ASTM D5854-96(2015)
(Practice)Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
Standard Practice for Mixing and Handling of Liquid Samples of Petroleum and Petroleum Products
SIGNIFICANCE AND USE
4.1 Representative samples of petroleum and petroleum products are required for the determination of chemical and physical properties used to establish standard volumes, prices, and compliance with commercial and regulatory specifications. The treatment of samples from the time of collection until they are analyzed requires care and effort to maintain their compositional integrity.
SCOPE
1.1 This practice covers the handling, mixing, and conditioning procedures that are required to ensure that a representative sample of the liquid petroleum or petroleum product is delivered from the primary sample container/receiver into the analytical test apparatus or into intermediate containers.
1.2 Annex A2 covers acceptance test criteria for power mixer and sample container combinations, while Annex A3 and Annex A4 detail acceptance tests for mixing systems. Appendix X1 is a guide for selecting sample containers.
1.3 For sampling procedures, refer to Practices D4057 (API MPMS Chapter 8.1) and D4177 (API MPMS Chapter 8.2). Practice D5842 (API MPMS Chapter 8.4) covers sampling and handling of light fuels for volatility measurement.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
General Information
Buy Standard
Standards Content (Sample)
NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: D5854 − 96 (Reapproved 2015)
Manual of Petroleum Measurement Standards (MPMS), Chapter 8.3
Standard Practice for
Mixing and Handling of Liquid Samples of Petroleum and
1
Petroleum Products
This standard is issued under the fixed designation D5854; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision.Anumber in parentheses indicates the year of last reapproval.A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope D4928Test Method forWater in Crude Oils by Coulometric
Karl Fischer Titration
1.1 This practice covers the handling, mixing, and condi-
D5842Practice for Sampling and Handling of Fuels for
tioning procedures that are required to ensure that a represen-
Volatility Measurement
tative sample of the liquid petroleum or petroleum product is
3
2.2 API Documents:
delivered from the primary sample container/receiver into the
analytical test apparatus or into intermediate containers. MPMS Chapter 8.1Practice for Manual Sampling of Petro-
leum and Petroleum Products (ASTM Practice D4057)
1.2 Annex A2 covers acceptance test criteria for power
MPMSChapter 8.2Practice for Automatic Sampling of Pe-
mixer and sample container combinations, while Annex A3
troleum and Petroleum Products (ASTM Practice D4177)
and Annex A4 detail acceptance tests for mixing systems.
MPMS Chapter 8.4Practice for Sampling and Handling of
Appendix X1 is a guide for selecting sample containers.
FuelsforVolatilityMeasurement(ASTMPracticeD5842)
1.3 For sampling procedures, refer to Practices D4057 (API
MPMSChapter10.9TestMethodforWaterinCrudeOilsby
MPMS Chapter 8.1) and D4177 (API MPMS Chapter 8.2).
Coulometric Karl Fischer Titration (ASTM Test Methods
PracticeD5842(API MPMSChapter8.4)coverssamplingand
D4928)
handling of light fuels for volatility measurement.
Recommended Practice 2003,Protection Against Ignitions
Arising Out of Static, Lighting, and Stray Currents
1.4 This standard does not purport to address all of the
safety concerns, if any, associated with its use. It is the Publication 2026,Safe Access/Egress Involving Floating
Roofs of Storage Tanks in Petroleum Service
responsibility of the user of this standard to establish appro-
priate safety and health practices and determine the applica- Publication 2217,Guideline for Confined SpaceWork in the
bility of regulatory limitations prior to use. Petroleum Industry
4
2.3 Department of Transportation:
2. Referenced Documents
Code of Federal Regulations, Title 49,Section 173
2
2.1 ASTM Standards: 4
2.4 Occupational Safety and Health Standards:
D4057Practice for Manual Sampling of Petroleum and
29 Code of Federal Regulations, Subpart Z, “Toxic and
Petroleum Products
Hazardous Substances,” Part 1910.1000 and following
D4177Practice for Automatic Sampling of Petroleum and
Petroleum Products
3. Terminology
D4306Practice for Aviation Fuel Sample Containers for
3.1 Definitions of Terms Specific to This Standard:
Tests Affected by Trace Contamination
3.1.1 intermediate container—the vessel into which all or
part of the sample from a primary container/receiver is
1 transferred for transport, storage, or ease of handling.
This practice is under the jurisdiction ofASTM Committee D02 on Petroleum
Products, Liquid Fuels, and Lubricants and the API Committee on Petroleum
3.1.2 petroleum—denotes petroleum crudes, as well as pe-
Measurement, and is the direct responsibility of Subcommittee D02.02 the joint
troleum products, normally associated with the petroleum
ASTM-API committee on Hydrocarbon Measurement for Custody Transfer (Joint
industry.
ASTM-API).
Current edition approved April 1, 2015. Published June 2015. Originally
approved in 1996. Last previous edition approved in 2010 as D5854–96 (2010).
DOI: 10.1520/D5854-96R15.
2 3
For referenced ASTM standards, visit the ASTM website, www.astm.org, or Available from American Petroleum Institute (API), 1220 L. St., NW,
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Washington, DC 20005-4070, http://www.api.org.
4
Standards volume information, refer to the standard’s Document Summary page on Available from the Superintendent of Documents, U.S. Government Printing
the ASTM website. Office, Washington, DC 20402.
© Jointly copyrighted by ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, USA and the American Petroleum Institute (API), 1220 L Street NW, Washington DC 20005, USA
1
---------------------- Page: 1 ----------------------
D5854 − 96 (2015)
3.1.3 primary container/receiver—the vessel in which a 6.2.9 Containers used with closed loop mixers may be
sample is initially collected. equipped with a discharge line inside the container which has
3.1.3.1 Discussion—Examples of pr
...
This document is not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation: D5854 − 96 (Reapproved 2010) D5854 − 96 (Reapproved 2015)
Manual of Petroleum Measurement Standards (MPMS), Chapter 8.3
Standard Practice for
Mixing and Handling of Liquid Samples of Petroleum and
1
Petroleum Products
This standard is issued under the fixed designation D5854; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This practice covers the handling, mixing, and conditioning procedures that are required to ensure that a representative
sample of the liquid petroleum or petroleum product is delivered from the primary sample container/receiver into the analytical
test apparatus or into intermediate containers.
1.2 Annex A2 covers acceptance test criteria for power mixer and sample container combinations, while Annex A3 and Annex
A4 detail acceptance tests for mixing systems. Appendix X1 is a guide for selecting sample containers.
1.3 For sampling procedures, refer to Practices D4057 (API MPMS Chapter 8.1) and D4177 (API MPMS Chapter 8.2). Practice
D5842 (API MPMS Chapter 8.4) covers sampling and handling of light fuels for volatility measurement.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use.
2. Referenced Documents
2
2.1 ASTM Standards:
D4057 Practice for Manual Sampling of Petroleum and Petroleum Products
D4177 Practice for Automatic Sampling of Petroleum and Petroleum Products
D4306 Practice for Aviation Fuel Sample Containers for Tests Affected by Trace Contamination
D4928 Test Method for Water in Crude Oils by Coulometric Karl Fischer Titration
D5842 Practice for Sampling and Handling of Fuels for Volatility Measurement
3
2.2 API Documents:
MPMS Chapter 8.1 Practice for Manual Sampling of Petroleum and Petroleum Products (ASTM Practice D4057)
MPMS Chapter 8.2 Practice for Automatic Sampling of Petroleum and Petroleum Products (ASTM Practice D4177)
MPMS Chapter 8.4 Practice for Sampling and Handling of Fuels for Volatility Measurement (ASTM Practice D5842)
MPMS Chapter 10.9 Test Method for Water in Crude Oils by Coulometric Karl Fischer Titration (ASTM Test Methods D4928)
Recommended Practice 2003, Protection Against Ignitions Arising Out of Static, Lighting, and Stray Currents
Publication 2026, Safe Access/Egress Involving Floating Roofs of Storage Tanks in Petroleum Service
Publication 2217, Guideline for Confined Space Work in the Petroleum Industry
4
2.3 Department of Transportation:
Code of Federal Regulations, Title 49, Section 173
4
2.4 Occupational Safety and Health Standards:
29 Code of Federal Regulations, Subpart Z, “Toxic and Hazardous Substances,” Part 1910.1000 and following
1
This practice is under the jurisdiction of ASTM Committee D02 on Petroleum Products, Liquid Fuels, and Lubricants and the API Committee on Petroleum Measurement,
and is the direct responsibility of Subcommittee D02.02.08 the joint ASTM-API committee on Sampling (API MPMS Chapter 8.0).
Current edition approved May 1, 2010April 1, 2015. Published May 2010 June 2015. Originally approved in 1996. Last previous edition approved in 20052010 as
D5854–96(2005).D5854 – 96 (2010). DOI: 10.1520/D5854-96R10.10.1520/D5854-96R15.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
3
Available from American Petroleum Institute (API), 1220 L. St., NW, Washington, DC 20005-4070, http://www.api.org.
4
Available from the Superintendent of Documents, U.S. Government Printing Office, Washington, DC 20402.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1
---------------------- Page: 1 ----------------------
D5854 − 96 (2015)
3. Terminology
3.1 Definitions of Terms Specific to This Standard:
3.1.1 intermediate container—the vessel into which all or part of the sample from a primary container/receiver is transferred
for transport, storage, or ease of handling.
3.1.2 petroleum—denotes petroleum crudes, as well as petroleum products, nor
...
Questions, Comments and Discussion
Ask us and Technical Secretary will try to provide an answer. You can facilitate discussion about the standard in here.