EN IEC 60754-3:2019
(Main)Test on gases evolved during combustion of materials from cables - Part 3: Measurement of low level of halogen content by ion chromatography
Test on gases evolved during combustion of materials from cables - Part 3: Measurement of low level of halogen content by ion chromatography
This part of EN 60754 specifies the apparatus and procedure for the measurement of the amount of halogens evolved during the combustion of materials taken from electric or optical fibre cable constructions. The method specified in this document is intended for the measurement of the content of chlorine (Cl), bromine (Br), fluorine (F) and iodine (I), by using the analytical technique of ion chromatography for analysing an aqueous solution resulting from the gases evolved during the combustion. The heating (combustion) procedure in this part of EN 60754 is the same as in EN 60754-2. The method is intended for materials with an individual halogen content not exceeding 10 mg/g. The method specified in this document is intended for the testing of individual components used in a cable construction. The use of this method will enable the verification of requirements which are stated in the appropriate cable specification for individual components of a cable construction. For reasons of precision, this method is not recommended for detecting values of halogens less than 0,1 mg/g of the sample taken.
Prüfung der bei der Verbrennung der Werkstoffe von Kabeln und isolierten Leitungen entstehenden Gase - Teil 3: Messung eines niedrigen Halogengehalts durch Ionenchromatographie
Essai sur les gaz émis lors de la combustion des matériaux prélevés sur câbles - Partie 3: Mesure d’une faible teneur en halogène par chromatographie ionique
L’IEC 60754-3:2018 spécifie l’appareillage et la procédure pour la mesure de la quantité d’halogènes émis lors de la combustion des matériaux prélevés sur un câble électrique ou à fibre optique. La méthode spécifiée dans la présente norme est destinée à mesurer la teneur en chlore (Cl), brome (Br), fluor (F) et iode (I) en utilisant la technique analytique de la chromatographie ionique pour l’analyse d’une solution aqueuse obtenue à partir des gaz dégagés pendant la combustion. La procédure de chauffage (combustion) dans cette partie de l’IEC 60754 est identique à celle utilisée dans l’IEC 60754-2. Cette méthode est destinée aux matériaux dont la teneur individuelle en halogène ne dépasse pas 10 mg/g. La méthode spécifiée dans la présente norme est destinée à l’essai des composants individuels utilisés dans la fabrication d’un câble. L’emploi de cette méthode d’essai permettra de vérifier les exigences indiquées dans la spécification appropriée du câble pour les composants individuels d’un câble. Pour des raisons de précision, l’utilisation de cette méthode n’est pas recommandée pour détecter des valeurs d’halogènes inférieures à 0,1 mg/g de l’échantillon prélevé.
Ugotavljanje nastajanja plinov pri gorenju kabelskih materialov - 3. del: Merjenje majhne koncentracije halogenov z ionsko kromatografijo (IEC 60754-3:2018)
Ta del standarda EN 60754 določa napravo in postopek za merjenje količine halogenov, nastalih pri gorenju materialov iz konstrukcij električnih ali optičnih kablov.
Metoda, določena v tem dokumentu, je namenjena merjenju vsebnosti klora (Cl), broma (Br), fluora (F) in joda (I) v plinih, ki se razvijajo med zgorevanjem, z analitično tehniko ionske kromatografije za analizo vodne raztopine.
Postopek segrevanja (zgorevanja) v tem delu standarda EN 60754 je enak kot v standardu EN 60754-2.
Metoda je namenjena za materiale z vsebnostjo halogena do 10 mg/g.
Metoda, določena v tem dokumentu, je namenjena preskušanju posameznih komponent, ki se uporabljajo pri konstrukciji kablov. Uporaba te metode bo omogočila preverjanje zahtev, ki so navedene v ustrezni specifikaciji kablov za posamezne komponente konstrukcij kablov.
Zaradi natančnosti ta metoda ni priporočljiva za zaznavanje vrednosti halogenov, manjših od 0,1 mg/g v odvzetem vzorcu.
General Information
Standards Content (Sample)
SLOVENSKI STANDARD
01-november-2019
Ugotavljanje nastajanja plinov pri gorenju kabelskih materialov - 3. del: Merjenje
majhne koncentracije halogenov z ionsko kromatografijo (IEC 60754-3:2018)
Test on gases evolved during combustion of materials from cables - Part 3:
Measurement of low level of halogen content by ion chromatography (IEC 60754-3:2018)
Prüfung der bei der Verbrennung der Werkstoffe von Kabeln und isolierten Leitungen
entstehenden Gase - Teil 3: Messung eines niedrigen Halogengehalts durch
Ionenchromatographie (IEC 60754-3:2018)
Essai sur les gaz émis lors de la combustion des matériaux prélevés sur câbles - Partie
3: Mesure d’une faible teneur en halogène par chromatographie ionique (IEC 60754-
3:2018)
Ta slovenski standard je istoveten z: EN IEC 60754-3:2019
ICS:
13.220.40 Sposobnost vžiga in Ignitability and burning
obnašanje materialov in behaviour of materials and
proizvodov pri gorenju products
29.060.20 Kabli Cables
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.
EUROPEAN STANDARD EN IEC 60754-3
NORME EUROPÉENNE
EUROPÄISCHE NORM
August 2019
ICS 13.220.40; 29.060.20
English Version
Test on gases evolved during combustion of materials from
cables - Part 3: Measurement of low level of halogen content by
ion chromatography
(IEC 60754-3:2018)
Essai sur les gaz émis lors de la combustion des matériaux Prüfung der bei der Verbrennung der Werkstoffe von
prélevés sur câbles - Partie 3: Mesure d'une faible teneur Kabeln und isolierten Leitungen entstehenden Gase -
en halogène par chromatographie ionique Teil 3: Messung eines niedrigen Halogengehalts durch
(IEC 60754-3:2018) Ionenchromatographie
(IEC 60754-3:2018)
This European Standard was approved by CENELEC on 2019-07-19. CENELEC members are bound to comply with the CEN/CENELEC
Internal Regulations which stipulate the conditions for giving this European Standard the status of a national standard without any alteration.
Up-to-date lists and bibliographical references concerning such national standards may be obtained on application to the CEN-CENELEC
Management Centre or to any CENELEC member.
This European Standard exists in three official versions (English, French, German). A version in any other language made by translation
under the responsibility of a CENELEC member into its own language and notified to the CEN-CENELEC Management Centre has the
same status as the official versions.
CENELEC members are the national electrotechnical committees of Austria, Belgium, Bulgaria, Croatia, Cyprus, the Czech Republic,
Denmark, Estonia, Finland, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, the
Netherlands, Norway, Poland, Portugal, Republic of North Macedonia, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland,
Turkey and the United Kingdom.
European Committee for Electrotechnical Standardization
Comité Européen de Normalisation Electrotechnique
Europäisches Komitee für Elektrotechnische Normung
CEN-CENELEC Management Centre: Rue de la Science 23, B-1040 Brussels
© 2019 CENELEC All rights of exploitation in any form and by any means reserved worldwide for CENELEC Members.
Ref. No. EN IEC 60754-3:2019 E
European foreword
This document (EN IEC 60754-3:2019) consists of the text of IEC 60754-3:2018 prepared by
IEC/TC 20 "Electric cables".
The following dates are fixed:
latest date by which this document has to be
• (dop) 2020-07-19
implemented at national level by publication of an
identical national standard or by endorsement
• latest date by which the national standards (dow) 2022-07-19
conflicting with this document have to be
withdrawn
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. CENELEC shall not be held responsible for identifying any or all such patent rights.
Endorsement notice
The text of the International Standard IEC 60754-3:2018 was approved by CENELEC as a European
Standard without any modification.
In the official version, for Bibliography, the following notes have to be added for the standards
indicated:
IEC 60684-2 NOTE Harmonized as EN 60684-2
IEC 60695-5-1 NOTE Harmonized as EN 60695-5-1
IEC 60754-1 NOTE Harmonized as EN 60754-1
IEC 60754-2 NOTE Harmonized as EN 60754-2
IEC 62321-3-2 NOTE Harmonized as EN 62321-3-2
Annex ZA
(normative)
Normative references to international publications
with their corresponding European publications
The following documents are referred to in the text in such a way that some or all of their content
constitutes requirements of this document. For dated references, only the edition cited applies. For
undated references, the latest edition of the referenced document (including any amendments)
applies.
NOTE 1 When an International Publication has been modified by common modifications, indicated by (mod), the relevant
EN/HD applies.
NOTE 2 Up-to-date information on the latest versions of the European Standards listed in this annex is available here:
www.cenelec.eu.
Publication Year Title EN/HD Year
ISO 1042 - Laboratory glassware - One-mark EN ISO 1042 -
volumetric flasks
ISO 3696 - Water for analytical laboratory use - EN ISO 3696 -
Specification and test methods
ISO 10304-1 - Water quality -- Determination of dissolved EN ISO 10304-1 -
anions by liquid chromatography of ions --
Part 1: Determination of bromide, chloride,
fluoride, nitrate, nitrite, phosphate and
sulfate
IEC 60754-3 ®
Edition 1.0 2018-03
INTERNATIONAL
STANDARD
Test on gases evolved during combustion of materials from cables –
Part 3: Measurement of low level of halogen content by ion chromatography
INTERNATIONAL
ELECTROTECHNICAL
COMMISSION
ICS 13.220.40; 29.060.20 ISBN 978-2-8322-5484-4
– 2 – IEC 60754-3:2018 © IEC 2018
CONTENTS
FOREWORD . 4
INTRODUCTION . 6
1 Scope . 7
2 Normative references . 7
3 Terms and definitions . 7
4 Test method principle . 8
5 Test apparatus . 8
5.1 General . 8
5.2 Tube furnace . 8
5.3 Quartz glass tube . 9
5.4 Combustion boat . 9
5.5 Bubbling devices for gases . 9
5.6 Air supply system . 10
5.7 Analytical balance . 10
5.8 Laboratory glassware . 10
5.9 Ion chromatographic system . 11
6 Test specimen . 11
6.1 General . 11
6.2 Conditioning of specimen . 11
6.3 Mass of specimen . 11
7 Test procedure . 11
7.1 General . 11
7.2 Blank test . 12
7.3 Test apparatus and arrangement . 12
7.4 Heating procedure . 12
7.5 Washing procedure . 12
7.6 Measurement of the halogens . 12
8 Evaluation of the test results . 13
9 Performance requirement . 13
10 Test report . 13
Annex A (informative) Recommended use and performance requirements . 20
A.1 Recommended use . 20
A.1.1 General . 20
A.1.2 Recommended use of IEC 60754-1, IEC 60754-2 and IEC 60754-3 . 21
A.2 Recommended performance requirements to assess materials described as
"halogen free" . 21
Bibliography . 22
Figure 1 – Device for inserting combustion boat and test specimen . 14
Figure 2 – Example of a gas washing bottle . 15
Figure 3 – Test apparatus: method 1 – Use of synthetic or compressed air from a bottle . 16
Figure 4 – Test apparatus: method 2 – Use of laboratory compressed air supply . 17
Figure 5 – Test apparatus: method 3 – Use of ambient air sucked by means of a
suction pump . 18
Figure 6 – Example of ion chromatographic system . 19
IEC 60754-3:2018 © IEC 2018 – 3 –
Table A.1 – Scope and recommended use of IEC 60754-1, IEC 60754-2 and
IEC 60754-3 . 21
Table A.2 – Recommended performance requirements to assess materials described
as "halogen free" . 21
– 4 – IEC 60754-3:2018 © IEC 2018
INTERNATIONAL ELECTROTECHNICAL COMMISSION
____________
TEST ON GASES EVOLVED DURING
COMBUSTION OF MATERIALS FROM CABLES –
Part 3: Measurement of low level of halogen
content by ion chromatography
FOREWORD
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