CEN/TS 17777:2022

Organic and organo-mineral fertilizers - Determination of specific elements

This document specifies references to the methods for the determination of the following specific elements in organic and organo-mineral fertilizers:
—   Determination of the total phosphorus content;
—   Determination of the total potassium content;
—   Determination of the total calcium content;
—   Determination of the total magnesium content;
—   Determination of the total sodium content;
—   Determination of the total sulphur content;
—   Determination of the inorganic arsenic content;
—   Determination of the cadmium content;
—   Determination of the total chromium content;
—   Determination of the total mercury content;
—   Determination of the total nickel content;
—   Determination of the total lead content;
—   Determination of the total copper content;
—   Determination of the total zinc content;
—   Determination of the water-soluble calcium content;
—   Determination of the water-soluble magnesium content;
—   Determination of the water-soluble sodium content;
—   Determination of the water-soluble sulphur content.
This document specifies references to the methods for the determination of the following specific elements in organo-mineral fertilizers:
—   Determination of the water-soluble phosphorus content;
—   Determination of the water-soluble potassium content;
—   Determination of the neutral ammonium citrate soluble phosphorus content
—   Determination of the formic acid soluble phosphorus content;
—   Determination of the total boron content;
—   Determination of the total cobalt content;
—   Determination of the total iron content
—   Determination of the total manganese content
—   Determination of the total molybdenum content;
—   Determination of the water-soluble boron content;
—   Determination of the water-soluble cobalt content;
—   Determination of the water-soluble copper content;
—   Determination of the water-soluble iron content;
—   Determination of the water-soluble manganese content;
—   Determination of the water-soluble molybdenum content;
—   Determination of the water-soluble zinc content.
This document is applicable to fertilizing products, which are classified as PFC 1(A) and PFC 1(B) or the PFC 1(A) and PFC 1(B) component in PFC 7 of Regulation (EU) 2019/1009 [1]. However, the present method was not validated for blends.

Organische und organisch-mineralische Düngemittel - Bestimmung spezifischer Elemente

Engrais organiques et organo-minéraux - Détermination des éléments spécifiques

Le présent document spécifie les références aux méthodes de détermination des éléments spécifiques suivants dans les engrais organiques et organo-minéraux :
—   Détermination de la teneur en phosphore total ;
—   Détermination de la teneur en potassium total ;
—   Détermination de la teneur en calcium total ;
—   Détermination de la teneur en magnésium total ;
—   Détermination de la teneur en sodium total ;
—   Détermination de la teneur en soufre total ;
—   Détermination de la teneur en arsenic inorganique ;
—   Détermination de la teneur en cadmium ;
—   Détermination de la teneur en chrome total ;
—   Détermination de la teneur en mercure total ;
—   Détermination de la teneur en nickel total ;
—   Détermination de la teneur en plomb total ;
—   Détermination de la teneur en cuivre total ;
—   Détermination de la teneur en zinc total ;
—   Détermination de la teneur en calcium soluble dans l'eau ;
—   Détermination de la teneur en magnésium soluble dans l'eau ;
—   Détermination de la teneur en sodium soluble dans l'eau ;
—   Détermination de la teneur en soufre soluble dans l'eau.
Le présent document spécifie les références aux méthodes de détermination des éléments spécifiques suivants dans les engrais organo-minéraux :
—   Détermination de la teneur en phosphore soluble dans l'eau ;
—   Détermination de la teneur en potassium soluble dans l'eau ;
—   Détermination de la teneur en phosphore soluble dans le citrate d'ammonium neutre ;
—   Détermination de la teneur en phosphore soluble dans l'acide formique ;
—   Détermination de la teneur en bore total ;
—   Détermination de la teneur en cobalt total ;
—   Détermination de la teneur en fer total ;
—   Détermination de la teneur en manganèse total ;
—   Détermination de la teneur en molybdène total ;
—   Détermination de la teneur en bore soluble dans l'eau ;
—   Détermination de la teneur en cobalt soluble dans l'eau ;
—   Détermination de la teneur en cuivre soluble dans l'eau ;
—   Détermination de la teneur en fer soluble dans l'eau ;
—   Détermination de la teneur en manganèse soluble dans l'eau ;
—   Détermination de la teneur en molybdène soluble dans l'eau ;
—   Détermination de la teneur en zinc soluble dans l'eau.
Le présent document est applicable aux fertilisants, qui sont classés comme PFC 1(A) et PFC 1(B) ou comme composant PFC 1(A) et PFC 1(B) dans la PFC 7 du règlement (UE) 2019/1009 [1]. Cependant, la présente méthode n'a pas été validée pour les combinaisons.

Organska in organsko-mineralna gnojila - Določevanje specifičnih elementov

Ta dokument vzpostavlja metodologijo za določevanje:
– skupne vsebnosti P2O5, K2O, CaO, MgO, Na2O, SO3 v organskih in organsko-mineralnih gnojilih;
– vsebnosti anorganskega As, Cd, skupni Cr, Hg, Ni, Pb, Cu, Zn v organskih in organsko-mineralnih gnojilih;  
– vsebnosti v vodi topnih CaO, MgO, Na2O, SO3 v organskih in organsko-mineralnih gnojilih;
– vsebnosti v vodi topnega P2O5, K2O v organsko-mineralnih gnojilih;
– vsebnosti P2O5, topnega v nevtralnem amonijevem citratu, v organsko-mineralnih gnojilih;
– vsebnosti P2O5, topnega v metanojski kislini, v organsko-mineralnih gnojilih;
– skupne vsebnosti B, Co, Fe, Mn, Mo v organsko-mineralnih gnojilih;
– vsebnosti v vodi topnih B, Co, Cu, Fe, Mn, Mo in Zn v organsko-mineralnih gnojilih.

General Information

• Status: Published
• Publication Date: 05-Apr-2022
• ICS: 65.080 - Fertilizers
• Technical Committee: CEN/TC 260 - Fertilizers and liming materials
• Drafting Committee: CEN/TC 260/WG 8 - Organic and organo-mineral fertilizers
• Current Stage: 6060 - Definitive text made available (DAV) - Publishing
• Start Date: 06-Apr-2022
• Due Date: 04-Feb-2023
• Completion Date: 06-Apr-2022
• Directive: 2019/1009 - Regulation (EU) 2019/1009 of the European Parliament and of the Council of 5 June 2019 laying down rules on the making available on the market of EU fertilising products and amending Regulations (EC) No 1069/2009 and (EC) No 1107/2009 and repealing Regulation (EC) No 2003/2003
• Mandate: M/564 - Fertilising products in support of Regulation (EU) 2019/1009
• Ref Project: SIST-TS CEN/TS 17777:2023 - Organic and organo-mineral fertilizers - Determination of specific elements

Standards Content (Sample)

SLOVENSKI STANDARD
01-februar-2023
Organska in organsko-mineralna gnojila - Določevanje specifičnih elementov
Organic and organo-mineral fertilizers - Determination of specific elements
Organische und organisch-mineralische Düngemittel - Bestimmung spezifischer
Elemente
Engrais organiques et organo-minéraux - Détermination des éléments spécifiques
Ta slovenski standard je istoveten z: CEN/TS 17777:2022
ICS:
65.080 Gnojila Fertilizers
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

CEN/TS 17777
TECHNICAL SPECIFICATION
SPÉCIFICATION TECHNIQUE
April 2022
TECHNISCHE SPEZIFIKATION
ICS 65.080
English Version
Organic and organo-mineral fertilizers - Determination of
specific elements
Engrais organiques et organo-minéraux - Organische und organisch-mineralische Düngemittel -
Détermination des éléments spécifiques Bestimmung spezifischer Elemente
This Technical Specification (CEN/TS) was approved by CEN on 13 March 2022 for provisional application.

The period of validity of this CEN/TS is limited initially to three years. After two years the members of CEN will be requested to
submit their comments, particularly on the question whether the CEN/TS can be converted into a European Standard.

CEN members are required to announce the existence of this CEN/TS in the same way as for an EN and to make the CEN/TS
available promptly at national level in an appropriate form. It is permissible to keep conflicting national standards in force (in
parallel to the CEN/TS) until the final decision about the possible conversion of the CEN/TS into an EN is reached.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway,
Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and
United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATIO N

EUROPÄISCHES KOMITEE FÜR NORMUN G

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2022 CEN All rights of exploitation in any form and by any means reserved Ref. No. CEN/TS 17777:2022 E
worldwide for CEN national Members.

Contents Page
European foreword . 3
Introduction . 4
1 Scope . 5
2 Normative references . 6
3 Terms and definitions . 7
4 Sampling and sample preparation . 7
5 Determination of specific elements . 7
5.1 Total phosphorus content. 7
5.2 Total potassium content . 7
5.3 Total calcium content . 7
5.4 Total magnesium content . 7
5.5 Total sodium content . 7
5.6 Total sulphur content . 7
5.7 Inorganic arsenic content . 7
5.8 Cadmium content . 8
5.9 Total chromium content . 8
5.10 Total mercury content . 8
5.11 Total nickel content . 8
5.12 Total lead content . 8
5.13 Total copper content . 8
5.14 Total zinc content . 8
5.15 Water-soluble calcium content . 8
5.16 Water-soluble magnesium content . 8
5.17 Water-soluble sodium content . 8
5.18 Water-soluble sulphur content . 8
5.19 Water-soluble phosphorus content . 8
5.20 Water-soluble potassium content . 9
5.21 Neutral ammonium citrate soluble phosphorus content . 9
5.22 Formic acid soluble phosphorus content . 9
5.23 Total boron content . 9
5.24 Total cobalt content . 9
5.25 Total iron content . 9
5.26 Total manganese content . 9
5.27 Total molybdenum content . 9
5.28 Water-soluble boron content . 9
5.29 Water-soluble cobalt content . 9
5.30 Water-soluble copper content . 9
5.31 Water-soluble iron content . 9
5.32 Water-soluble manganese content . 10
5.33 Water-soluble molybdenum content . 10
5.34 Water-soluble zinc content . 10
Bibliography . 11

European foreword
This document (CEN/TS 17777:2022) has been prepared by Technical Committee CEN/TC 260
“Fertilizers and liming materials” the secretariat of which is held by DIN.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
This document has been prepared under a standardization request given to CEN by the European
Commission and the European Free Trade Association.
Any feedback and questions on this document should be directed to the users’ national standards body.
A complete listing of these bodies can be found on the CEN website.
According to the CEN/CENELEC Internal Regulations, the national standards organisations of the
following countries are bound to announce this Technical Specification: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland,
Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Republic of
North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United
Kingdom.
Introduction
Regulation (EU) 2019/1009 [1] lays down the rules on the making available on the market of EU
fertiliz
...