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ASTM D5766/D5766M-23

(Test Method)

Standard Test Method for Open-Hole Tensile Strength of Polymer Matrix Composite Laminates

Standard Test Method for Open-Hole Tensile Strength of Polymer Matrix Composite Laminates

SIGNIFICANCE AND USE
5.1 Refer to Guide D8509.
SCOPE
1.1 This test method determines the open-hole tensile strength of multidirectional polymer matrix composite laminates reinforced by high-modulus fibers. The composite material forms are limited to continuous-fiber or discontinuous-fiber (tape or fabric, or both) reinforced composites in which the laminate is balanced and symmetric with respect to the test direction. The range of acceptable test laminates and thicknesses are described in 8.2.1.  
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the two systems may result in non-conformance with the standard.  
1.2.1 Within the text the inch-pound units are shown in brackets.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
31-Aug-2023
ICS
83.120 - Reinforced plastics
Technical Committee
D30 - Composite Materials
Drafting Committee
D30.05 - Structural Test Methods
Current Stage
Ref Project

Relations

Refers
ASTM D5229/D5229M-20 - Standard Test Method for Moisture Absorption Properties and Equilibrium Conditioning of Polymer Matrix Composite Materials
Effective Date
01-Mar-2020

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Standards Content (Sample)

This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D5766/D5766M − 23
Standard Test Method for
Open-Hole Tensile Strength of Polymer Matrix Composite
1
Laminates
This standard is issued under the fixed designation D5766/D5766M; the number immediately following the designation indicates the
year of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last
reapproval. A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope tive Density) of Plastics by Displacement
D883 Terminology Relating to Plastics
1.1 This test method determines the open-hole tensile
D2584 Test Method for Ignition Loss of Cured Reinforced
strength of multidirectional polymer matrix composite lami-
Resins
nates reinforced by high-modulus fibers. The composite mate-
D2734 Test Methods for Void Content of Reinforced Plastics
rial forms are limited to continuous-fiber or discontinuous-fiber
D3039/D3039M Test Method for Tensile Properties of Poly-
(tape or fabric, or both) reinforced composites in which the
mer Matrix Composite Materials
laminate is balanced and symmetric with respect to the test
D3171 Test Methods for Constituent Content of Composite
direction. The range of acceptable test laminates and thick-
Materials
nesses are described in 8.2.1.
D3878 Terminology for Composite Materials
1.2 The values stated in either SI units or inch-pound units
D5229/D5229M Test Method for Moisture Absorption Prop-
are to be regarded separately as standard. The values stated in
erties and Equilibrium Conditioning of Polymer Matrix
each system may not be exact equivalents; therefore, each
Composite Materials
system shall be used independently of the other. Combining
D8509 Guide for Test Method Selection and Test Specimen
values from the two systems may result in non-conformance
Design for Bolted Joint Related Properties
with the standard.
E6 Terminology Relating to Methods of Mechanical Testing
1.2.1 Within the text the inch-pound units are shown in
E177 Practice for Use of the Terms Precision and Bias in
brackets.
ASTM Test Methods
1.3 This standard does not purport to address all of the
E456 Terminology Relating to Quality and Statistics
safety concerns, if any, associated with its use. It is the E691 Practice for Conducting an Interlaboratory Study to
responsibility of the user of this standard to establish appro-
Determine the Precision of a Test Method
priate safety, health, and environmental practices and deter-
E1309 Guide for Identification of Fiber-Reinforced
mine the applicability of regulatory limitations prior to use. Polymer-Matrix Composite Materials in Databases (With-
3
1.4 This international standard was developed in accor-
drawn 2015)
dance with internationally recognized principles on standard- E1434 Guide for Recording Mechanical Test Data of Fiber-
ization established in the Decision on Principles for the
Reinforced Composite Materials in Databases (Withdrawn
3
Development of International Standards, Guides and Recom- 2015)
mendations issued by the World Trade Organization Technical
3. Terminology
Barriers to Trade (TBT) Committee.
3.1 Definitions—Terminology D3878 defines terms relating
2. Referenced Documents
to high-modulus fibers and their composites. Terminology
2
D883 defines terms relating to plastics. Terminology E6 defines
2.1 ASTM Standards:
terms relating to mechanical testing. Terminology E456 and
D792 Test Methods for Density and Specific Gravity (Rela-
Practice E177 define terms relating to statistics. In the event of
a conflict between terms, Terminology D3878 shall have
1
This test method is under the jurisdiction of ASTM Committee D30 on precedence over the other standards.
Composite Materials and is the direct responsibility of Subcommittee D30.05 on
3.2 Definitions of Terms Specific to This Standard—Refer to
Structural Test Methods.
Guide D8509.
Current edition approved Sept. 1, 2023. Published September 2023. Originally
approved in 1995. Last previous edition approved in 2018 as D5766/
3.3 Symbols:
D5766M – 11 (2018). DOI: 10.1520/D5766_D5766M-23.
A = cross-sectional area of a specimen
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
3
Standards volume information, refer to the standard’s Document Summary page on The last approved version of this historical standard is referenced on
the ASTM website. www.astm.org.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D5766/D5766M − 23
CV = coefficient of variation statist
...

This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D5766/D5766M − 11 (Reapproved 2018) D5766/D5766M − 23
Standard Test Method for
Open-Hole Tensile Strength of Polymer Matrix Composite
1
Laminates
This standard is issued under the fixed designation D5766/D5766M; the number immediately following the designation indicates the
year of original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last
reapproval. A superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This test method determines the open-hole tensile strength of multidirectional polymer matrix composite laminates reinforced
by high-modulus fibers. The composite material forms are limited to continuous-fiber or discontinuous-fiber (tape or fabric, or
both) reinforced composites in which the laminate is balanced and symmetric with respect to the test direction. The range of
acceptable test laminates and thicknesses are described in 8.2.1.
1.2 The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each
system may not be exact equivalents; therefore, each system shall be used independently of the other. Combining values from the
two systems may result in non-conformance with the standard.
1.2.1 Within the text the inch-pound units are shown in brackets.
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of
regulatory limitations prior to use.
1.4 This international standard was developed in accordance with internationally recognized principles on standardization
established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued
by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
2. Referenced Documents
2
2.1 ASTM Standards:
D792 Test Methods for Density and Specific Gravity (Relative Density) of Plastics by Displacement
D883 Terminology Relating to Plastics
D2584 Test Method for Ignition Loss of Cured Reinforced Resins
D2734 Test Methods for Void Content of Reinforced Plastics
D3039/D3039M Test Method for Tensile Properties of Polymer Matrix Composite Materials
D3171 Test Methods for Constituent Content of Composite Materials
D3878 Terminology for Composite Materials
D5229/D5229M Test Method for Moisture Absorption Properties and Equilibrium Conditioning of Polymer Matrix Composite
Materials
D8509 Guide for Test Method Selection and Test Specimen Design for Bolted Joint Related Properties
1
This test method is under the jurisdiction of ASTM Committee D30 on Composite Materials and is the direct responsibility of Subcommittee D30.05 on Structural Test
Methods.
Current edition approved June 1, 2018Sept. 1, 2023. Published July 2018September 2023. Originally approved in 1995. Last previous edition approved in 20112018 as
D5766/D5766M – 11.D5766/D5766M – 11 (2018). DOI: 10.1520/D5766_D5766M-11R18.10.1520/D5766_D5766M-23.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
D5766/D5766M − 23
E6 Terminology Relating to Methods of Mechanical Testing
E177 Practice for Use of the Terms Precision and Bias in ASTM Test Methods
E456 Terminology Relating to Quality and Statistics
E691 Practice for Conducting an Interlaboratory Study to Determine the Precision of a Test Method
3
E1309 Guide for Identification of Fiber-Reinforced Polymer-Matrix Composite Materials in Databases (Withdrawn 2015)
3
E1434 Guide for Recording Mechanical Test Data of Fiber-Reinforced Composite Materials in Databases (Withdrawn 2015)
3. Terminology
3.1 Definitions—Terminology D3878 defines terms relating to high-modulus fibers and their composites. Terminology D883
defines terms relating to plastics. Terminology E6 defines terms relating to mechanical testing. Terminology E456 and Practice
E177 define terms relating to statistics. In the event of a conflict between terms, Terminology D3878 shall have precedence over
the other standards.
3.2 Definitions of Terms Specific to This Stand
...

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SIGNIFICANCE AND USE
5.1 Susceptibility to damage from concentrated out-of-plane forces is one of the major design concerns of many structures made of advanced composite laminates. Knowledge of the damage resistance and damage tolerance properties of a laminated composite plate is useful for product development and material selection.  
5.2 The residual strength data obtained using this test method is most commonly used in material specifications and research and development activities. The data are not intended for use in establishing design allowables, as the results are specific to the geometry and physical conditions tested and are generally not scalable to other configurations. Its usefulness in establishing quality assurance requirements is also limited, due to the inherent variability of induced damage, as well as the dependency of damage tolerance response upon the pre-existent damage state.  
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ASTM D7766/D7766M-23(Practice)
Standard Practice for Damage Resistance Testing of Sandwich Constructions

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5.1 This practice provides supplemental instructions that allow Test Methods D6264/D6264M (for quasi-static indentation testing) and D7136/D7136M (for drop-weight impact testing) to determine damage resistance properties of sandwich constructions. Susceptibility to damage from concentrated out-of-plane forces is one of the major design concerns of many structures made using sandwich constructions. Knowledge of the damage resistance properties of a sandwich panel is useful for product development and material selection.  
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FIG. 1 Quasi-Static Indentation Test  
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1.6 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.6.1 Within the text, the inch-pound units are shown in brackets.  
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
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Standard Test Method for Compressive Residual Strength Properties of Damaged Sandwich Composite Panels

SIGNIFICANCE AND USE
5.1 Susceptibility to damage from concentrated out-of-plane forces is one of the major design concerns of many structures made of sandwich constructions. Knowledge of the damage resistance and residual strength properties of a sandwich construction is useful for product development and material selection.  
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5.3 The properties obtained using this test method can provide guidance in regard to the anticipated residual strength capability of sandwich constructions of similar facesheet and core material, adhesive, facesheet and core thickness, facesheet stacking sequence, and so forth. However, it must be understood that the residual strength of sandwich constructions is highly dependent upon several factors including geometry, thickness, stiffness, support conditions, and so forth. Significant differences in the relationships between the damage state and the residual compressive strength can result due to differences in these parameters.  
5.4 The compression strength from this test may not be equivalent to the compression strength of sandwich structures subjected to flexural compression testing.  
5.5 The reporting section requires items that tend to influence residual compressive strength to be reported; these include the following: facesheet and core materials, core density, cell size and wall thickness if applicable, film adhesive, methods of material fabrication, accuracy of lay-up orientation, facesheet stacking sequence and thickness, core thickness, overall specimen thickness, specimen geometry, specimen preparation, specimen conditioning, environment of testing, type, size and location of damage (including method of non-destructive inspection), specimen/fixture alignment and gripping, time at temperature, and speed of testing.  
5.6 Results from the residual strength assessmen...
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1.1 This test method covers compression residual strength properties of sandwich constructions that have been subjected to quasi-static indentation or drop-weight impact per Practice D7766/D7766M.
Note 1: When used to determine the residual strength of drop-weight impacted plates, this test method is commonly referred to as the Sandwich Compression After Impact test method.  
1.2 Several important test specimen parameters (for example, facesheet thickness, core thickness, and core density) are not mandated by this test method; however, repeatable results require that these parameters be specified and reported.  
1.3 The method utilizes a flat, rectangular specimen, previously subjected to a damaging event, which is tested under edgewise compressive loading using a stabilization fixture.  
1.4 The properties generated by this test method are highly dependent upon several factors, which include; specimen geometry, sandwich component materials and dimensions (facesheet, core, and adhesive), methods of fabrication, the type, size, and location of damage and boundary conditions. Thus, results are generally not scalable to other sandwich constructions, and are particular to the combination of geometric and physical conditions tested.  
1.5 This test method can be used to test undamaged specimens, but care should be taken to prevent undesirable failure modes such as end crushing. Test Methods C364 and D7249/D7249M are the recommended test methods for undamaged sandwich panel compression strength by edgewise compression or long beam flexure, respectively.  
1.6 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.6.1 Within the text, t...

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ASTM
ASTM D7291/D7291M-22(Test Method)
Standard Test Method for Through-Thickness “Flatwise” Tensile Strength and Elastic Modulus of a Fiber-Reinforced Polymer Matrix Composite Material

SIGNIFICANCE AND USE
5.1 This test method is designed to produce through-thickness failure data for structural design and analysis, quality assurance, and research and development. Factors that influence the through-thickness tensile strength, and should therefore be reported, include the following: material and fabric reinforcement, methods of material and fabric preparation, methods of processing and specimen fabrication, specimen stacking sequence, specimen conditioning, environment of testing, specimen alignment, speed of testing, time at temperature, void content, and volume reinforcement content.
SCOPE
1.1 This test method determines the through-thickness “flatwise” tensile strength and elastic modulus of fiber reinforced polymer matrix composite materials. A tensile force is applied normal to the plane of the composite laminate using adhesively bonded thick metal end-tabs. The composite material forms are limited to continuous fiber (unidirectional reinforcement or two-dimensional fabric) or discontinuous fiber (nonwoven or chopped) reinforced composites.  
1.2 The through-thickness strength results using this test method will in general not be comparable to Test Method D6415 since this method subjects a relatively large volume of material to an almost uniform stress field while Test Method D6415 subjects a small volume of material to a non-uniform stress field.  
1.3 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.3.1 Within the text, the inch-pound units are shown in brackets.  
1.4 This standard may involve hazardous materials, operations, and equipment.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM C365/C365M-22(Test Method)
Standard Test Method for Flatwise Compressive Properties of Sandwich Cores

SIGNIFICANCE AND USE
5.1 Flatwise compressive strength and modulus are fundamental mechanical properties of sandwich cores that are used in designing sandwich panels. Deformation data can be obtained, and from a complete force versus deformation curve, it is possible to compute the compressive stress at any applied force (such as compressive stress at proportional limit force or compressive strength at the maximum force) and to compute the effective modulus of the core.  
5.2 This test method provides a standard method of obtaining the flatwise compressive strength and modulus for sandwich core structural design properties, material specifications, research and development applications, and quality assurance.  
5.3 In order to prevent local crushing of some honeycomb cores, it is often desirable to stabilize the facing plane surfaces with a suitable material, such as a thin layer of resin or thin facings. Flatwise compressive strength data may be generated using either stabilized specimens (reported as stabilized compression strength) or non-stabilized specimens (reported as bare compression strength). It is customary aerospace industry practice to determine compression modulus only when using stabilized specimens.  
5.4 Factors that influence the flatwise compressive strength and shall therefore be reported include the following: core material, methods of material fabrication, core geometry (cell size), core density, specimen geometry, specimen preparation, specimen conditioning, environment of testing, specimen alignment, loading procedure, and speed of testing.
SCOPE
1.1 This test method covers the determination of compressive strength and modulus of sandwich cores. These properties are usually determined for design purposes in a direction normal to the plane of the face sheets (also referred to as the facing plane) as the core would be placed in a structural sandwich construction. The test procedures pertain to compression in this direction in particular, but also can be applied with possible minor variations to determining compressive properties in other directions. Permissible core material forms include those with continuous bonding surfaces (such as balsa wood and foams) as well as those with discontinuous bonding surfaces (such as honeycomb).  
1.2 This test method does not cover the determination of compressive core crush properties. Reference Test Method D7336/D7336M for determination of static energy absorption properties of honeycomb sandwich core materials.  
1.3 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.3.1 Within the text, the inch-pound units are shown in brackets.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM
ASTM C366/C366M-16(2022)e1(Test Method)
Standard Test Methods for Measurement of Thickness of Sandwich Cores

SIGNIFICANCE AND USE
5.1 Normally, a close tolerance is desirable for core thickness so that sandwich panels may be manufactured with all the sandwich components fitting properly and without crushing the core.  
5.2 These test methods are designed for measuring thickness of core as it is produced and are not intended for use in determining dimensions of core specimens for other tests.  
5.3 These test methods provide standard methods of obtaining the core thickness of flat sandwich core materials, and provide a basis for determining average thickness dimensions. The thickness properties derived may be used in design properties, material specifications, research and development applications, and quality assurance.  
5.4 Factors that influence core thickness measurement and shall therefore be reported include the following: core material through-thickness rigidity, surface roughness, specimen geometry (including warpage), specimen preparation, methods of dimensional measurement, specimen conditioning, and moisture content during dimensional measurements.
SCOPE
1.1 These test methods cover plant manufacturing procedures for measuring the thickness of flat sandwich cores. Permissible core material forms include those with continuous bonding surfaces (such as balsa wood and foams) as well as those with discontinuous bonding surfaces (such as honeycomb). The two test methods covered include the following:  
1.1.1 Test Method A—Roller-Type Thickness Tester.  
1.1.2 Test Method B—Disk-Type Thickness Tester.
Note 1: These test methods are designed for measuring thickness of core as it is produced and are not intended for use in determining dimensions of core specimens for other tests.  
1.2 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.2.1 Within the text, the inch-pound units are shown in brackets.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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ASTM D3800-22(Test Method)
Standard Test Method for Density of High-Modulus Fibers

SIGNIFICANCE AND USE
5.1 Fiber density is useful in the evaluation of new materials at the research and development level and is one of the material properties normally given in fiber specifications.  
5.2 Fiber density is used to determine fiber strength and modulus of both a fiber bundle and an individual filament. These properties are based on load or modulus slope over an effective area. Fiber density may be used with lineal mass of the fiber to give an approximation of effective tow area. Tow area divided by the average number of filaments in a tow gives an approximation of the effective area of an individual filament.  
5.3 Fiber density is used as a constituent property when determining reinforcement volume and void volume based on reinforcement mass and laminate density.
SCOPE
1.1 This test method covers the determination of the density of high-modulus fibers and is applicable to both continuous and discontinuous fibers.  
1.2 Units—The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard may involve hazardous materials, operations, and equipment. This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. See Section 9 for additional information.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

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