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ASTM D5832-98(2021)

(Test Method)

Standard Test Method for Volatile Matter Content of Activated Carbon Samples

Standard Test Method for Volatile Matter Content of Activated Carbon Samples

SIGNIFICANCE AND USE
5.1 Volatile matter, when determined as herein described, may be used as a relative measure of the extent of carbonization in an activated carbon and the extent of loading of volatile material on an activated carbon that has been used in an adsorption application.  
5.2 Combined with other information, the volatile matter of an activated carbon may be useful in evaluating its performance in an adsorption application.  
5.3 Other automated methods for the determination of the volatile content of solids, such as using a thermogravimetric analyzer (TGA), can be used in place of this test method with equally reliable results.
SCOPE
1.1 This test method covers the determination of the percentage of gaseous products, exclusive of moisture vapor, present in virgin and used activated carbons which are released under specific conditions of the test.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
31-May-2021
ICS
71.060.10 - Chemical elements
Technical Committee
D28 - Activated Carbon
Drafting Committee
D28.04 - Gas Phase Evaluation Tests
Current Stage
Ref Project

Relations

Refers
ASTM D3175-20 - Standard Test Method for Volatile Matter in the Analysis Sample of Coal and Coke
Effective Date
01-Feb-2020
Refers
ASTM D3175-18 - Standard Test Method for Volatile Matter in the Analysis Sample of Coal and Coke
Effective Date
01-Dec-2018
Refers
ASTM D3175-17 - Standard Test Method for Volatile Matter in the Analysis Sample of Coal and Coke
Effective Date
01-Feb-2017
Refers
ASTM D2652-11 - Standard Terminology Relating to Activated Carbon
Effective Date
15-Jun-2011
Refers
ASTM D3175-11 - Standard Test Method for Volatile Matter in the Analysis Sample of Coal and Coke
Effective Date
01-Apr-2011
Refers
ASTM D2867-09 - Standard Test Methods for Moisture in Activated Carbon
Effective Date
01-Nov-2009
Refers
ASTM D3175-07 - Standard Test Method for Volatile Matter in the Analysis Sample of Coal and Coke
Effective Date
01-Mar-2007
Refers
ASTM D2652-05a - Standard Terminology Relating to Activated Carbon
Effective Date
01-Jul-2005
Refers
ASTM D2652-05 - Standard Terminology Relating to Activated Carbon
Effective Date
01-Jun-2005
Refers
ASTM D2867-04 - Standard Test Methods for Moisture in Activated Carbon
Effective Date
01-Apr-2004
Refers
ASTM D3175-02 - Standard Test Method for Volatile Matter in the Analysis Sample of Coal and Coke
Effective Date
10-Sep-2002
Refers
ASTM D2652-94(1999) - Standard Terminology Relating to Activated Carbon
Effective Date
10-Feb-1999
Refers
ASTM D2867-99 - Standard Test Methods for Moisture in Activated Carbon
Effective Date
10-Feb-1999

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ASTM D5832-98(2021) - Standard Test Method for Volatile Matter Content of Activated Carbon SamplesASTM D5832-98(2021) - Standard Test Method for Volatile Matter Content of Activated Carbon Samples
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ASTM D5832-98(2021) - Standard Test Method for Volatile Matter Content of Activated Carbon Samples
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D5832 − 98 (Reapproved 2021)
Standard Test Method for
Volatile Matter Content of Activated Carbon Samples
This standard is issued under the fixed designation D5832; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope rigidly controlled conditions. The measured mass loss, cor-
rected for moisture as determined in Test Method D2867,
1.1 This test method covers the determination of the per-
establishes the volatile matter content of the activated carbon
centage of gaseous products, exclusive of moisture vapor,
sample.
present in virgin and used activated carbons which are released
under specific conditions of the test.
5. Significance and Use
1.2 The values stated in SI units are to be regarded as
5.1 Volatile matter, when determined as herein described,
standard. No other units of measurement are included in this
may be used as a relative measure of the extent of carboniza-
standard.
tion in an activated carbon and the extent of loading of volatile
1.3 This standard does not purport to address all of the
material on an activated carbon that has been used in an
safety concerns, if any, associated with its use. It is the
adsorption application.
responsibility of the user of this standard to establish appro-
5.2 Combined with other information, the volatile matter of
priate safety, health, and environmental practices and deter-
mine the applicability of regulatory limitations prior to use. an activated carbon may be useful in evaluating its perfor-
mance in an adsorption application.
1.4 This international standard was developed in accor-
dance with internationally recognized principles on standard-
5.3 Other automated methods for the determination of the
ization established in the Decision on Principles for the
volatile content of solids, such as using a thermogravimetric
Development of International Standards, Guides and Recom-
analyzer (TGA), can be used in place of this test method with
mendations issued by the World Trade Organization Technical
equally reliable results.
Barriers to Trade (TBT) Committee.
6. Apparatus
2. Referenced Documents
6.1 Crucible and Cover, high-temperature porcelain, high
2.1 ASTM Standards:
form, 30 cc capacity.
D2652 Terminology Relating to Activated Carbon
D2867 Test Methods for Moisture in Activated Carbon
6.2 Oven, forced-air circulation, capable of temperature
D3175 Test Method for Volatile Matter in the Analysis
regulation up to 250 °C.
Sample of Coal and Coke
6.3 Moisture Determination Apparatus, as described in Test
3. Terminology
Method D2867.
3.1 Definitions—For definitions of terms used in this test
6.4 Muffle Furnace, gravity circulation, capable of tempera-
method relating to activated carbon, refer to Terminology
ture regulation at 950 6 25 °C. An electric furnace similar to
D2652.
the one described in Test Method D3175 is suitable for use in
this test method.
4. Summary of Test Method
6.5 Desiccator, glass, with indicating type desiccant.
4.1 Volatile matter is determined by establishing the loss in
mass resulting from heating an activated carbon sample under
6.6 Balance, analytical, capable of 0.1 mg sensitivity.
This test method is under the jurisdiction of ASTM Committee D28 on
7. Hazards
Activated Carbon and is the direct responsibility of Subcommittee D28.04 on Gas
Phase Evaluation Tests.
7.1 Thefurnaceusedinthistestmethodshouldbelocatedin
Current edition approved June 1, 2021. Published June 2021. Originally
a well-ventilated area to eliminate exposure to possible toxic
approved in 1995. Last previous edition approved in 2014 as D5832 – 98 (2014).
vapors that may evolve from the carbon sample during the
DOI: 10.1520/D5832-98R21.
For referenced ASTM standards, visit the ASTM website, www.astm.org, or high-temperature heating.
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
7.2 Exercise care when working with the high-temperature
Standards volume information, refer to the standard’s Document Sum
...

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ASTM D2652-22(Terminology)
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2.1 This terminology ensures that terms peculiar to activated carbon are adequately defined so that other standards in which such terms are used can be understood and interpreted properly.  
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ASTM D3860-98(2020)(Practice)
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5.1 This practice is used when activated carbon is considered as an adsorbent in treating water. Since both granular and powdered activated carbons are commercially available, a standard practice is needed to ensure that the activated carbons are evaluated under the same test conditions. Specified particle size carbon is to be used to ensure that the same test conditions are used. The practice is generally performed at 20 °C; however, other temperatures may be used and noted.
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4.1 This test method is applicable only for determination of the volatile moisture content resulting from adsorption of water vapor from the atmosphere, and is not intended to give representative moisture data for graphite that has been exposed to liquid water contamination.
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ASTM D2652-22(Terminology)
Standard Terminology Relating to Activated Carbon

SIGNIFICANCE AND USE
2.1 This terminology ensures that terms peculiar to activated carbon are adequately defined so that other standards in which such terms are used can be understood and interpreted properly.  
2.2 This terminology is useful to those who are not conversant with the terms related to activated carbon. However, it is also a ready reference for those directly associated with activated carbon to resolve differences and ensure commonality of usage, particularly in the preparation of ASTM standards.  
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1.3 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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