Plastics - Preparation of PVC pastes for test purposes - Planetary-mixer method (ISO 4612:2018)

This document specifies two methods, A and B, for the preparation of pastes (also known as plastisols) from appropriate PVC resins, plasticizers and other ingredients using a planetary mixing process.
Both method A and method B can be used to prepare pastes of any composition. Method A (single-speed) is particularly applicable to resins prone to heat build-up during paste preparation, while method B (two-speed) might be preferred for repetitive work, e.g. for process control during resin manufacture, because of its shorter mixing time.
Such pastes can be used for a variety of test purposes, including the determination of rheological properties for resin designation and specification.

Kunststoffe - Herstellung von PVC-Pasten für Prüfzwecke - Planetenmischerverfahren (ISO 4612:2018)

Dieses Dokument legt zwei Verfahren, A und B, für die Herstellung von Pasten (auch bekannt als Plastisole) fest, hergestellt aus geeigneten PVC Harzen, Weichmachern und anderen Inhaltsstoffen, wobei nach einem Planetenmischerprozess gearbeitet wird.
Beide Verfahren A und B können verwendet werden, um Pasten aller Zusammensetzungen herzustellen. Verfahren A (konstante Rührerdrehzahl) gilt speziell für Harze, die während der Pastenherstellung zu Wärmeaufbau neigen, wohingegen Verfahren B (zwei Rührerdrehzahlen) aufgrund kürzerer Mischzeit für sich wiederholende Arbeiten, z. B. bei der Prozesskontrolle während der Herstellung des Harzes, bevorzugt werden kann.
Solche Pasten können für eine Vielzahl von Prüfzwecken verwendet werden, einschließlich der Bestimmung von rheologischen Eigenschaften für die Kennzeichnung und Spezifizierung von Harzen.

Plastiques - Préparation des pâtes PVC pour essais - Méthodes utilisant un mélangeur planétaire (ISO 4612:2018)

Le présent document spécifie deux méthodes, A et B, pour la préparation des pâtes (encore appelées plastisols) à partir de résines PVC, de plastifiants et autres ingrédients, en utilisant un mélangeur de type planétaire.
Les deux méthodes A et B peuvent être utilisées pour la préparation de pâtes de toute composition. La méthode A (à une seule vitesse) est particulièrement adaptée aux résines qui ont tendance à s'échauffer au cours de la préparation de la pâte, tandis que la méthode B (à deux vitesses) peut avoir la préférence dans le cas de tâches répétitives du fait de sa plus courte durée de mélangeage. C'est le cas, par exemple, lors du contrôle du procédé de fabrication des résines.
Ces pâtes peuvent être utilisées pour une grande variété d'essais, y compris la détermination des propriétés rhéologiques aux fins de désignation et de spécification.

Polimerni materiali - Priprava preskusnih PVC past - Metoda z mešalnikom (planetary mixer) (ISO 4612:2018)

Ta dokument določa dve metodi, A in B, za pripravo past (imenovanih tudi plastisoli) iz ustreznih PVC smol, mehčal in drugih sestavin z uporabo metode z mešalnikom (planetary mixer).
Obe metodi, A in B, je mogoče uporabiti za pripravo past s kakršno koli sestavo. Metoda A (enohitrostna) je še posebej uporabna za smole, ki se med pripravo paste segrevajo, medtem ko je metoda B (dvohitrostna) zaradi krajšega časa mešanja lahko boljša za ponavljajoče se delo, npr. nadzor postopka med proizvodnjo smole.
Take paste je mogoče uporabljati za različne preskusne namene, vključno z določanjem reoloških lastnosti za označevanje in določanje smole.

General Information

Status
Published
Publication Date
18-Dec-2018
Withdrawal Date
29-Jun-2019
Technical Committee
Drafting Committee
Current Stage
6060 - Definitive text made available (DAV) - Publishing
Start Date
19-Dec-2018
Completion Date
19-Dec-2018

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SLOVENSKI STANDARD
01-marec-2019
1DGRPHãþD
SIST EN ISO 4612:2000
Polimerni materiali - Priprava preskusnih PVC past - Metoda z mešalnikom
(planetary mixer) (ISO 4612:2018)
Plastics - Preparation of PVC pastes for test purposes - Planetary-mixer method (ISO
4612:2018)
Kunststoffe - Herstellung von PVC-Pasten für Prüfzwecke - Planetenmischerverfahren
(ISO 4612:2018)
Plastiques - Préparation des pâtes PVC pour essais - Méthodes utilisant un mélangeur
planétaire (ISO 4612:2018)
Ta slovenski standard je istoveten z: EN ISO 4612:2018
ICS:
83.080.20 Plastomeri Thermoplastic materials
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

EN ISO 4612
EUROPEAN STANDARD
NORME EUROPÉENNE
December 2018
EUROPÄISCHE NORM
ICS 83.080.20 Supersedes EN ISO 4612:1999
English Version
Plastics - Preparation of PVC pastes for test purposes -
Planetary-mixer method (ISO 4612:2018)
Plastiques - Préparation des pâtes PVC pour essais - Kunststoffe - Herstellung von PVC-Pasten für
Méthodes utilisant un mélangeur planétaire (ISO Prüfzwecke - Planetenmischerverfahren (ISO
4612:2018) 4612:2018)
This European Standard was approved by CEN on 2 December 2018.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this
European Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references
concerning such national standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN
member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by
translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management
Centre has the same status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and United Kingdom.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2018 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 4612:2018 E
worldwide for CEN national Members.

Contents Page
European foreword . 3

European foreword
This document (EN ISO 4612:2018) has been prepared by Technical Committee ISO/TC 61 "Plastics" in
collaboration with Technical Committee CEN/TC 249 “Plastics” the secretariat of which is held by NBN.
This European Standard shall be given the status of a national standard, either by publication of an
identical text or by endorsement, at the latest by June 2019, and conflicting national standards shall be
withdrawn at the latest by June 2019.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CEN shall not be held responsible for identifying any or all such patent rights.
This document supersedes EN ISO 4612:1999.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the
following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria,
Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia,
France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta,
Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and the United Kingdom.
Endorsement notice
The text of ISO 4612:2018 has been approved by CEN as EN ISO 4612:2018 without any modification.

INTERNATIONAL ISO
STANDARD 4612
Third edition
2018-12
Plastics — Preparation of PVC pastes
for test purposes — Planetary-mixer
method
Plastiques — Préparation des pâtes PVC pour essais — Méthodes
utilisant un mélangeur planétaire
Reference number
ISO 4612:2018(E)
©
ISO 2018
ISO 4612:2018(E)
© ISO 2018
All rights reserved. Unless otherwise specified, or required in the context of its implementation, no part of this publication may
be reproduced or utilized otherwise in any form or by any means, electronic or mechanical, including photocopying, or posting
on the internet or an intranet, without prior written permission. Permission can be requested from either ISO at the address
below or ISO’s member body in the country of the requester.
ISO copyright office
CP 401 • Ch. de Blandonnet 8
CH-1214 Vernier, Geneva
Phone: +41 22 749 01 11
Fax: +41 22 749 09 47
Email: copyright@iso.org
Website: www.iso.org
Published in Switzerland
ii © ISO 2018 – All rights reserved

ISO 4612:2018(E)
Contents Page
Foreword .iv
1 Scope . 1
2 Normative reference . 1
3 Terms and definitions . 1
4 Principle . 1
5 Apparatus and materials. 2
6 Resin sample and conditioning . 2
7 Preparation of paste . 4
7.1 Method A . 4
7.2 Method B . 5
8 Paste-preparation report . 6
ISO 4612:2018(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
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ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
The procedures used to develop this document and those intended for its further maintenance are
described in the ISO/IEC Directives, Part 1. In particular, the different approval criteria needed for the
different types of ISO documents should be noted. This document was drafted in accordance with the
editorial rules of the ISO/IEC Directives, Part 2 (see www .iso .org/directives).
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights. Details of
any patent rights identified during the development of the document will be in the Introduction and/or
on the ISO list of patent declarations received (see www .iso .org/patents).
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expressions related to conformity assessment, as well as information about ISO's adherence to the
World Trade Organization (WTO) principles in the Technical Barriers to Trade (TBT) see www .iso
.org/iso/foreword .html.
This document was prepared by Technical Committee ISO/TC 61, Plastics, Subcommittee SC 9,
Thermoplastic materials.
This third edition cancels and replaces the second edition (ISO 4612:1999), of which it constitutes a
minor revision to update the reference in Clause 2.
Any feedback or questions on this document should be directed to the user’s national standards body. A
complete listing of these bodies can be found at www .iso .org/members .html.
iv © ISO 2018 – All rights reserved

INTERNATIONAL STANDARD ISO 4612:2018(E)
Plastics — Preparation of PVC pastes for test purposes —
Planetary-mixer method
1 Scope
This document specifies two methods, A and B, for the preparation of pastes (also known as plastisols)
from appropriate PVC resins, plasticizers
...

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