of the following: supply lot, production shift/time segment, production equipment or production line, operator, designated shipment, production run, or a combination herein.  
5.2.2 If not specified by the purchaser, the manufacturer will define sampling and testing frequency based on the following: process capability or capability analysis, historical trends, level of detection rate required, confidence level requirements, known variations or special causes, or both. Every attempt to ensure conforming product is being produced, identify potential nonconforming product or proper isolation and identification, will be carried out by the manufacturer.  
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SCOPE
1.1 This practice describes a procedure for the division of shipments of yarn into test lots and the sampling of such lots for testing.  
1.1.1 This practice can be used for lot sample testing of yarns for both pre-fabric production and post-fabric production.  
1.2 This practice is applicable to single, plied, or cabled yarns, and cords, made of any fiber or mixture of fibers, and supported on any form of package, including beams.  
1.3 This practice also describes procedures for the sampling of yarn(s) removed from woven or knitted fabrics; however, when thus sampled, the yarns are usually not representative of entire shipments, as referred to in 1.1. Consequently, the resultant sampling can only be used to determine the characteristics of the yarn and is usually not used for acceptance testing. Moreover, it should be recognized that the characteristics of yarns from fabrics may be different than the characteristics of the same yarn(s), prior to being entered into the fabric manufacturing process.  
1.4 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical...

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ASTM
ASTM D3693-02(2021)(Specification)
Standard Specification for Labeled Length per Holder of Sewing Thread

ABSTRACT
This specification covers the requirements for the labeled lengths per holder of sewing threads of all materials. The test specimen is a thread holder whether a cone, tube, spool, ready-made bobbin, or any other holders. The observed length for all holders such as home sewing spools, ready-made bobbins, or all other holders which depends on the sampling size shall equal or exceed a certain percentage of the minimum allowable labeled length.
SCOPE
1.1 This specification covers requirements for the labeled lengths of sewing threads of all materials.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D2731-21(Test Method)
Standard Test Method for Elastic Properties of Elastomeric Yarns (CRE Type Tensile Testing Machines)

SIGNIFICANCE AND USE
5.1 This test method is considered satisfactory for acceptance testing of commercial shipments since current estimates of between-laboratory precision are acceptable and the method is used extensively in the trade for acceptance testing.  
5.1.1 If there are differences of practical significance between reported test results for two laboratories (or more), comparative tests should be performed to determine if there is a statistical bias between them, using competent statistical assistance. As a minimum, use samples for such comparative tests that are as homogeneous as possible, drawn from the same lot of material as the samples that resulted in disparate results during initial testing, and randomly assigned in equal numbers to each laboratory. The test results from the laboratories involved should be compared using a statistical test for unpaired data, at a probability level chosen prior to the testing series. If bias is found, either its cause must be found and corrected, or future test results for that material must be adjusted in consideration of the known bias.  
5.2 Force at Specified Elongation (FASE) is a measure of the tensile force occurring while extending a textile material within specified limits. This characteristic of elastomeric yarn indicates the resistance that will have to be overcome by the wearer while putting on a garment made of the material and is also an indication of the garment's resistance to deformation caused by normal body movements during wear. The elongations used for these measurements are typically 100 %, 200 % and 300 %.  
5.3 Permanent Deformation (set) is a measure of the increase in length of an elastomeric yarn resulting from cyclic stretching and relaxation. The characteristic is a visible indication of the realignment of intermolecular bonds within the elastic material. As with stress decay, the amount of set increases with yarn extension; however, for any particular extension, little or no additional set takes place after...
SCOPE
1.1 This test method covers the determination of elastic properties of “as produced” elastomeric yarns made from rubber, spandex or other elastomers. Elastic properties include force at specified elongations, permanent deformation and stress decay. Other hysteresis related properties can be calculated.
Note 1: For a method designed specifically for testing rubber threads, refer to Test Method D2433.  
1.2 This test method is not applicable to covered, wrapped, or core-spun yarns or yarns spun from elastomeric staple.  
1.3 This test method is applicable to elastomeric yarns having a range of 40 to 3200 dtex (36 to 2900 denier).  
1.4 The values stated in either SI units or U.S. Customary units are to be regarded separately as standard. Within the text, the U.S. Customary units are in parentheses. The values stated in each system are not exact equivalents; therefore, each system shall be used independently of the other.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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