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ASTM D4376-02(2012)

(Specification)

Standard Specification for Vapor-Degreasing Grade Perchloroethylene

Standard Specification for Vapor-Degreasing Grade Perchloroethylene

ABSTRACT
This specification covers the requirements and corresponding test methods for vapor-degreasing grade perchloroethylene. When tested, materials shall conform to the following physical properties: specific gravity; distillation range (initial boiling point and dry point); acidity as HCl; alkalinity as NaOH; water content; appearance; color in Pt-co units; halides content; nonvolatile residues content; acid acceptance; and copper corrosion behavior.
SCOPE
1.1 This specification covers vapor-degreasing grade perchloroethylene.  
Note 1—Guide D3844 and Practice D4276 provide additional important information on solvent properties.
TABLE 1 Physical Properties    PropertySpecificationTest Method Specific gravity, 25/25°C1.606 to 1.625D2111 Distillation range (760 mm Hg)D1078  Initial boiling point, °C, min120.0  Dry point, °C, max125.0 Acidity (as HCl), weight, %, max0.0005D2989 Alkalinity (as NaOH), weight,
%, max0.030D2989 Water, weight, %, max0.0050D3401 AppearanceClear and free
from suspended
matterD3741 Color, Pt-Co, max20D2108 Halide (as Cl−), weight, %, max0.0005D2988 Nonvolatile residue, weight,
%, max0.0050D2109 Acid acceptance, as NaOH,
weight, %, min0.10D2942 Copper corrosion, weight loss,
mg, maxD3316  Flask10  Soxhlet20  Condenser20  Acidity as HCl, max, mL,
NaOH15

General Information

Status
Historical
Publication Date
29-Feb-2012
ICS
25.220.10 - Surface preparation
71.100.99 - Other products of the chemical industry
Technical Committee
D26 - Halogenated Organic Solvents and Fire Extinguishing Agents
Drafting Committee
D26.02 - Vapor Degreasing
Current Stage
Ref Project

Relations

Replaces
ASTM D4376-02(2007) - Standard Specification for Vapor-Degreasing Grade Perchloroethylene
Effective Date
01-Mar-2012
Replaced By
ASTM D4376-15 - Standard Specification for Vapor-Degreasing Grade Perchloroethylene
Effective Date
01-Jun-2015

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ASTM D4376-02(2012) - Standard Specification for Vapor-Degreasing Grade PerchloroethyleneASTM D4376-02(2012) - Standard Specification for Vapor-Degreasing Grade Perchloroethylene
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ASTM D4376-02(2012) - Standard Specification for Vapor-Degreasing Grade Perchloroethylene
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NOTICE: This standard has either been superseded and replaced by a new version or withdrawn.
Contact ASTM International (www.astm.org) for the latest information
Designation:D4376 −02(Reapproved 2012)
Standard Specification for
Vapor-Degreasing Grade Perchloroethylene
This standard is issued under the fixed designation D4376; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope* D3316 Test Method for Stability of Perchloroethylene with
Copper
1.1 This specification covers vapor-degreasing grade per-
2 D3401 Test Methods for Water in Halogenated Organic
chloroethylene.
Solvents and Their Admixtures
NOTE 1—Guide D3844 and Practice D4276 provide additional impor-
D3741 Test Methods for Appearance of Admixtures Con-
tant information on solvent properties.
taining Halogenated Organic Solvents
D3844 Guide for Labeling Chlorinated Hydrocarbon Sol-
2. Referenced Documents
vent Containers
2.1 ASTM Standards:
D4276 Practice for Confined Area Entry
D1078 Test Method for Distillation Range of Volatile Or-
2.2 Other Documents:
ganic Liquids
49 CFR 100 to 199 Department ofTransportation Hazardous
D2108 Test Method for Color of Halogenated Organic
Materials Regulations
Solvents and Their Admixtures (Platinum-Cobalt Scale)
29 CFR 1919.1200 Department of Labor, OSHA Regula-
D2109 Test Methods for Nonvolatile Matter in Halogenated
tions on Hazard Communications
Organic Solvents and Their Admixtures
D2111 Test Methods for Specific Gravity and Density of
3. Properties
Halogenated Organic Solvents and Their Admixtures
3.1 Vapor-degreasing grade perchloroethylene shall con-
D2942 Test Method for Total Acid Acceptance of Haloge-
form to the requirements prescribed in Table 1.
nated Organic Solvents (Nonreflux Methods)
D2988 Test Methods for Water-Soluble Halide Ion in Halo-
4. Packaging and Package Marking
genated Organic Solvents and Their Admixtures
4.1 Package and label industrial or commercial quantities in
D2989 Test Method for Acidity-Alkalinity of Halogenated
accordance with DOT regulations 49 CFR 100 to 199, and in
Organic Solvents and Their Admixtures
accordance with state and local regulations, and with OSHA
regulations found in 29 CFR 1910.1200.
This specification is under the jurisdiction of ASTM Committee D26 on
Halogenated Organic Solvents and Fire Extinguishing Agents and is the direct
5. Keywords
responsibility of Subcommittee D26.02 on Vapor Degreasing.
Current edition approved March 1, 2012. Published June 2012. Originally
5.1 perchloroethylene; tetrachloroethylene; vapor degreas-
approved in 1984. Last previous edition approved in 2007 as D4376 – 02 (2007).
ing
DOI: 10.1520/D4376-02R12.
Contains inhibitors.
For referenced ASTM standards, visit the ASTM website, www.astm.org, or
contact ASTM Customer Service at service@astm.org. For Annua
...

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