Standard Guide for Sampling Plan and Core Sampling for Prebaked Anodes Used in Aluminum Production

SIGNIFICANCE AND USE
Core sampling is an acceptable way of obtaining a test specimen without destroying the usefulness of an anode block.
4.1.1 Test specimen obtained by this guide can be used by producers and users of carbon anodes for the purpose of conducting the tests in Note 1 to obtain comparative physical properties.
Sampling shall not weaken the anode or increase the likelihood of premature failure.
SCOPE
1.1 This guide covers sampling for prebaked carbon anodes used in the production of aluminum, and details procedures for taking test samples from anode blocks. It covers equipment and procedures for obtaining samples from anode blocks in a manner that does not destroy the block or prevent its subsequent use as originally intended. However, the user must determine the subsequent use of the sampled anode blocks. Preferred locations for taking samples from single units of anodes are covered in this guide.
1.1.1 Information for sampling of shaped refractory products, in general, is given in ISO 5022. This standard details the statistical basis for sampling plans for acceptance testing of a consignment or lot. Anodes used in the production of aluminum have specific requirements for sampling and while the statistical basis for sampling given in ISO 5022 applies, further or modified requirements may also apply.
1.2 The values stated in SI units are to be regarded as the standard. The values given in parentheses are for information only.
This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.Note 1
The following ASTM standards are noted as sources of useful information: Test Methods C 559, C 611, C 651, C 747, C 1025, C 1039, and E 1225.

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Designation:D6353–06
Standard Guide for
Sampling Plan and Core Sampling for Prebaked Anodes
1
Used in Aluminum Production
This standard is issued under the fixed designation D6353; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope* C559 Test Method for Bulk Density by Physical Measure-
ments of Manufactured Carbon and Graphite Articles
1.1 This guide covers sampling for prebaked carbon anodes
C611 Test Method for Electrical Resistivity of Manufac-
used in the production of aluminum, and details procedures for
tured Carbon and Graphite Articles at Room Temperature
takingtestsamplesfromanodeblocks.Itcoversequipmentand
C651 Test Method for Flexural Strength of Manufactured
procedures for obtaining samples from anode blocks in a
Carbon and GraphiteArticles Using Four-Point Loading at
manner that does not destroy the block or prevent its subse-
Room Temperature
quent use as originally intended. However, the user must
C747 Test Method for Moduli of Elasticity and Fundamen-
determine the subsequent use of the sampled anode blocks.
tal Frequencies of Carbon and Graphite Materials by Sonic
Preferred locations for taking samples from single units of
Resonance
anodes are covered in this guide.
C1025 Test Method for Modulus of Rupture in Bending of
1.1.1 Information for sampling of shaped refractory prod-
Electrode Graphite
ucts, in general, is given in ISO 5022. This standard details the
C1039 Test Methods for Apparent Porosity, Apparent Spe-
statistical basis for sampling plans for acceptance testing of a
cific Gravity, and Bulk Density of Graphite Electrodes
consignment or lot. Anodes used in the production of alumi-
E1225 Test Method for Thermal Conductivity of Solids by
num have specific requirements for sampling and while the
Means of the Guarded-Comparative-Longitudinal Heat
statistical basis for sampling given in ISO 5022 applies, further
Flow Technique
or modified requirements may also apply.
3
2.2 ISO Standards:
1.2 The values stated in SI units are to be regarded as
ISO 5022 Shapedrefractoryproducts-Samplingandaccep-
standard. No other units of measurement are included in this
tance testing
standard.
1.3 This standard does not purport to address all of the
3. Terminology
safety concerns, if any, associated with its use. It is the
3.1 Definitions of Terms Specific to This Standard:
responsibility of the user of this standard to establish appro-
3.1.1 block—a carbon anode, a single unit.
priate safety and health practices and determine the applica-
3.1.2 prebaked—a baked carbon article or block.
bility of regulatory limitations prior to use.
3.1.3 sample—the portion of carbon obtained from an
NOTE 1—The followingASTM standards are noted as sources of useful
anode.
information: Test Methods C559, C611, C651, C747, C1025, C1039, and
3.1.4 test specimen—an article prepared from a sample.
E1225.
4. Significance and Use
2. Referenced Documents
4.1 Core sampling is an acceptable way of obtaining a test
2
2.1 ASTM Standards:
specimen without destroying the usefulness of an anode block.
4.1.1 Test specimen obtained by this guide can be used by
1
producers and users of carbon anodes for the purpose of
This guide is under the jurisdiction of ASTM Committee D02 on Petroleum
Products and Lubricants and is the direct responsibility of Subcommittee D02.05 on
conducting the tests in Note 1 to obtain comparative physical
Properties of Fuels, Petroleum Coke and Carbon Material.
properties.
Current edition approved July 1, 2006. Published July 2006. Originally approved
4.2 Sampling shall not weaken the anode or increase the
in 1998. Last previous edition approved in 2003 as D6353–98(2003). DOI:
10.1520/D6353-06. likelihood of premature failure.
2
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
3
Standards volume information, refer to the standard’s Document Summary page on Available from American National Standards Institute (ANSI), 25 W. 43rd St.,
the ASTM website. 4th Floor, New York, NY 10036.
*A Summary of Changes section appears at the end of this standard.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

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D6353–06
5. Apparatus minimum dimension (usually the diameter) should be at least
three times the maximum particle size of the dry aggregate
5.1 Core Drill Bit, similar to that shown in Fig. 1, driven by
used in the manufacture of the anode block. The dimensions of
suitable equipment. Use
...

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