ASTM D5395-03
(Specification)Standard Specification for Reclaimed Methylene Chloride
Standard Specification for Reclaimed Methylene Chloride
SCOPE
1.1 This specification covers the grade of methylene chloride typically needed in various industries for noncritical applications, such as in paint stripping formulations. It may be used as a reference document by purchasers or by persons establishing in-house methylene chloride recovery programs.
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
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Designation: D 5395 – 03
Standard Specification for
,
1 2
Reclaimed Methylene Chloride
This standard is issued under the fixed designation D 5395; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (e) indicates an editorial change since the last revision or reapproval.
TABLE 1 Physical Properties
1. Scope
Property Specification Test Method
1.1 This specification covers the grade of methylene chlo-
Specific gravity, 25/25 1.318 to 1.323 D 2111
ride typically needed in various industries for noncritical
Acidity, as HCl, ppm, max 1.0 D 2989
applications, such as in paint stripping formulations. It may be
Water, ppm, max 500 D 3401or E 1064
used as a reference document by purchasers or by persons
Appearance Clear and free from D 3741
suspended matter
establishing in-house methylene chloride recovery programs.
Color, Pt-Co, max 50 D 2108
Nonvolatile residue, ppm, max 50 D 2109
2. Referenced Documents
Chloride, ppm, max 1.0 D 2988
Assay, weight % 95.0 D 6806
2.1 ASTM Standards:
1,1,1-Trichloroethane content, 0.5 D 6806
D 2108 Test Method for Color of Halogenated Organic
weight %, max
3
Solvents and Their Admixtures (Platinum-Cobalt Scale)
D 2109 Test Methods for Nonvolatile Matter in Haloge-
3
4
nated Organic Solvents and Their Admixtures
2.2 U.S. Governmnet Documents:
D 2111 Test Methods for Specific Gravity of Halogenated
49 CFR 100 to 199 Department of Transportation Hazard-
3
Organic Solvents and Their Admixtures
ous Materials Regulations
D 2988 Test Method for Water-Soluble Halide Ion in Halo-
29 CFR 1919.1200 Department of Labor, OSHA Regula-
3
genated Organic Solvents and Their Admixtures
tions on Hazard Communications
D 2989 Test Method for Acidity-Alkalinity of Halogenated
3
3. Properties
Organic Solvents and Their Admixtures
D 3401 Test Methods for Water in Halogenated Organic
3.1 Reclaimed methylene chloride shall meet the require-
3
Solvents and Their Admixtures
ments of Table 1.
D 3741 Test Method for Appearance of Admixtures Con-
3
4. Packaging and Package Marking
taining Halogenated Organic Solvents
D 6806 Practice for Analysis of Halogenated Organic Sol-
4.1 Package and label industrial or commercial quantities in
3
vents and Their Ad
...
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