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ASTM D5772-17

(Test Method)

Standard Test Method for Cloud Point of Petroleum Products and Liquid Fuels (Linear Cooling Rate Method)

Standard Test Method for Cloud Point of Petroleum Products and Liquid Fuels (Linear Cooling Rate Method)

SIGNIFICANCE AND USE
5.1 For petroleum products and diesel fuels, the cloud point is an index of the lowest temperature of its utility for certain applications. Wax crystals of sufficient quantity can plug filters used in some fuel systems.  
5.2 Petroleum blending operations require precise measurement of the cloud point.  
5.3 This test method can determine the temperature of the test specimen at which wax crystals have formed sufficiently to be observed as a cloud, with a resolution of 0.1 °C.  
5.4 This test method provides results that when rounded to the next lower integer are equivalent to Test Method D2500.  
5.5 This test method is more precise than Test Method D2500.
SCOPE
1.1 This test method covers the description of the determination of the cloud point of petroleum products and biodiesel fuels that are transparent in layers 40 mm in thickness by an automatic instrument using a linear cooling rate.  
1.2 This test method covers the range of temperatures from −60 °C to 49 °C with temperature resolution of 0.1 °C, however, the range of temperatures included in the 1997 interlaboratory cooperative test program only covered the temperature range of –56 °C to +34 °C.  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Historical
Publication Date
30-Apr-2017
ICS
75.080 - Petroleum products in general
Technical Committee
D02 - Petroleum Products, Liquid Fuels, and Lubricants
Drafting Committee
D02.07 - Flow Properties
Current Stage
Ref Project

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ASTM D5772-17 - Standard Test Method for Cloud Point of Petroleum Products and Liquid Fuels (Linear Cooling Rate Method)ASTM D5772-17 - Standard Test Method for Cloud Point of Petroleum Products and Liquid Fuels (Linear Cooling Rate Method)
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D5772 − 17
Designation: IP 445/09
Standard Test Method for
Cloud Point of Petroleum Products and Liquid Fuels (Linear
1
Cooling Rate Method)
This standard is issued under the fixed designation D5772; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
INTRODUCTION
This test method describes an alternative procedure for the determination of cloud point of
petroleum products of Test Method D2500/IP 219 using an automatic apparatus. The temperature
results from this test method have been found to be equivalent to Test Method D2500/IP 219. When
specification requires Test Method D2500/IP 219, do not substitute this test method or any other
method without obtaining comparative data and agreement from the specifier.
1. Scope* 2. Referenced Documents
2
2.1 ASTM Standards:
1.1 This test method covers the description of the determi-
D2500Test Method for Cloud Point of Petroleum Products
nation of the cloud point of petroleum products and biodiesel
and Liquid Fuels
fuels that are transparent in layers 40mm in thickness by an
D4057Practice for Manual Sampling of Petroleum and
automatic instrument using a linear cooling rate.
Petroleum Products
1.2 This test method covers the range of temperatures from
D4177Practice for Automatic Sampling of Petroleum and
−60°C to 49°C with temperature resolution of 0.1°C,
Petroleum Products
however, the range of temperatures included in the 1997
2.2 Energy Institute Standard:
interlaboratory cooperative test program only covered the
3
IP219Test Method for Cloud Point of Petroleum Products
temperature range of –56°C to +34°C.
1.3 The values stated in SI units are to be regarded as
3. Terminology
standard. No other units of measurement are included in this
3.1 Definitions:
standard.
3.1.1 biodiesel, n—afuelcomprisedofmono-alkylestersof
1.4 This standard does not purport to address all of the
long-chain fatty acids derived from vegetable oils or animal
safety concerns, if any, associated with its use. It is the
fats, designated B100.
responsibility of the user of this standard to establish appro-
3.1.1.1 Discussion—Biodiesel is typically produced by a
priate safety and health practices and determine the applica-
reaction of vegetable oil or animal fat with an alcohol such as
bility of regulatory limitations prior to use.
methanol or ethanol in the presence of a catalyst to yield
1.5 This international standard was developed in accor- mono-estersandglycerin.Thefueltypicallymaycontainupto
14differenttypesoffattyacidsthatarechemicallytransformed
dance with internationally recognized principles on standard-
ization established in the Decision on Principles for the into fatty acid methyl esters (FAME).
Development of International Standards, Guides and Recom-
3.1.2 biodiesel blend, n—a blend of biodiesel fuel with
mendations issued by the World Trade Organization Technical
petroleum-based diesel fuel designated BXX, where XX is the
Barriers to Trade (TBT) Committee.
volume percentage of biodiesel.
1 2
This test method is under the jurisdiction of ASTM Committee D02 on For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Petroleum Products, Liquid Fuels, and Lubricants and is the direct responsibility of contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
Subcommittee D02.07 on Flow Properties. Standards volume information, refer to the standard’s Document Summary page on
Current edition approved May 1, 2017. Published May 2017. Originally the ASTM website.
3
approved in 1995. Last previous edition approved in 2015 as D5772–15. DOI: Available from Energy Institute, 61 New Cavendish St., London, WIG 7AR,
10.1520/D5772-17. U.K., http://www.energyinst.org.uk.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D5772 − 17
3.1.3 cloud point, n—in petroleum products and biodiesel lization of the wax in the specimen is detected by the optical
fuels, the temperature of a liquid specimen when the smallest barrier, is recorded with a resolution of 0.1°C. The specimen
observable cluster of wax crystals first occurs upon cooling is then heated to the original starting temperature.
under prescribed conditions.
3.1.3.1 Discussion—The cloud point occurs when the tem-
5. Significance and Use
perature of the specimen is low enough to cause wax crystals
5.1 For petroleum products and diesel fuels, the cloud point
to precipitate. In a homogeneous liquid, the cloud is always
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D5772 − 15 D5772 − 17
Designation: IP 445/09
Standard Test Method for
Cloud Point of Petroleum Products and Liquid Fuels (Linear
1
Cooling Rate Method)
This standard is issued under the fixed designation D5772; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
INTRODUCTION
This test method describes an alternative procedure for the determination of cloud point of
petroleum products of Test Method D2500/IP 219 using an automatic apparatus. The temperature
results from this test method have been found to be equivalent to Test Method D2500/IP 219. When
specification requires Test Method D2500/IP 219, do not substitute this test method or any other
method without obtaining comparative data and agreement from the specifier.
1. Scope*
1.1 This test method covers the description of the determination of the cloud point of petroleum products and biodiesel fuels
that are transparent in layers 40 mm in thickness by an automatic instrument using a linear cooling rate.
1.2 This test method covers the range of temperatures from −60 °C to 49 °C with temperature resolution of 0.1 °C, however,
the range of temperatures included in the 1997 interlaboratory cooperative test program only covered the temperature range of
–56 °C to +34 °C.
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
1.5 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
D2500 Test Method for Cloud Point of Petroleum Products and Liquid Fuels
D4057 Practice for Manual Sampling of Petroleum and Petroleum Products
D4177 Practice for Automatic Sampling of Petroleum and Petroleum Products
2.2 Energy Institute Standard:
3
IP 219 Test Method for Cloud Point of Petroleum Products
3. Terminology
3.1 Definitions:
1
This test method is under the jurisdiction of ASTM Committee D02 on Petroleum Products, Liquid Fuels, and Lubricants and is the direct responsibility of Subcommittee
D02.07 on Flow Properties.
Current edition approved April 1, 2015May 1, 2017. Published April 2015May 2017. Originally approved in 1995. Last previous edition approved in 20102015 as
D5772 – 10.D5772 – 15. DOI: 10.1520/D5772-15.10.1520/D5772-17.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
3
Available from Energy Institute, 61 New Cavendish St., London, WIG 7AR, U.K., http://www.energyinst.org.uk.
*A Summary of Changes section appears at the end of this standard
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D5772 − 17
3.1.1 biodiesel, n—a fuel comprised of mono-alkyl esters of long-chain fatty acids derived from vegetable oils or animal fats,
designated B100.
3.1.1.1 Discussion—
Biodiesel is typically produced by a reaction of vegetable oil or animal fat with an alcohol such as methanol or ethanol in the
presence of a catalyst to yield-mono-esters yield mono-esters and glycerin. The fuel typically may contain up to 14 different types
of fatty acids that are chemically transformed into fatty acid methyl esters (FAME).
3.1.2 biodiesel blend, n—a blend of biodiesel fuel with petroleum-based diesel fuel designated BXX, where XX is the volume
percentage of biodiesel.
3.1.3 cloud point, n—in petroleum products and biodiesel fuels, the temperature of a liquid specimen when the smallest
observable cluster of hydrocarbonwax crystals first occurs upon cooling under prescribed conditions.
3.1.3.1 Discussion—
The cloud point o
...

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SCOPE
1.1 This practice covers the procedures for calculating the estimated kinematic viscosity of a blend of two or more petroleum products, such as lubricating oil base stocks, fuel components, residual fuel oil with kerosene, crude oils, and related products, from their kinematic viscosities and blend fractions.  
1.2 This practice allows for the estimation of the fraction of each of two petroleum products needed to prepare a blend meeting a specific viscosity.  
1.3 This practice may not be applicable to other types of products, or to materials which exhibit strong non-Newtonian properties, such as viscosity index improvers, additive packages, and products containing particulates.  
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 Logarithms may be either common logarithms or natural logarithms, as long as the same are used consistently. This practice uses common logarithms. If natural logarithms are used, the inverse function, exp(×), must be used in place of the base 10 exponential function, 10×, used herein.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and to determine the applicability of regulatory limitations prior to use.  
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ASTM
ASTM D4952-23(Test Method)
Standard Test Method for Qualitative Analysis for Active Sulfur Species in Fuels and Solvents (Doctor Test)

SIGNIFICANCE AND USE
5.1 Sulfur present as mercaptans or as hydrogen sulfide in distillate fuels and solvents can attack many metallic and non-metallic materials in fuel and other distribution systems. A negative result in the doctor test ensures that the concentration of these compounds is insufficient to cause such problems in normal use.
SCOPE
1.1 This test method covers and is intended primarily for the detection of mercaptans in motor fuel, kerosine, and similar petroleum products. This method may also provide information on hydrogen sulfide and elemental sulfur that may be present in these sample types.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  For specific warning statements, see 7.3.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM D2887-23(Test Method)
Standard Test Method for Boiling Range Distribution of Petroleum Fractions by Gas Chromatography

SIGNIFICANCE AND USE
5.1 The boiling range distribution of petroleum fractions provides an insight into the composition of feedstocks and products related to petroleum refining processes. The gas chromatographic simulation of this determination can be used to replace conventional distillation methods for control of refining operations. This test method can be used for product specification testing with the mutual agreement of interested parties.  
5.2 Boiling range distributions obtained by this test method are essentially equivalent to those obtained by true boiling point (TBP) distillation (see Test Method D2892). They are not equivalent to results from low efficiency distillations such as those obtained with Test Method D86 or D1160.  
5.3 Procedure B was tested with biodiesel mixtures and reports the Boiling Point Distribution of FAME esters of vegetable and animal origin mixed with ultra low sulfur diesel.
SCOPE
1.1 This test method covers the determination of the boiling range distribution of petroleum products. The test method is applicable to petroleum products and fractions having a final boiling point of 538 °C (1000 °F) or lower at atmospheric pressure as measured by this test method. This test method is limited to samples having a boiling range greater than 55.5 °C (100 °F), and having a vapor pressure sufficiently low to permit sampling at ambient temperature.
Note 1: Since a boiling range is the difference between two temperatures, only the constant of 1.8 °F/°C is used in the conversion of the temperature range from one system of units to another.  
1.1.1 Procedure A (Sections 6 – 14)—Allows a larger selection of columns and analysis conditions such as packed and capillary columns as well as a Thermal Conductivity Detector in addition to the Flame Ionization Detector. Analysis times range from 14 min to 60 min.  
1.1.2 Procedure B (Sections 15 – 23)—Is restricted to only 3 capillary columns and requires no sample dilution. In addition, Procedure B is used not only for the sample types described in Procedure A but also for the analysis of samples containing biodiesel mixtures B5, B10, and B20. The analysis time, when using Procedure B (Accelerated D2887), is reduced to about 8 min.  
1.2 This test method is not to be used for the analysis of gasoline samples or gasoline components. These types of samples must be analyzed by Test Method D7096.  
1.3 The values stated in SI units are to be regarded as standard. The values given in parentheses after SI units are provided for information only and are not considered standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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