IEC 60811-605:2012

Electric and optical fibre cables - Test methods for non-metallic materials - Part 605: Physical tests - Measurement of carbon black and/or mineral filler in polyethylene compounds

IEC 60811-605:2012 describes the test methods for measuring the content of carbon black added for UV stabilization of polyethylene and polyolefin compounds. These methods are not suitable for halogenated compounds. Method A is suitable only for polyethylene and polypropylene compounds. Method B is suitable for polyolefine compounds. IEC 60811-605:2012 cancels and replaces Clauses 11 and 12 of IEC 60811-4-1:2004, which is withdrawn. Full details of the replacements are shown in Annex A of IEC 60811-100:2012. There are no specific technical changes with respect to the previous edition, but see the foreword to IEC 60811-100:2012.
This publication is to be read in conjunction with IEC 60811-100:2012.

Câbles électriques et à fibres optiques - Méthodes d'essai pour les matériaux non-métalliques - Partie 605: Essais physiques - Mesure du taux de noir de carbone et/ou des charges minérales dans les mélanges en polyéthylène

La CEI 60811-605:2012 décrit les méthodes d'essai pour la mesure du taux de noir de carbone ajouté pour assurer la résistance aux UV des mélanges à base de polyéthylène et polyoléfine. Ces méthodes ne sont pas adaptées aux mélanges halogénés. La méthode A est applicable uniquement aux mélanges à base de polyéthylène et de polypropylène. La méthode B est applicable aux mélanges à base de polyoléfine. La CEI 60811-605:2012 annule et remplace les Articles 11 et 12 de la CEI 60811-4-1:2004, qui est supprimée. L'ensemble des informations relatives aux remplacements figure dans l'Annexe A de la CEI 60811-100:2012. Aucune modification technique n'a été effectuée par rapport à l'édition précédente; voir cependant l'avant-propos de la CEI 60811-100:2012.
Cette publication doit être lue conjointement avec la CEI 60811-100:2012.

General Information

• Status: Published
• Publication Date: 12-Mar-2012
• ICS: 01 - GENERALITIES. TERMINOLOGY. STANDARDIZATION. DOCUMENTATION
• ICS: 29.035.01 - Insulating materials in general
• ICS: 29.060.20 - Cables
• Technical Committee: TC 20 - Electric cables
• Drafting Committee: WG 17 - TC 20/WG 17
• Current Stage: PPUB - Publication issued
• Start Date: 31-Mar-2012
• Completion Date: 13-Mar-2012

Relations

• Replaces: IEC 60811-4-1:2004 - Insulating and sheathing materials of electric and optical cables - Common test methods - Part 4-1: Methods specific to polyethylene and polypropylene compounds - Resistance to environmental stress cracking - Measurement of the melt flow index - Carbon black and/or mineral filler content measurement in polyethylene by direct combustion - Measurement of carbon black content by thermogravimetric analysis (TGA) - Assessment of carbon black dispersion in polyethylene using a microscope
• Effective Date: 05-Sep-2023

Standards Content (Sample)

IEC 60811-605 ®
Edition 1.0 2012-03
INTERNATIONAL
STANDARD
NORME
INTERNATIONALE
Electric and optical fibre cables – Test methods for non-metallic materials –
Part 605: Physical tests – Measurement of carbon black and/or mineral filler
in polyethylene compounds
Câbles électriques et à fibres optiques – Méthodes d’essai pour les matériaux
non-métalliques –
Partie 605: Essais physiques – Mesure du taux de noir de carbone et/ou des
charges minérales dans les mélanges en polyéthylène

All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized in any form
or by any means, electronic or mechanical, including photocopying and microfilm, without permission in writing from
either IEC or IEC's member National Committee in the country of the requester.
If you have any questions about IEC copyright or have an enquiry about obtaining additional rights to this publication,
please contact the address below or your local IEC member National Committee for further information.

Droits de reproduction réservés. Sauf indication contraire, aucune partie de cette publication ne peut être reproduite ni
utilisée sous quelque forme que ce soit et par aucun procédé, électronique ou mécanique, y compris la photocopie et les
microfilms, sans l'accord écrit de la CEI ou du Comité national de la CEI du pays du demandeur.
Si vous avez des questions sur le copyright de la CEI ou si vous désirez obtenir des droits supplémentaires sur cette
publication, utilisez les coordonnées ci-après ou contactez le Comité national de la CEI de votre pays de résidence.

IEC Central Office Tel.: [phone]
3, rue de Varembé Fax: [phone]
CH-1211 Geneva 20 [e-mail]
Switzerland www.iec.ch
About the IEC
The International Electrotechnical Commission (IEC) is the leading global organization that prepares and publishes
International Standards for all electrical, electronic and related technologies.

About IEC publications
The technical content of IEC publications is kept under constant review by the IEC. Please make sure that you have the
latest edition, a corrigenda or an amendment might have been published.

Useful links:
IEC publications search - www.iec.ch/searchpub Electropedia - www.electropedia.org
The advanced search enables you to find IEC publications The world's leading online dictionary of electronic and
by a variety of criteria (reference number, text, technical electrical terms containing more than 30 000 terms and
committee,…). definitions in English and French, with equivalent terms in
It also gives information on projects, replaced and additional languages. Also known as the International
withdrawn publications. Electrotechnical Vocabulary (IEV) on-line.

IEC Just Published - webstore.iec.ch/justpublished Customer Service Centre - webstore.iec.ch/csc
Stay up to date on all new IEC publications. Just Published If you wish to give us your feedback on this publication
details all new publications released. Available on-line and or need further assistance, please contact the
also once a month by email. Customer Service Centre: [e-mail].

A propos de la CEI
La Commission Electrotechnique Internationale (CEI) est la première organisation mondiale qui élabore et publie des
Normes internationales pour tout ce qui a trait à l'électricité, à l'électronique et aux technologies apparentées.

A propos des publications CEI
Le contenu technique des publications de la CEI est constamment revu. Veuillez vous assurer que vous possédez
l’édition la plus récente, un corrigendum ou amendement peut avoir été publié.

Liens utiles:
Recherche de publications CEI - www.iec.ch/searchpub Electropedia - www.electropedia.org
La recherche avancée vous permet de trouver des Le premier dictionnaire en ligne au monde de termes
publications CEI en utilisant différents critères (numéro de électroniques et électriques. Il contient plus de 30 000
référence, texte, comité d’études,…). termes et définitions en anglais et en français, ainsi que
Elle donne aussi des informations sur les projets et les les termes équivalents dans les langues additionnelles.
publications remplacées ou retirées. Egalement appelé Vocabulaire Electrotechnique
International (VEI) en ligne.
Just Published CEI - webstore.iec.ch/justpublished
Service Clients - webstore.iec.ch/csc
Restez informé sur les nouvelles publications de la CEI.
Just Published détaille les nouvelles publications parues. Si vous désirez nous donner des commentaires sur
Disponible en ligne et aussi une fois par mois par email. cette publication ou si vous avez des questions
contactez-nous: [e-mail].
IEC 60811-605 ®
Edition 1.0 2012-03
INTERNATIONAL
STANDARD
NORME
INTERNATIONALE
Electric and optical fibre cables – Test methods for non-metallic materials –

Part 605: Physical tests – Measurement of carbon black and/or mineral filler

in polyethylene compounds
Câbles électriques et à fibres optiques – Méthodes d’essai pour les matériaux

non-métalliques –
Partie 605: Essais physiques – Mesure du taux de noir de carbone et/ou des

charges minérales dans les mélanges en polyéthylène

INTERNATIONAL
ELECTROTECHNICAL
COMMISSION
COMMISSION
ELECTROTECHNIQUE
PRICE CODE
INTERNATIONALE
CODE PRIX J
ICS 29.035.01; 29.060.20 ISBN 978-2-88912-998-0

– 2 – 60811-605  IEC:2012
CONTENTS
FOREWORD . 3
INTRODUCTION . 5
1 Scope . 6
2 Normative references . 6
3 Terms and definitions . 6
4 Test method . 6
4.1 General . 6
4.2 Method A – Measurement of carbon black and/or mineral filler content in
polyethylene by direct combustion . 6
4.2.1 Sample and test piece preparation . 6
4.2.2 Test procedure . 6
4.2.3 Expression of results . 7
4.3 Method B – Thermogravimetric analysis of the carbon black content in
polyolefin compounds . 7
4.3.1 Principle . 7
4.3.2 Reagents . 8
4.3.3 Apparatus . 8
4.3.4 Procedure . 8
5 Test report. 8
Bibliography . 9

60811-605  IEC:2012 – 3 –
INTERNATIONAL ELECTROTECHNICAL COMMISSION
____________
ELECTRIC AND OPTICAL FIBRE CABLES –
TEST METHODS FOR NON-METALLIC MATERIALS –

Part 605: Physical tests –
Measurement of carbon black and/or mineral filler
in polyethylene compounds
FOREWORD
1) The International Electrotechnical Commission (IEC) is a worldwide organization for standardization comprising
all national electrotechnical committees (IEC National Committees). The object of IEC is to promote
international co-operation on all questions concerning standardization in the electrical and electronic fields. To
this end and in addition to other activities, IEC publishes International Standards, Technical Specifications,
Technical Reports, Publicly Available Specifications (PAS) and Guides (hereafter referred to as “IEC
Publication(s)”). Their preparation is entrusted to technical committees; any IEC National Committee interested
in the subject dealt with may participate in this preparatory work. International, governmental and non-
governmental organizations liaising with the IEC also participate in this preparation. IEC collaborates closely
with the International Organization for Standardization (ISO) in accordance with conditions determined by
agreement between the two organizations.
2) The formal decisions or agreements of IEC on technical matters express, as nearly as possible, an international
consensus of opinion on the relevant subjects since each technical committee has representation from all
interested IEC National Committees.
3) IEC Publications have the form of recommendations for international use and are accepted by IEC National
Committees in that sense. While all reasonable efforts are made to ensure that the technical content of IEC
Publications is accurate, IEC cannot be held responsible for the way in which they are used or for any
misinterpretation by any end user.
4) In order to promote international uniformity, IEC National Committees undertake to apply IEC Publications
transparently to the maximum extent possible in their national and regional publications. Any divergence
between any IEC Publication and the corresponding national or regional publication shall be clearly indicated in
the latter.
5) IEC itself does not provide any attestation of conformity. Independent certification bodies provide conformity
assessment services and, in some areas, access to IEC marks of conformity. IEC is not responsible for any
services carried out by independent certification bodies.
6) All users should ensure that they have the latest edition of this publication.
7) No liability shall attach to IEC or its directors, employees, servants or agents including individual experts and
members of its technical committees and IEC National Committees for any personal injury, property damage or
other damage of any nature whatsoever, whether direct or indirect, or for costs (including legal fees) and
expenses arising out of the publication, use of, or reliance upon, this IEC Publication or any other IEC
Publications.
8) Attention is drawn to the Normative references cited in this publication. Use of the referenced publications is
indispensable for the correct application of this publication.
9) Attention is drawn to the possibility that some of the elements of this IEC Publication may be the subject of
patent rights. IEC shall not be held responsible for identifying any or all such patent rights.
International Standard IEC 60811-605 has been prepared by IEC technical committee 20:
Electric cables.
This Part 605 of IEC 60811 cancels and replaces Clauses 11 and 12 of IEC 60811-4-1:2004,
which is withdrawn. Full details of the replacements are shown in Annex A of
IEC 60811-100:2012.
There are no specific technical changes with respect to the previous edition, but see the
foreword to IEC 60811-100:2012.

– 4 – 60811-605  IEC:2012
The text of this standard is based on the following documents:
FDIS Report on voting
20/1314/FDIS 20/1363/RVD
Full information on the voting for the approval of this standard can be found in the report on
voting indicated in the above table.
This publication has been drafted in accordance with the ISO/IEC Directives, Part 2.
This part of IEC 60811 shall be used in conjunction with IEC 60811-100.
A list of all the parts in the IEC 60811 series, published under the general title Electric and
optical fibre cables – Test methods for non-metallic materials, can be found on the IEC
website.
The committee has decided that the contents of this publication will remain unchanged until
the stability date indicated on the IEC web site under "http://webstore.iec.ch" in the data
related to the specific publication. At this date, the publication will be
• reconfirmed,
• withdrawn,
• replaced by a revised edition, or
• amended.
60811-605  IEC:2012 – 5 –
INTRODUCTION
The IEC 60811 series specifies the test methods to be used for testing non-metallic materials
of all types of cables. These test methods are intended to be referenced in standards for
cable construction and for cable materials.
NOTE 1 Non-metallic materials are typically used for insulating, sheathing, bedding, filling or taping within cables.
NOTE 2 These test methods are accepted as basic and fundamental and have been developed and used over
many years principally for the materials in all energy cables. They have also been widely accepted and used for
other cables, in particular optical fibre cables, communication and control cables and cables for ships and offshore
applications.
– 6 – 60811-605  IEC:2012
ELECTRIC AND OPTICAL FIBRE CABLES –
TEST METHODS FOR NON-METALLIC MATERIALS –

Part 605: Physical tests –
Measurement of carbon black and/or mineral filler
in polyethylene compounds
1 Scope
This Part 605 of IEC 60811 describes the test methods for measuring the content of carbon
black added for UV stabilization of polyethylene and polyolefin compounds. These methods
are not suitable for halogenated compounds.
Method A is suitable only for polyethylene and polypropylene compounds.
Method B is suitable for
...