iTeh StandardsiTeh Standards
EURUSD
Your shopping cart is empty.
ASTM

ASTM F318-04

(Practice)

Standard Practice for Sampling Airborne Particulate Contamination in Clean Rooms for Handling Aerospace Fluids

Standard Practice for Sampling Airborne Particulate Contamination in Clean Rooms for Handling Aerospace Fluids

SCOPE
1.1 This practice covers a procedure for sampling airborne particulate matter larger than 5 µm in size. The method is designed to be used in specific areas, commonly called "clean rooms" in the aerospace industry where aerospace fluids are handled.
Note--Practice F50 is an alternative procedure.
1.2  This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.

General Information

Status
Historical
Publication Date
31-Aug-2004
ICS
13.040.30 - Workplace atmospheres
Technical Committee
E21 - Space Simulation and Applications of Space Technology
Drafting Committee
E21.05 - Contamination
Current Stage
Ref Project

Relations

Replaces
ASTM F318-78(2000) - Standard Practice for Sampling Airborne Particulate Contamination in Clean Rooms for Handling Aerospace Fluids
Effective Date
01-Sep-2004
Replaced By
ASTM F318-06 - Standard Practice for Sampling Airborne Particulate Contamination in Cleanrooms for Handling Aerospace Fluids
Effective Date
01-Apr-2006
Referred By
ASTM E2352-19 - Standard Practice for Aerospace Cleanrooms and Associated Controlled Environments—Cleanroom Operations
Effective Date
01-Sep-2004
Referred By
ASTM F312-08(2023) - Standard Test Methods for Microscopical Sizing and Counting Particles from Aerospace Fluids on Membrane Filters
Effective Date
01-Sep-2004

Buy Standard

ASTM F318-04 - Standard Practice for Sampling Airborne Particulate Contamination in Clean Rooms for Handling Aerospace FluidsASTM F318-04 - Standard Practice for Sampling Airborne Particulate Contamination in Clean Rooms for Handling Aerospace Fluids
PreviousNext
Standard
ASTM F318-04 - Standard Practice for Sampling Airborne Particulate Contamination in Clean Rooms for Handling Aerospace Fluids
English language
3 pages
sale 15% off
Preview
sale 15% off
Preview

Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:F318–04
Standard Practice for
Sampling Airborne Particulate Contamination in Cleanrooms
1
for Handling Aerospace Fluids
This standard is issued under the fixed designation F 318; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
1. Scope F 312 Test Methods for Microscopical Sizing and Counting
Particles from Aerospace Fluids on Membrane Filters
1.1 This practice covers a procedure for sampling airborne
particulate matter larger than 5 µm in size. The method is
3. Terminology
designed to be used in specific areas, commonly called
3.1 Definitions:
cleanrooms in the aerospace industry, where aerospace fluids
3.1.1 cleanroom—an area in which the temperature, humid-
are handled.
ity,andtheairborneparticulatecontaminationarecontrolledas
NOTE 1—Practice F 50 is an alternative procedure.
required.
3.1.2 uninterrupted airflow pattern—the pattern of airflow
1.2 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the that exists in a given area, when no personnel or equipment are
present to interrupt the airflow.
responsibility of the user of this standard to establish appro-
priate safety and health practices and determine the applica-
4. Summary of Practice
bility of regulatory limitations prior to use.
4.1 This practice is based on the impingement of particles
2. Referenced Documents
onafiltermembraneusingavacuumtechnique.Thenumberof
2
air samples required in a given area will be based upon the
2.1 ASTM Standards:
D 1193 Specification for Reagent Water geometric floor area, the disturbance to the uninterrupted
airflow pattern, and the room volume. See also Practice E 2042
D 1836 Specification for Commercial Hexanes
D 2021 Specification for Neutral Detergent, 40 Percent and Test Method F 25.
3
Alkylbenzene Sulfonate Type
5. Apparatus
E 2042 Practice for Cleaning and Maintaining Controlled
5.1 Filter Holder—Aerosol open-type for a filter mem-
Areas and Clean Rooms
brane.
F 25 Test Method for Sizing and Counting Airborne Par-
5.2 Vacuum Pump or Aspirator—Minimum capacity 25 in.
ticulate Contamination in Clean Rooms and Other Dust-
(635 mm) Hg at 10 standard L/min.
Controlled Areas Designed for Electronic and Similar
5.3 Flowmeter—Orifice-type, rotameter-type or equivalent
Applications
positive flow-indicating device, capable of being calibrated to
F 50 Practice for Continuous Sizing and Counting of Air-
a 65 % flow accuracy under sample area ambient conditions.
borne Particles in Dust-ControlledAreas and Clean Rooms
Calibration must be at a given vacuum using a given diameter
Using Instruments Capable of Detecting Single Sub-
and length of line from the vacuum source to the filter holder
Micrometre and Larger Particles
containing a filter membrane of the same pore size as used in
the test sample.
1
This practice is under the jurisdiction of ASTM Committee E21 on Space
5.4 Membrane Filter—A nominal overall diameter with
Simulation andApplications of Space Technology and is the direct responsibility of
grid lines, in dimensional accord with the filter holder, may be
Subcommittee E21.05 on Contamination.
used. The pore size should be selected with regard to pertinent
Current edition approved Sept. 1, 2004. Published September 2004. Originally
approved in 1965. Last previous edition approved in 2000 as F 318 – 78 (2000).
particle ranges and a specified flow rate across an effective
2
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
sampling area of 1000 mm 6 5 %. Color contrast is recom-
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
mended to aid in identification of particulate matter.
Standards volume information, refer to the standard’s Document Summary page on
the ASTM website. 5.5 Forceps—Stainless steel, nonmagnetic, unserrated tips.
3
Withdrawn.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
F318–04
5.6 Microscope and Associated Apparatus—For a descrip- 7.5 Special consideration of all permanent and temporary
tion of a suitable apparatus, refer to Test Methods F 312. sensitive work areas within the cleanroom, such as laminar
flow stations for critical assembly, will require air samples as
5.7 Wash Bottle, fitted with an in-line filtration capability.
needed.
6. Reagents and Materials
8. Preparation of Apparatus
6.1 Purity of Reagents—Reagent grade chemicals shall be
8.1 Prior to sampling, clean the filter holder and forceps by
used in all tests. Unless otherwise indicated, it is intend
...

Questions, Comments and Discussion

Ask us and Technical Secretary will try to provide an answer. You can facilitate discussion about the standard in here.

This May Also Interest You

ASTM
ASTM F50-21(Practice)
Standard Practice for Continuous Sizing and Counting of Airborne Particles in Dust-Controlled Areas and Clean Rooms Using Instruments Capable of Detecting Single Sub-Micrometre and Larger Particles

SIGNIFICANCE AND USE
5.1 The primary purpose of this practice is to describe a procedure for collecting near real-time data on airborne particle concentration and size distribution in clean areas as indicated by single particle counting techniques. Implementation of some government and industry specifications requires acquisition of particle size and concentration data using an SPC.  
5.2 The processing requirements of many products manufactured in a clean room involves environmental cleanliness levels so low that a single particle counter with capability for detecting very small particles is required to characterize clean room air. Real-time information on concentration of airborne particles in size ranges from less than 0.1 μm to 5 μm and greater can be obtained only with an SPC. Definition of particles larger than approximately 0.05 μm may be carried out with direct measurement of light scattering from individual particles; other techniques may be required for smaller particles, such as preliminary growth by condensation before particle measurement.  
5.3 Particle size data are referenced to the particle system used to calibrate the SPC. Differences in detection, electronic and sample handling systems among the various SPCs may contribute to differences in particle characterization. Care must be exercised in attempting to compare data from particles that vary significantly in composition or shape from the calibration base material. Variations may also occur between instruments using similar particle sensing systems with different operating parameters. These effects should be recognized and minimized by using standard methods for SPC calibration and operation.  
5.4 In applying this practice, the fundamental assumption is made that the particles in the sample passing through the SPC are representative of the particles in the entire dust-controlled area being analyzed. Care is required that good sampling procedures are used and that no artifacts are produced at any point in the samp...
SCOPE
1.1 This practice covers the determination of the particle concentration, by number, and the size distribution of airborne particles in dust-controlled areas and clean rooms, for particles in the size range of approximately 0.01 to 5.0 μm. Particle concentrations not exceeding 3.5 × 106 particles/m 3 (100 000/ft3) are covered for all particles equal to and larger than the minimum size measured.  
1.2 This practice uses an airborne single particle counting device (SPC) whose operation is based on measuring the signal produced by an individual particle passing through the sensing zone. The signal must be directly or indirectly related to particle size.  
Note 1: The SPC type is not specified here. The SPC can be a conventional optical particle counter (OPC), an aerodynamic particle sizer, a condensation nucleus counter (CNC) operating in conjunction with a diffusion battery or differential mobility analyzer, or any other device capable of counting and sizing single particles in the size range of concern and of sampling in a cleanroom environment.  
1.3 Individuals performing tests in accordance with this practice shall be trained in use of the SPC and shall understand its operation.  
1.4 Since the concentration and the particle size distribution of airborne particles are subject to continuous variations, the choice of sampling probe configuration, locations, and sampling times will affect sampling results. Further, the differences in the physical measurement, electronic, and sample handling systems between the various SPCs and the differences in physical properties of the various particles being measured can contribute to variations in the test results. These differences should be recognized and minimized by using a standard method of primary calibration and by minimizing variability of sample acquisition procedures.  
1.5 Sample acquisition procedures and equipment may be selected for specific applications based on ...

  • Standard
    6 pages
    English language
    sale 15% off
  • Standard
    6 pages
    English language
    sale 15% off
ASTM
ASTM F25/F25M-21(Test Method)
Standard Test Method for Sizing and Counting Airborne Particulate Contamination in Cleanrooms and Other Dust-Controlled Areas

ABSTRACT
This test method covers the apparatuses required, sampling methods, standard procedures and calculations, and test reports for counting and sizing airborne microparticulate matter, the sampling areas for which are specifically those with contamination levels typical of cleanrooms and dust-controlled areas. The test method is based on the microscopical examination of particles impinged upon a membrane filter with the aid of a vacuum. Sampling may be done in a cleanroom, clean zone, or other controlle areas, or in a duct or pipe, wherein the number of sampling points is proportional to the floor area of the enclosure to be checked. The apparatus and facilities required are typical of a laboratory for the study of macroparticle contamination. The operator must have adequate basic training in microscopy and the techniques of particle sizing and counting.
SCOPE
1.1 This test method covers counting and sizing airborne particulate matter 5 µm and larger (macroparticles). The sampling areas are specifically those with contamination levels typical of cleanrooms and dust-controlled areas.  
1.2 Units—The values stated in either SI units or inch-pound units are to be regarded separately as standard. The values stated in each system are not necessarily exact equivalents; therefore, to ensure conformance with the standard, each system shall be used independently of the other, and values from the two systems shall not be combined.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    8 pages
    English language
    sale 15% off
  • Standard
    8 pages
    English language
    sale 15% off
ASTM
ASTM F91-06(2019)(Practice)
Standard Practice for Testing for Leaks in the Filters Associated With Laminar Flow Clean Rooms and Clean Work Stations by Use of a Condensation Nuclei Detector

ABSTRACT
This practice covers the testing of the integrity of high-efficiency particulate air (HEPA) filters installed in laminar flow clean rooms of the ceiling to floor or wall to wall type, and laminar flow clean work stations using condensation nuclei detector. The recommended practice may be used to detect faults or voids in the filter media itself or in the joints between the filter and the room or work station structure. The preparation for testing and the procedure for the proper testing are presented in details.
SCOPE
1.1 This practice covers the testing of the integrity of high-efficiency particulate air (HEPA) filters installed in laminar flow clean rooms of the ceiling to floor or wall to wall type, and laminar flow clean work stations. The recommended practice may be used to detect faults or voids in the filter media itself or in the joints between the filter and the room or work station structure. The determination of filter media efficiency is not within the scope of this practice.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.2.1 Exception—The values given in parentheses in inch-pound units are for information only.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    2 pages
    English language
    sale 15% off
ASTM
ASTM E2889-23(Practice)
Standard Practice for Control of Respiratory Hazards in the Metal Removal Fluid Environment

SIGNIFICANCE AND USE
4.1 Exposure to aerosols in the industrial metal removal environment has been associated with adverse respiratory effects.  
4.2 Use of this practice will mitigate occupational exposure and effects of exposure to aerosols in the metal removal environment.  
4.3 Through implementation of this practice, users should be able to reduce instances and severity of respiratory irritation and disease through the effective use of a metal removal fluid management program, appropriate product selection, appropriate machine tool design, proper air handling mechanisms, and control of microorganisms.
SCOPE
1.1 This practice sets forth guidelines to control respiratory hazards in the metal removal environment.  
1.2 This practice does not include prevention of dermatitis, which is the subject of Practice E2693, but it does adopt a similar systems management approach with many control elements in common.  
1.3 This practice focuses on employee exposure via inhalation of metal removal fluids and associated airborne agents.  
1.4 Metal removal fluids used for wet machining operations (such as cutting, drilling, milling, or grinding) that remove metal to produce the finished part are a subset of metalworking fluids. This practice does not apply to other operations (such as stamping, rolling, forging, or casting) that use metalworking fluids other than metal removal fluids. These other types of metalworking fluid operations are not included in this document because of limited information on health effects, including epidemiology studies, and on control technologies. Nonetheless, some of the exposure control approaches and guidance contained in this document may be useful for managing respiratory hazards associated with other types of metalworking fluids.  
1.5 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.6 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    11 pages
    English language
    sale 15% off
  • Standard
    11 pages
    English language
    sale 15% off
ASTM
ASTM D4185-23(Test Method)
Standard Test Method for Measurement of Metals in Workplace Atmospheres by Flame Atomic Absorption Spectrophotometry

SIGNIFICANCE AND USE
5.1 The health of workers in many industries is at risk through exposure by inhalation to toxic metals. Industrial hygienists and other public health professionals need to determine the effectiveness of measures taken to control workers' exposures, and this is generally achieved by making workplace air measurements. Exposure to some metal-containing particles has been demonstrated to cause dermatitis, skin ulcers, eye problems, chemical pneumonitis, and other physical disorders (16).3  
5.2 FAAS is capable of quantitatively determining many metals in air samples at the levels required by federal, state, and local occupational health and air pollution regulations. The analysis results can be used for the assessment of workplace exposures to metals in workplace air. The suitability of FAAS for elemental analysis for exposure assessment purposes must be investigated prior to carrying out workplace air sampling, in consideration of relevant occupational exposure limit values (OELVs) for metals of concern.
SCOPE
1.1 This test method covers the collection, dissolution, and determination of trace metals in workplace atmospheres, by flame atomic absorption spectrophotometry (FAAS).  
1.2 The estimated method detection limits and optimum working concentration ranges for 21 metals are given in Table 1.  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  (Specific safety precautionary statements are given in Section 9.)  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    8 pages
    English language
    sale 15% off
  • Standard
    8 pages
    English language
    sale 15% off
ASTM
ASTM D4856-23(Test Method)
Standard Test Method for Determination of Sulfuric Acid Mist in Workplace Atmospheres Collected on Mixed Cellulose Ester Filters (Ion Chromatographic Analysis)

SIGNIFICANCE AND USE
5.1 Sulfuric acid is used in the manufacture of fertilizer, explosives, dyestuffs, other acids, parchment paper, glue, lead acid batteries, textiles, etc., and in the pickling of metals.  
5.2 This test method has been found to be satisfactory in the measurement of sulfuric acid for comparison with relevant occupational exposure limits.
Note 2: In some countries the occupational exposure limit value (OELV) for sulfuric acid is related to the thoracic aerosol fraction; in such cases it is recommended to use a sampler for the thoracic aerosol fraction (ISO 20581).6
SCOPE
1.1 This ion chromatographic test method describes the determination of sulfuric acid mist in air samples collected from workplace atmospheres on a mixed cellulose ester (MCE) filter.
Note 1: Other filter types such as quartz fiber, polytetrafluoroethylene (PTFE), and polyvinyl chloride (PVC) filters are also suitable.  
1.2 The lower detection limit of this test method is 0.001 mg/sample or 0.017 mg/m3 of sulfuric acid (H2SO4) mist in 60 L of air sampled at 1 L/min.  
1.3 This test method is subject to interference from soluble and partially soluble sulfate salts. Other sulfur-containing compounds can be oxidized to sulfate and also interfere.  
1.4 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.5 No detailed instrument operating instructions are provided because of differences among various makes and models of ion chromatography (IC) systems. Instead, the analyst shall follow the instructions provided by the manufacturer of the particular instrument, analytical column, and suppressors used.  
1.6 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For specific precautionary statements, see Section 9.  
1.7 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    4 pages
    English language
    sale 15% off
  • Standard
    4 pages
    English language
    sale 15% off
ASTM
ASTM D5156-22(Test Method)
Standard Test Methods for Continuous Measurement of Ozone in Ambient, Workplace, and Indoor Atmospheres (Ultraviolet Absorption)

SIGNIFICANCE AND USE
5.1 Standards for O3  in the atmosphere have been promulgated by government authorities to protect the health and welfare of the public (6) and also for the protection of industrial workers (7).  
5.2 Although O3  itself is a toxic material, in ambient air it is primarily the photochemical oxidants formed along with O3  in polluted air exposed to sunlight that cause smog symptoms such as lachrymation and burning eyes. Ozone is much more easily monitored than these photochemical oxidants and provides a good indication of their concentrations, and it is therefore the substance that is specified in air quality standards and regulations.
SCOPE
1.1 This test method describes the sampling and continuous analysis of ozone (O3) in the atmosphere at concentrations ranging from 10 to 2000 μg/m3 of O3  in air (5 ppb(v) to 1 ppm(v)).  
1.1.1 The test method is limited to applications by its sensitivity to interferences as described in Section 6. The interference sensitivities may limit its use for ambient and workplace atmospheres.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.3 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.4 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    7 pages
    English language
    sale 15% off
  • Standard
    7 pages
    English language
    sale 15% off
ASTM
ASTM D7202-22(Test Method)
Standard Test Method for Determination of Beryllium in the Workplace by Extraction and Optical Fluorescence Detection

SIGNIFICANCE AND USE
5.1 Exposure to beryllium can cause a potentially fatal disease, and occupational exposure limits for beryllium in air and on surfaces have been established to reduce exposure risks to potentially affected workers (4-7). Sampling and analytical methods for beryllium are needed in order to meet the challenges relating to exposure assessment and risk reduction. Sampling and analysis methods, such as the procedure described in this test method, are desired in order to facilitate on-site and fixed-site laboratory measurement of trace beryllium. Beryllium analysis results can then be used as a basis for exposure assessment and protection of human health.
SCOPE
1.1 This test method is intended for use in the determination of beryllium by sampling workplace air and surface dust.  
1.2 This test method assumes that air and surface samples are collected using appropriate and applicable ASTM International standard practices for sampling of workplace air and surface dust. These samples are typically collected using air filter sampling, vacuum sampling or wiping techniques. See Guide E1370 for guidance on air sampling strategies, and Guide D7659 for guidance on selection of surface sampling techniques.  
1.3 Determination of beryllium in soil is not within the scope of this test method. See Test Method D7458 for determination of beryllium in soil samples.  
1.4 This test method includes a procedure for extraction (dissolution) of beryllium in weakly acidic medium (pH of 1 % aqueous ammonium bifluoride is 4.8), followed by field analysis of aliquots of the extract solution using a beryllium-specific-optically fluorescent dye.  
1.5 The procedure is suitable for on-site use in the field for occupational and environmental hygiene monitoring purposes. The method is also applicable for use in fixed-site laboratories.  
1.6 No detailed operating instructions are provided because of differences among various makes and models of suitable fluorometric instruments. Instead, the analyst shall follow the instructions provided by the manufacturer of the particular instrument. This test method does not address comparative accuracy of different devices or the precision between instruments of the same make and model.  
1.7 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.8 This test method contains notes that are explanatory and not part of mandatory requirements of the standard.  
1.9 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.10 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    9 pages
    English language
    sale 15% off
  • Standard
    9 pages
    English language
    sale 15% off
ASTM
ASTM D6494-22(Test Method)
Standard Test Method for Determination of Asphalt Fume Particulate Matter in Workplace Atmospheres as Benzene Soluble Fraction

SIGNIFICANCE AND USE
5.1 Asphalt is a material used in the construction of roads and as a roofing material and sealant.  
5.2 This test method provides a means of evaluating exposure to asphalt fume in the working environment at the presently recommended exposure guidelines (for example, Threshold Limit Values and Biological Exposure Indices, ACGIH).7  
5.3 This procedure has been adapted from NIOSH Method 5023 (withdrawn prior to 4th edition (1994) and replaced in 1998 with NIOSH Method 5042) and OSHA Method 58 to reduce the level of background contamination providing better reproducibility.
SCOPE
1.1 This test method covers the determination of asphalt fume particulate matter (as benzene soluble fraction) and total particulate matter weight in workplace atmospheres using a polytetrafluoroethylene (PTFE) filter methodology.  
1.2 This procedure has been adapted from NIOSH Method 5023 (withdrawn prior to 4th edition (1994) and replaced in 1998 with NIOSH Method 5042) and OSHA Method 58. This adaptation was made to reduce the level of background contamination providing better reproducibility.  
1.3 This procedure is compatible with high flow rate personal sampling equipment–0.5 to 2.0 L/min. It can be used for personal or area monitoring.  
1.4 The sampling method develops a time-weighted average (TWA) sample and can be used to determine short-term exposure limit (STEL).  
1.5 The applicable concentration range for the TWA sample is from 0.2 to 2.0 mg/m3.
Note 1: A study has suggested candidate solvents for benzene replacement.2 A less toxic solvent for this analysis would be more appropriate, although the substitution with a solvent other than benzene needs further validations with field data.  
1.6 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.7 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use. For more specific precautionary statements, see Section 9.  
1.8 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    5 pages
    English language
    sale 15% off
  • Standard
    5 pages
    English language
    sale 15% off
ASTM
ASTM D4600-22(Test Method)
Standard Test Method for Determination of Benzene-Soluble Particulate Matter in Workplace Atmospheres

SIGNIFICANCE AND USE
5.1 This test method provides a means of evaluating exposures to benzene-soluble particulate matter in a concentration range that can be related to occupational exposures.
SCOPE
1.1 This test method describes the sampling and gravimetric determination of benzene-soluble particulate matter that has become airborne as a result of certain industrial processes. This test method can be used to determine the total weight of benzene-soluble materials and to provide a sample that may be used for specific and detailed analyses of the soluble components.  
1.2 The limit of detection is 0.05 mg/m3 by sampling a 1 m3 volume of air.
Note 1: Other volatile organic solvents have been used for this determination and whereas a less toxic solvent for this analysis might be desirable, the substitution of a solvent other than benzene is unwise at this time. A tremendous volume of environmental sampling data based on benzene-soluble determinations has been accumulated over many years in several industries.2 Some of the determinations have been used in epidemiological studies. Furthermore, the use of benzene is specified in existing United States federal standards.3 As a result, it appears imprudent to use a different solvent until the qualitative and quantitative relationship of analyses derived from benzene and a substitute solvent is established. With proper care, benzene can be safely used in the laboratory.  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety, health, and environmental practices and determine the applicability of regulatory limitations prior to use.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

  • Standard
    4 pages
    English language
    sale 15% off
  • Standard
    4 pages
    English language
    sale 15% off