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ASTM D2917-07(2021)

(Specification)

Standard Specification for Methyl Isoamyl Ketone

Standard Specification for Methyl Isoamyl Ketone

ABSTRACT
This specification covers the properties and requirements for 98 % grade methyl isoamyl ketone for use in paint, varnish, lacquer, and related products. The material shall be sampled and tested appropriately, and shall conform to properties as to apparent specific gravity, color (Pt-Co scale), distillation (initial boiling and dry points), water content, acidity as acetic acid, and purity.
SCOPE
1.1 This specification covers methyl isoamyl ketone (98 % grade) for use in paint, varnish, lacquer, and related products.  
1.2 The following applies to all specified limits in this standard: for purposes of determining conformance with this standard, an observed value or a calculated value shall be rounded off “to the nearest unit” in the last right-hand digit used in expressing the specification limit, in accordance with the rounding-off method of Practice E29.  
1.3 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
1.4 For specific hazard information and guidance, see the supplier’s Material Safety Data Sheet.  
1.5 This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.

General Information

Status
Published
Publication Date
30-Jun-2021
ICS
87.060.30 - Solvents
Technical Committee
D01 - Paint and Related Coatings, Materials, and Applications
Drafting Committee
D01.35 - Solvents, Plasticizers, and Chemical Intermediates
Current Stage
Ref Project

Relations

Refers
ASTM D1613-06(2012) - Standard Test Method for Acidity in Volatile Solvents and Chemical Intermediates Used in Paint, Varnish, Lacquer, and Related Products
Effective Date
01-Jun-2012
Refers
ASTM D1078-11 - Standard Test Method for Distillation Range of Volatile Organic Liquids
Effective Date
15-Nov-2011
Refers
ASTM D5386-10 - Standard Test Method for Color of Liquids Using Tristimulus Colorimetry
Effective Date
01-Jan-2010
Refers
ASTM D3893-03(2009) - Standard Test Method for Purity of Methyl Amyl Ketone and Methyl Isoamyl Ketone by Gas Chromatography
Effective Date
01-Dec-2009
Refers
ASTM E29-08 - Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
Effective Date
01-Oct-2008
Refers
ASTM D1476-02(2007) - Standard Test Method for Heptane Miscibility of Lacquer Solvents
Effective Date
01-Jun-2007
Refers
ASTM D268-01(2007) - Standard Guide for Sampling and Testing Volatile Solvents and Chemical Intermediates for Use in Paint and Related Coatings and Material
Effective Date
01-Jun-2007
Refers
ASTM D1364-02(2007) - Standard Test Method for Water in Volatile Solvents (Karl Fischer Reagent Titration Method)
Effective Date
01-Jun-2007
Refers
ASTM E29-06b - Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
Effective Date
15-Nov-2006
Refers
ASTM E29-06a - Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
Effective Date
15-Sep-2006
Refers
ASTM E29-06 - Standard Practice for Using Significant Digits in Test Data to Determine Conformance with Specifications
Effective Date
01-May-2006
Refers
ASTM D1613-06 - Standard Test Method for Acidity in Volatile Solvents and Chemical Intermediates Used in Paint, Varnish, Lacquer, and Related Products
Effective Date
01-Apr-2006
Refers
ASTM D5386-05 - Standard Test Method for Color of Liquids Using Tristimulus Colorimetry
Effective Date
15-Oct-2005
Refers
ASTM D1078-05 - Standard Test Method for Distillation Range of Volatile Organic Liquids
Effective Date
15-May-2005
Refers
ASTM D1209-05 - Standard Test Method for Color of Clear Liquids (Platinum-Cobalt Scale)
Effective Date
15-May-2005

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ASTM D2917-07(2021) - Standard Specification for Methyl Isoamyl KetoneASTM D2917-07(2021) - Standard Specification for Methyl Isoamyl Ketone
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ASTM D2917-07(2021) - Standard Specification for Methyl Isoamyl Ketone
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This international standard was developed in accordance with internationally recognized principles on standardization established in the Decision on Principles for the
Development of International Standards, Guides and Recommendations issued by the World Trade Organization Technical Barriers to Trade (TBT) Committee.
Designation: D2917 −07 (Reapproved 2021)
Standard Specification for
Methyl Isoamyl Ketone
This standard is issued under the fixed designation D2917; the number immediately following the designation indicates the year of
original adoption or, in the case of revision, the year of last revision. A number in parentheses indicates the year of last reapproval. A
superscript epsilon (´) indicates an editorial change since the last revision or reapproval.
1. Scope Fischer Reagent Titration Method) (Withdrawn 2021)
D1476 Test Method for Heptane Miscibility of Lacquer
1.1 This specification covers methyl isoamyl ketone (98 %
Solvents (Withdrawn 2021)
grade) for use in paint, varnish, lacquer, and related products.
D1613 Test Method for Acidity in Volatile Solvents and
1.2 The following applies to all specified limits in this
Chemical Intermediates Used in Paint, Varnish, Lacquer,
standard: for purposes of determining conformance with this
and Related Products
standard, an observed value or a calculated value shall be
D3893 Test Method for Purity of Methyl Amyl Ketone and
rounded off “to the nearest unit” in the last right-hand digit
Methyl Isoamyl Ketone by Gas Chromatography
used in expressing the specification limit, in accordance with
D4052 Test Method for Density, Relative Density, and API
the rounding-off method of Practice E29.
Gravity of Liquids by Digital Density Meter
1.3 The values stated in SI units are to be regarded as D5386 Test Method for Color of Liquids Using Tristimulus
Colorimetry
standard. No other units of measurement are included in this
standard. E29 Practice for Using Significant Digits in Test Data to
Determine Conformance with Specifications
1.4 For specific hazard information and guidance, see the
E300 Practice for Sampling Industrial Chemicals
supplier’s Material Safety Data Sheet.
2.2 U.S. Federal Specification:
1.5 This international standard was developed in accor-
PPP-C-2020 Chemicals, Liquid, Dry, and Paste: Packaging
dance with internationally recognized principles on standard-
of
ization established in the Decision on Principles for the
Development of International Standards, Guides and Recom-
3. Properties
mendations issued by the World Trade Organization Technical
3.1 Methyl isoamyl ketone shall conform to the following
Barriers to Trade (TBT) Committee.
requirements:
Apparent specific gravity:
2. Referenced Documents
20/20 °C 0.812 to 0.815
2.1 ASTM Standards: or
25/25 °C 0.809 to 0.812
D268 Guide for Sampling and Testing Volatile Solvents and
Color, Pt-Co scale, max (Note 1) 15
Chemical Intermediates for Use in Paint and Related
Distillation, °C
Coatings and Material (Withdrawn 2021) Initial boiling point, min 140
Dry point, max 148
D1078 Test Method for Distillation Range of Volatile Or-
Water, wt %, max 0.1
ganic Liquids
Acidity as acetic acid, wt %, max 0.02
Purity, wt %, min 98
D1209 Test Method for Color of Clear Liquids (Platinum-
__________________
Cobalt Scale)
NOTE 1—Instrumental Pt-Co color determined by Test Method D5386
D1364 Test Method for Water in Volatile Solvents (Karl
has been shown to have no statistically significant difference from Pt-Co
color determined by Test Method D1209. However, it is not known
whether methyl isoamyl ketone was part of the sample set included in the
This specification is under the jurisdiction of ASTM Committee D01 on Paint
interlaboratory study.
and Related Coatings, Materials, andApplications and is
...

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5.1 In order to calculate the volatile organic content (VOC) of paints containing EPA exempt solvents, it is necessary to know the acetone, methyl acetate, or parachlorobenzotrifluoride content. This gas chromatographic test method provides a simple and direct way for measuring these solvents. Each analyte is measured with respect to a unique internal standard. For acetone, the internal standard used is acetone-d6, for methyl acetate it is methyl acetate-d3, and for PCBTF it is metachlorobenzotrifluoride (MCBTF). These unique analyte/internal standard pairs behave very nearly as single solvents with respect to evaporation rate and adsorption rate onto a coated silica fiber (SPME) but are separable on a gas chromatograph (GC) capillary column. The only critical analytical technique required for successfully performing this test method is the ability of an analyst to weigh a paint sample and internal standard, corresponding to the analyte of interest, into a septum capped vial. After weighing, solvent evaporation has no effect on the final value of the determination. Since whole paint is not injected into the gas chromatograph, the analytical system is never compromised.
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1.1 This test method is for the determination of acetone, methyl acetate, or parachlorobenzotrifluoride (PCBTF), or combination of any of the three, in paints and coatings, by solid phase microextraction (SPME) headspace sampling, and subsequent injection into a gas chromatograph. It has been evaluated for cellulose nitrate, acrylic, and urethane solvent-borne systems. The established working range of this test method is: acetone, 28 to 90 %; methyl acetate, 12 to 22 %; parachlorobenzotrifluoride, 10 to 17 %. There is no reason to believe that it will not work outside these ranges. A minor modification of this test method would make it suitable for the analysis of the same analytes in water-borne coatings (see Note 1).
Note 1: Water-borne paints are internally standardized and diluted with water followed by addition of solid sodium chloride.  
1.2 The values stated in SI units are to be regarded as standard. No other units of measurement are included in this standard.  
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