Standard Test Method for Creep and Creep Rupture of Continuous Fiber-Reinforced Advanced Ceramics Under Tensile Loading at Elevated Temperatures

SIGNIFICANCE AND USE
This test method may be used for material development, material comparison, quality assurance, characterization, and design data generation.  
Continuous fiber-reinforced ceramic matrix composites are candidate materials for structural applications requiring high degrees of wear and corrosion resistance and toughness at high temperatures.  
Creep tests measure the time-dependent deformation of a material under constant load at a given temperature. Creep rupture tests provide a measure of the life of the material when subjected to constant mechanical loading at elevated temperatures. In selecting materials and designing parts for service at elevated temperatures, the type of test data used will depend on the criteria for load-carrying capability which best defines the service usefulness of the material.  
Creep and creep rupture tests provide information on the time-dependent deformation and on the time-of-failure of materials subjected to uniaxial tensile stresses at elevated temperatures. Uniform stress states are required to effectively evaluate any nonlinear stress-strain behavior which may develop as the result of cumulative damage processes (for example, matrix cracking, matrix/fiber debonding, fiber fracture, delamination, etc.) which may be influenced by testing mode, testing rate, processing or alloying effects, environmental influences, or elevated temperatures. Some of these effects may be consequences of stress corrosion or subcritical (slow) crack growth. It is noted that ceramic materials typically creep more rapidly in tension than in compression. Therefore, creep data for design and life prediction should be obtained in both tension and compression.  
The results of tensile creep and tensile creep rupture tests of specimens fabricated to standardized dimensions from a particular material or selected portions of a part, or both, may not totally represent the creep deformation and creep rupture properties of the entire, full-size end product or its ...
SCOPE
1.1 This test method covers the determination of the time-dependent deformation and time-to-rupture of continuous fiber-reinforced ceramic composites under constant tensile loading at elevated temperatures. This test method addresses, but is not restricted to, various suggested test specimen geometries. In addition, test specimen fabrication methods, allowable bending, temperature measurements, temperature control, data collection, and reporting procedures are addressed.  
1.2 This test method is intended primarily for use with all advanced ceramic matrix composites with continuous fiber reinforcement: unidirectional (1-D), bidirectional (2-D), and tridirectional (3-D). In addition, this test method may also be used with glass matrix composites with 1-D, 2-D, and 3-D continuous fiber reinforcement. This test method does not address directly discontinuous fiber-reinforced, whisker-reinforced, or particulate-reinforced ceramics, although the test methods detailed here may be equally applicable to these composites.  
1.3 Values expressed in this test method are in accordance with the International System of Units (SI) and .
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Hazard statements are noted in 7.1 and 7.2.

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ASTM C1337-10 - Standard Test Method for Creep and Creep Rupture of Continuous Fiber-Reinforced Advanced Ceramics Under Tensile Loading at Elevated Temperatures
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Standards Content (Sample)

NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation: C1337 − 10
StandardTest Method for
Creep and Creep Rupture of Continuous Fiber-Reinforced
Advanced Ceramics Under Tensile Loading at Elevated
1
Temperatures
This standard is issued under the fixed designation C1337; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope 2. Referenced Documents
2
1.1 This test method covers the determination of the time- 2.1 ASTM Standards:
dependent deformation and time-to-rupture of continuous C1145 Terminology of Advanced Ceramics
fiber-reinforced ceramic composites under constant tensile C1275 Test Method for Monotonic Tensile Behavior of
loading at elevated temperatures. This test method addresses, Continuous Fiber-Reinforced Advanced Ceramics with
but is not restricted to, various suggested test specimen Solid Rectangular Cross-Section Test Specimens at Am-
geometries. In addition, test specimen fabrication methods, bient Temperature
allowable bending, temperature measurements, temperature D3878 Terminology for Composite Materials
control, data collection, and reporting procedures are ad- E4 Practices for Force Verification of Testing Machines
dressed. E6 Terminology Relating to Methods of Mechanical Testing
E83 Practice for Verification and Classification of Exten-
1.2 This test method is intended primarily for use with all
someter Systems
advanced ceramic matrix composites with continuous fiber
E139 Test Methods for Conducting Creep, Creep-Rupture,
reinforcement: unidirectional (1-D), bidirectional (2-D), and
and Stress-Rupture Tests of Metallic Materials
tridirectional (3-D). In addition, this test method may also be
E220 Test Method for Calibration of Thermocouples By
used with glass matrix composites with 1-D, 2-D, and 3-D
Comparison Techniques
continuous fiber reinforcement. This test method does not
E230 Specification and Temperature-Electromotive Force
address directly discontinuous fiber-reinforced, whisker-
(EMF) Tables for Standardized Thermocouples
reinforced,orparticulate-reinforcedceramics,althoughthetest
E337 Test Method for Measuring Humidity with a Psy-
methods detailed here may be equally applicable to these
chrometer (the Measurement of Wet- and Dry-Bulb Tem-
composites.
peratures)
1.3 Values expressed in this test method are in accordance
E1012 Practice for Verification of Testing Frame and Speci-
withtheInternationalSystemofUnits(SI)andIEEE/ASTMSI
men Alignment Under Tensile and Compressive Axial
10 .
Force Application
1.4 This standard does not purport to address all of the IEEE/ASTM SI 10 American National Standard for Use of
safety concerns, if any, associated with its use. It is the
theInternationalSystemofUnits(SI):TheModernMetric
responsibility of the user of this standard to establish appro- System
priate safety and health practices and determine the applica-
3. Terminology
bility of regulatory limitations prior to use. Hazard statements
3.1 Definitions:
are noted in 7.1 and 7.2.
3.1.1 The definitions of terms relating to tensile testing
appearing in Terminology E6 apply to the terms used in this
test method. The definitions relating to advanced ceramics
1
This test method is under the jurisdiction of ASTM Committee C28 on
Advanced Ceramics and is the direct responsibility of Subcommittee C28.07 on
2
Ceramic Matrix Composites. For referenced ASTM standards, visit the ASTM website, www.astm.org, or
Current edition approved Dec. 1, 2010. Published January 2011. Originally contact ASTM Customer Service at service@astm.org. For Annual Book of ASTM
approved in 1996. Last previous edition approved in 2005 as C1337 – 96 (2005). Standards volume information, refer to the standard’s Document Summary page on
DOI: 10.1520/C1337-10. the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959. United States
1

---------------------- Page: 1 ----------------------
C1337 − 10
appearinginTerminologyC1145applytothetermsusedinthis velop as the result of cumulative damage processes (for
test method. The definitions of terms relating to fiber rein- example, matrix cracking, matrix/fiber debonding, fiber frac-
forced composites appearing in Terminology D3878 apply to ture, delamination, etc.) which may be influenced by testing
the terms used in this test method. Additional terms used in mode, testing rate, processing or alloying effects, environmen-
conjunction with this test method are defined in the following: tal influences, or elevated temperatures. Some of these effects
3.1.2 continuous fiber-reinforced ceramic matrix composite may be consequences of stress corrosion or subcritical (slow)
(CF
...

This document is not anASTM standard and is intended only to provide the user of anASTM standard an indication of what changes have been made to the previous version. Because
it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. In all cases only the current version
of the standard as published by ASTM is to be considered the official document.
Designation:C1337–96 (Reapproved 2005) Designation:C1337–10
Standard Test Method for
Creep and Creep Rupture of Continuous Fiber-Reinforced
Ceramic Composites underAdvanced Ceramics Under
1
Tensile Loading at Elevated Temperatures
This standard is issued under the fixed designation C1337; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope
1.1 This test method covers the determination of the time-dependent deformation and time-to-rupture of continuous
fiber-reinforced ceramic composites under constant tensile loading at elevated temperatures. This test method addresses, but is not
restricted to, various suggested test specimen geometries. In addition, test specimen fabrication methods, allowable bending,
temperature measurements, temperature control, data collection, and reporting procedures are addressed.
1.2 This test method is intended primarily for use with all advanced ceramic matrix composites with continuous fiber
reinforcement: unidirectional (1-D), bidirectional (2-D), and tridirectional (3-D). In addition, this test method may also be used
with glass matrix composites with 1-D, 2-D, and 3-D continuous fiber reinforcement. This test method does not address directly
discontinuous fiber-reinforced, whisker-reinforced, or particulate-reinforced ceramics, although the test methods detailed here may
be equally applicable to these composites.
1.3 Values expressed in this test method are in accordance with the International System of Units (SI) and IEEE/ASTM SI 10
.
1.4 This standard does not purport to address all of the safety concerns, if any, associated with its use. It is the responsibility
of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory
limitations prior to use. Hazard statements are noted in 7.1 and 7.2.
2. Referenced Documents
2
2.1 ASTM Standards:
C1145 Terminology of Advanced Ceramics
C1275 Test Method for Monotonic Tensile Behavior of Continuous Fiber-Reinforced Advanced Ceramics with Solid
Rectangular Cross-Section Test Specimens at Ambient Temperature
D3878 Terminology for Composite Materials
E4 Practices for Force Verification of Testing Machines
E6 Terminology Relating to Methods of Mechanical Testing
E83 Practice for Verification and Classification of Extensometer Systems
E139 Test Methods for Conducting Creep, Creep-Rupture, and Stress-Rupture Tests of Metallic Materials
E220 Test Method for Calibration of Thermocouples By Comparison Techniques
E230 Specification and Temperature-Electromotive Force (EMF) Tables for Standardized Thermocouples
E337 Test Method for Measuring Humidity with a Psychrometer (the Measurement of Wet- and Dry-Bulb Temperatures)
E1012 PracticeforVerificationofTestFrameandSpecimenAlignmentUnderTensileandCompressiveAxialForceApplication
IEEE/ASTM SI 10 American National Standard for Use of the International System of Units (SI): The Modern Metric System
3. Terminology
3.1 Definitions—The definitions of terms relating to tensile testing appearing in Terminology E6 apply to the terms used in this
test method. The definitions relating to advanced ceramics appearing in Terminology C1145 apply to the terms used in this test
method. The definitions of terms relating to fiber reinforced composites appearing in Terminology D3878 apply to the terms used
in this test method. Additional terms used in conjunction with this test method are defined in the following:
1
This test method is under the jurisdiction ofASTM Committee C28 onAdvanced Ceramics and is the direct responsibility of Subcommittee C28.07 on Ceramic Matrix
Composites.
Current edition approved JuneDec. 1, 2005.2010. Published June 2005.January 2011. Originally approved in 1996. Last previous edition approved in 20002005 as
C1337 – 96 (2000).(2005). DOI: 10.1520/C1337-96R05.10.1520/C1337-10.
2
For referencedASTM standards, visit theASTM website, www.astm.org, or contactASTM Customer Service at service@astm.org. For Annual Book of ASTM Standards
volume information, refer to the standard’s Document Summary page on the ASTM website.
Copyright © ASTM International, 100 Barr Harbor Drive, PO Box C700, West Conshohocken, PA 19428-2959, United States.
1

---------------------- Page: 1 ----------------------
C1337–10
3.1.1 continuous fiber-reinforced ceramic matrix composit
...

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