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ASTM D5267-97

(Test Method)

Standard Test Method for Determination of Extrudability of Cartridge Adhesives

Standard Test Method for Determination of Extrudability of Cartridge Adhesives

SCOPE
1.1 This test method covers a means of measuring the amount of force necessary to extrude an adhesive from a cartridge at a given temperature.
1.2 The values stated in inch-pound units are to be regarded as the standard. The values given in parentheses are for information only.
1.3 This standard does not purport to address all of the safety problems, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
09-Mar-1997
ICS
83.180 - Adhesives
Technical Committee
D14 - Adhesives
Drafting Committee
D14.10 - Working Properties
Current Stage
Ref Project

Relations

Replaced By
ASTM D5267-97(2005) - Standard Test Method for Determination of Extrudability of Cartridge Adhesives
Effective Date
01-Oct-2005
Referred By
ASTM D6465-99(2016) - Standard Guide for Selecting Aerospace and General Purpose Adhesives and Sealants
Effective Date
10-Mar-1997

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ASTM D5267-97 - Standard Test Method for Determination of Extrudability of Cartridge AdhesivesASTM D5267-97 - Standard Test Method for Determination of Extrudability of Cartridge Adhesives
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ASTM D5267-97 - Standard Test Method for Determination of Extrudability of Cartridge Adhesives
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D5267–97
Standard Test Method for
Determination of Extrudability of Cartridge Adhesives
This standard is issued under the fixed designation D 5267; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This test method measures the amount of force neces-
sary to extrude an adhesive from a cartridge at a given
temperature.
1.2 The values stated in inch-pound units are to be regarded
as the standard. The values given in parentheses are for
information only.
1.3 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the
responsibility of the user of this standard to establish appro-
priate safety and health practices and determine the applica-
bility of regulatory limitations prior to use.
2. Referenced Documents
2.1 ASTM Standards:
D 907 Terminology of Adhesives
3. Terminology
3.1 Definitions—Many terms in this test method are defined
in Terminology D 907.
4. Significance and Use
4.1 Cartridge adhesives are typically used at job sites in a
wide variety of temperature ranges. These products may be
exposed to cold temperatures, where one of the limiting
application factors is whether the product can be extruded from
the cartridge.
4.2 The test method quantitatively measures the force nec-
essary to extrude a cartridge adhesive at a given temperature.
This provides the formulator with results that can assist in
FIG. 1 Test Fixture for Measuring Extrusion from Cartridge
formulation development and the end user with information for
use in selecting a product for general usage.
5. Apparatus
4.3 By measuring (the ease of) extrusion from the cartridge,
5.1 The test fixture is shown in Fig. 1. Details are shown in
the test method can also be used as a quality control tool to
Figs. 2-4. Make the framework from aluminum. Make the rod
measure the shelf life stability of a product.
and plunger combination from steel.
5.2 The test fixture is designed to be fitted onto a test
This test method is under the jurisdiction of ASTM Committee D-14 on
machine capable of measuring compressive strength.
Adhesives and is the direct responsibility of Subcommittee D14.10 on Working
Properties.
Current edition approved March 10, 1997. Published April 1998. Originally
published as D 5267 – 92. Last previous edition D 5267 – 92. The apparatus is also available from Browning Technology, Inc., 1256 Stanley
Annual Book of ASTM Standards, Vol 15.06. Ave., Dayton, OH 45404.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
D5267–97
FIG. 3 Cartridge Brace and Rear Support Assembly
FIG. 2 Base Support for Test Fixture
6. Conditioning
8.1.3 Temperature of adhesive.
6.1 Before measuring extrudability, condition the cartridge
8.1.4 Crosshead speed used for extrusion.
filled with adhesive until it reaches the desired constant
8.1.5 Force (in psi) used initially to extrude the adhesive
temperature.
from the cartridge and the average to maintain a constant flow
of adhesive.
7. Procedure
7.1 Mount the test fixture to the test machine for stability.
9. Precision and Bias
7.2 After conditioning the cartridge, cut off enough of the
9.1 Precision:
tip, perpendicular to the cartridge, to ensure an inside diameter
of ⁄4 in. (6.3 mm). If the cartridge has a foil or plastic liner,
9.1.1 Table1presentsroundrobindatageneratedfromthree
puncture it completely to
...

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Section  
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4.1 The purpose of this classification system is to provide a method of identifying adhesives in order to give industry a system that can be used universally for materials. It further provides a means for specifying these materials by the use of the standards that are developed using this guide.  
4.2 This classification system was developed to permit the addition of future adhesives.
SCOPE
1.1 This guide provides a classification system for tabulating the properties of adhesives suitable for holding parts or assemblies together. The use of this guide also provides information necessary for the development of standard specifications for adhesives.  
Note 1: This classification system may serve many of the needs of industries using adhesives. This guide is subject to revision as the need requires; therefore, the latest revision should always be used.  
1.2 Limitations—This classification system is intended to be a means of identifying adhesives. It is not intended for the selection of materials. Material selection should be made by those having expertise in the adhesives field after careful consideration of the design and the performance required of the part, the environment to which it will be exposed, the attachment process to be employed, the inherent properties of the material not covered in this document, and the economic factors.  
1.3 This classification system is based on the premise that adhesives can be arranged into broad generic families using basic properties to arrange the materials into groups, classes, and grades.  
1.4 In all cases where the provisions of this classification system would conflict with the referenced ASTM specification for a particular material, the latter shall take precedence.  
1.5 The values stated in SI units, as detailed in IEEE/ASTM SI 10, are to be regarded as the standard.  
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1.1 This terminology standard is a compilation of definitions used in the science and technology of the adhesives industry. Terms that are generally understood or adequately defined in other readily available sources are not included.  
1.2 Any changes in this standard since 1988 are documented as follows:  
1.2.1 Appendix X1 gives a history of revisions made since 1988. Table X1.1 lists the terms that are affected as: (1) Terms Added, (2) Terms Revised, and (3) Terms Deleted.
1.2.1.1 In Table X1.1, the year of publication in Volume 15.06 is shown in parentheses following the term.  
1.2.2 In the text of the standard, the year of publication is shown following each definition. Also, the following codes are included after the year of publication to describe the type change that was made: (A) Addition, (R) Revision, or (E) Edited.  
1.2.3 Deletions are shown in Appendix X1, suitably footnoted. The deleted terms do not appear in the text of the standard.  
1.2.4 Any special circumstances not covered by 1.2.2 and 1.2.3 are documented in Table X1.1, suitably footnoted.  
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